Hach MTC10101 Скачать руководство пользователя страница 13

DOC272.53.80033

13

Troubleshooting

Message or 
symptom

Possible cause

Action

Probe not supported

Software not updated

Update the HQd software to the newest revision at 

www.hach.com/SoftwareDownloads

. Refer to the HQd 

Series Meter Manual.

HQd meter does not support IntelliCAL 
probe.

Contact a Hach Technical Support Representative.

Connect a probe or 
Probe requires 
service

Electrode not connected properly

Disconnect, then connect the electrode. Tighten the 
locking nut.

Software not updated

Update the HQd software to the newest revision at 

www.hach.com/download-resources

.

Damaged electrode

Verify connectivity with another electrode or meter to 
confirm isolated issue with the electrode. Contact a Hach 
Technical Representative.

Large number of methods stored on 
probe.

Continue to let probe connect. Do not disconnect probe. 

Standard not 
recognized error

Storage cap not removed.

Remove storage cap.

Incorrect or contaminated standard 
solution

Use fresh standard solution as specified in
the method.

mV reading is same 
for all solutions

Storage cap not removed

Remove the storage cap.

Electrical issue

Contact a Hach Technical Support Representative.

Slow response time

Contaminated reference junctions

Rinse reference junction with deionized water thoroughly, 
shake the electrode downward to remove any air bubbles 
and soak in 3.0 M KCl storage solution for 1-2 hours.

Contaminated platinum sensor

Clean the electrode.

Electrode not conditioned/pre-treated 
for reducing type samples

To significantly reduce the response time for reducing type 
samples the platinum disc must undergo the following:
--The platinum disc must be clean and smooth.
--Immerse the platinum disc for 3-10 minutes in Reducing 
Solution for ORP Electrodes prior to sample analysis.
--Rinse the electrode with sample, then measure. 

Low sample temperature or 
temperature difference between 
samples.

Check the sample temperature. The lower the 
temperature or the greater the difference of temperatures 
between samples, traditionally the longer the response 
time.

Platinum electrode not conditioned for 
reducing-type samples.

The platinum disc must be clean and smooth.
Immerse the platinum disc for 3-10 minutes in Reducing 
Solution for ORP Electrodes prior to sample analysis.
Rinse the electrode with sample, then measure. 

Out of range

Measure value is outside the 
calibration/measurement range of the 
electrode.

Recalibrate using freshly prepared standards

Clean the electrode and recalibrate

Verify that the sample is within the range of the electrode

Содержание MTC10101

Страница 1: ...EC European electrical equipment users must now return old or end of life equipment to the Producer for disposal at no charge to the user Note For return for recycling please contact the equipment pr...

Страница 2: ...int free cloth 4 If the electrode will not be used immediately fill the storage cap halfway with Hach Electrode Storage Solution or 3M KCl and install the cap 5 Install the shroud and locking ring and...

Страница 3: ...be must have the correct service life time stamp Set the date and time in the meter before attaching the probe It is not necessary to recalibrate when moving a probe from one HQd meter to another if t...

Страница 4: ...er blot dry and place it in the standard solution Make sure that the sample level is above the reference junction 5 Push Read Stir gently The display will show Stabilizing and a progress bar as the pr...

Страница 5: ...estion mark until the electrode is recalibrated Recalibrate the electrode to correct the status indicator Calibration on page 3 Measurement Measurement notes Data is stored automatically in the data l...

Страница 6: ...nect the electrode to the meter 3 Rinse the electrode with the sample and place the electrode in fresh sample 4 Push Read The display will show Stabilizing and a progress bar as the probe stabilizes i...

Страница 7: ...ng many substances in solution A redox titration consists of adding to an unknown sample small increments of a titrant that converts the unknown to a different oxidation state After each addition of t...

Страница 8: ...ng the potential after each addition Near the end point when large potential changes appear add increments of 0 1 0 2 mL Continue the titration 3 4 mL past the end point 5 Plot the electrode potential...

Страница 9: ...d 1 Unscrew the locking ring and slide the shroud and locking ring off the probe 2 Slide the shroud and locking ring off the probe To install the shroud 1 Place the locking ring on the probe body with...

Страница 10: ...ings which cannot be changed A saved method can be used instead of repeatedly adjusting individual settings Changes made to a user defined method are automatically saved with the existing name Multipl...

Страница 11: ...V The measurement limits can be set to match the acceptable values for the sample When the measurement is above the upper limit setting or below the lower limit setting the meter will show an Out of l...

Страница 12: ...200 0 mV Custom standard value Custom standards are characterized at 25 C Table 4 Calibration options settings Settings Option Description Table 5 Check standard options settings Settings Options Desc...

Страница 13: ...sponse time Contaminated reference junctions Rinse reference junction with deionized water thoroughly shake the electrode downward to remove any air bubbles and soak in 3 0 M KCl storage solution for...

Страница 14: ...ts Check standard value is outside of limits set in the current method Verify that the standard is within the limits of the current method Create a new method that expands the acceptable limits Measur...

Страница 15: ...storage cap lid 1 5829800 Field kit Includes glove kit and 5 120 mL sample cups 1 5825800 Glove kit only for HQd meters 1 5828700 IntelliCAL probe stand for standard probes 1 8506600 Meter stand 1 850...

Страница 16: ...insert for meter and two probe storage cavities space for storage of HQd meter with protective glove 1 8505600 Rugged shroud kit 1 5825900 Consumables Electrode cleaning solution 500 mL 2965249 Electr...

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