Hach PHC735 Скачать руководство пользователя страница 11

Section 6 Sample measurement

The procedure that follows is applicable to meters that can connect to Intellical pH probes. Refer to
the applicable meter documentation for meter operation and probe-specific settings.

6.1 Sample requirements

N O T I C E

 

Make sure that the sample type is compatible with the probe, or probe damage can occur.

• Samples must be aqueous. The probe can also make measurements in samples that are not fully

aqueous and in some solvents that dissolve in water. Read the results with caution because the
pH scale changes when the solvent system changes.

• Samples can contain components that react with silver (e.g., TRIS, proteins and sulfides). The

Red Rod tubes protect the probe from interference with such components.

• Proteins can collect on the sensing element. Make sure that the probe stays clean if proteins are in

the sample.

• Do not measure samples that are hotter or colder than the specified operating temperature of the

probe. Refer to 

Specifications

 on page 3.

• High purity or low ionic strength (LIS) samples absorb gases from the air that can change the

sample pH. For stable measurements, use an LIS chamber or a flow cell.

6.2 Sample measurement notes

Read the notes that follow before sample measurements.

• Rinse the probe with deionized water and dry with a lint-free cloth between measurements to

prevent contamination.

• If complete traceability is necessary, enter a sample ID and operator ID before measurement.

Refer to the meter manual for instructions.

• The meter automatically saves the measurement data when the user manually reads each data

point and when the meter is set to read at regular intervals. The user must manually save each
data point when the meter is set to read continuously.

• Air bubbles below the sensor can cause a slow response or error in the measurement. Make sure

to remove air bubbles before and during measurements.

6.3 Sample measurement procedure

1. 

 Collect the

sample.

2. 

 Open the filling

hole.

3. 

 Rinse the probe

with deionized water.
Dry the probe with a
lint-free cloth.

4. 

 Put the probe in

the sample with the
sensor and
reference junction
fully in the sample.
Do not put the probe
on the bottom or
sides of the beaker.

English

   

9

Содержание PHC735

Страница 1: ...DOC022 53 80434 PHC735 05 2021 Edition 2 User Manual...

Страница 2: ......

Страница 3: ...rocedure 8 Section 6 Sample measurement 9 6 1 Sample requirements 9 6 2 Sample measurement notes 9 6 3 Sample measurement procedure 9 Section 7 Verify the calibration 10 7 1 Verification procedure 10...

Страница 4: ...Table of Contents 2...

Страница 5: ...kaline samples Figure 1 Probe overview 1 Probe soaker bottle with storage solution 5 Probe soaker bottle holder 2 Filling hole plug 6 Electrode filling and storage solution 3 Protective tape and filli...

Страница 6: ...nufacturing defects but not improper use or wear Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical probes are intended for use by individuals who measure water qu...

Страница 7: ...probe with a blocked filling hole will not operate correctly New probes are filled with electrolyte filling solution and have a soaker bottle that contains storage solution to keep the glass bulb and...

Страница 8: ...e meter starts for the first time or after battery replacement 8 Connect the probe to the meter 9 Remove the filling hole plug before use Keep the level of the electrolyte filling solution above the l...

Страница 9: ...e pH units apart For a one point calibration use a pH buffer near the expected sample pH Use the default calibration options or change the options in the probe settings menu Use the single display mod...

Страница 10: ...ffer solution Make sure that the sensor and reference junction are fully in the solution Do not put the probe on the bottom or sides of the beaker 6 Shake the probe from side to side to refresh the re...

Страница 11: ...purity or low ionic strength LIS samples absorb gases from the air that can change the sample pH For stable measurements use an LIS chamber or a flow cell 6 2 Sample measurement notes Read the notes...

Страница 12: ...res the selected pH buffer value to the measured pH value and accepts or rejects the measurement The user can change the pH buffer solution and acceptance criteria for verification in the probe specif...

Страница 13: ...ample material stays on the probe 1 Rinse the probe with deionized water Use warm 35 45 C 95 113 F deionized water to remove storage solution that dries on the probe Dry the probe body with a lint fre...

Страница 14: ...nctions Electrode cleaning solution for porous pin diaphragm reference junctions Thiourea 3 hours with stirring or until the porous plug becomes white 8 2 Fill the probe Add electrolyte filling soluti...

Страница 15: ...s less than 0 5 cm 0 2 in or when the sample temperature is more than 60 C 140 F Refer to Figure 5 and Table 2 for preparation Mix some of the filling solution with the crystals to help move the cryst...

Страница 16: ...d KCl crystals from the probe as possible Discard the solution and KCl crystals 3 Remove the remaining KCl crystals as follows a Fill the probe half full with deionized water Close the filling hole b...

Страница 17: ...N O T I C E Probes can become permanently damaged if kept in a storage solution that is not specified by the manufacturer Use only the specified storage solution saturated KCl Do not store the probe i...

Страница 18: ...ilization or inaccurate measurements The sample absorbs carbon dioxide CO2 from the air which causes the pH value to slowly decrease in low ionic strength LIS or high purity samples Use the LIS chambe...

Страница 19: ...Item no pH 4 01 buffer solution Singlet one use packets 20 mL each 20 pkg 2770020 pH 7 00 buffer solution Singlet one use packets 20 mL each 20 pkg 2770120 pH 10 01 buffer solution Singlet one use pac...

Страница 20: ...pkg SM5010 Beaker 30 mL plastic red 80 pkg SM5011 Beaker 30 mL plastic yellow 80 pkg SM5012 Beaker 30 mL plastic blue 80 pkg SM5013 Beaker 30 mL plastic green 80 pkg SM5014 Beaker dispenser and holder...

Страница 21: ......

Страница 22: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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