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Gilson dispensman, Руководство пользователя

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Gilson dispensman Скачать руководство пользователя страница 16

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SPARE PARTS

 

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DISPENSMAN

®

DESCRIPTION

PART NUMBER

 

Calibration tool

F107122

Protective sleeve for discharge tube, 2.5 mL, 5 mL, and 10 mL

F107145

9

Discharge tube, 2.5 mL

F107124

9

Discharge tube, 5 and 10 mL

F107125

22

Reflux tube, 40mm, l.Ø:3mm, A.Ø: 4 mm

F107127

21

Telescopic tube, 125 – 240 mm

F107133

21

Telescopic tube, 250 – 480 mm

F107135

21

Telescopic tube, 70 – 140 mm

F107136

21

Telescopic tube, 195 – 350 mm

F107137

11

Thread adapters made of PP invert GL A45/A32

F107139

11

Thread adapters made of PP GL A32/A45

F107140

11

Thread adapters made of PP GL A32/S40

F107141

11

Thread adapters made of PP GL A32/A38

F107142

11

Thread adapters made of PP GL A32/A28

F107143

11

Thread adapters made of PP GL A32/A25

F107144

8

Chapter 10

SPARE PARTS

Spare Parts for Small Volumes (2.5, 5, and 10 mL)

Spare Parts for Large Volumes (25 and 50 mL)

DESCRIPTION

PART NUMBER

Calibration tool

F107123

Protective sleeve for discharge tube, 25 and 50 mL

F107146

9

Discharge tube, 25 and 50 mL

F107126

22

Reflux tube, 40mm, l.Ø:6mm, A.Ø: 7 mm

F107128

21

Telescopic tube, 170 – 330 mm

F107134

21

Telescopic tube, 250 – 480 mm

F107138

11

Thread adapters made of PP invert GL A45/A32

F107139

11

Thread adapters made of PP GL A32/A45

F107140

11

Thread adapters made of PP GL A32/S40

F107141

11

Thread adapters made of PP GL A32/A38

F107142

11

Thread adapters made of PP GL A32/A28

F107143

11

Thread adapters made of PP GL A32/A25

F107144

Acetaldehyde

Butyric acid

Glycol

Acetic acid 100%

Calcium carbonate

Glycolic acid 50%

Acetic acid 96%

Calcium chloride

Hexanoic acid 

Acetone

Calcium hydroxide

Hexanol

Acetonitrile

Calcium hypochlorite

Hydriodic acid 57%

Acetylacetone

Chloro naphthalene

Hydrochloric acid 20%

Acrylic acid

Chloroacetaldehyde 45%

Isoamyl alcohol

Acrylonitrile

Chloroacetic acid

Isobutanol

Adipic acid

Chloroacetone

Isopropanol

Allyl alcohol

Chlorobenzene

Isopropyl ether

Aluminium chloride

Chlorobutane

Lactid acid

Amino acids

Chromic acid 50%

Methoxybenzene

Ammonia 20%

Chromosulfuric acid

Methyl alcohol

Ammonium chloride

Copper sulfate

Methyl benzoate

Ammonium fluoride

Cumene

Methyl butyl ether

Ammonium sulfate

Cyclohexanone

Methyl ethyl ketone

n-Amyl acetate

Decane

Methyl formate

Amyl alcohol

1-Decanol

Methyl propyl ketone

Aniline

Dibenzyl ether

Mineral oil

Barium chloride

Dichlorobenzene

Monochloroacetic acid

Benzaldehyde

Diethanolamine

Nitric acid 30%

Benzol

Diethylamine

Nitrobenzene

Benzoyl chloride

1.2 Diethylbenzene

Oleic acid

Benzyl alcohol

Diethylene glycol

Oxalic acid

Benzylamine

Dimethyl sulfoxide

Perchloric acid

Benzylchloride

Dimethylaniline

Phenol

Boric acid 10%

Dimethylformamide

Phenylethanol

Bromobenzene

Diphenyl ether

Phenilhydrazine

Bromonaphthalene

Ethanolamine

Phosphoric acid 85%

Butanediol

Ethyl acetate

Phosphoric acid 85% + Sulfuric 

acid 98%, 1:1

1-Butanol

Ethyl alcohol

Piperidine

n-Butyl acetate

Formaldehyde 40%

Potassium chloride

Butyl methyl ether

Formamide

Potassium dichromate

Butylamine

Glycerol

Potassium hydroxide

8

LT801577_D _UG DISPENSMAN.indd   16

09/11/2017   15:01:15

Содержание dispensman

Страница 1: ...User s Guide EN LT801577_D _UG DISPENSMAN indd 1 09 11 2017 15 01 11 ...

Страница 2: ...LATION 8 Telescopic Tube 8 Bottle Adapter 8 OPERATION 9 Volume adjustment 9 Air Purging 9 Dispensing 10 Anti Drop system 10 MAINTENANCE 11 Disassembly 11 Assembly 11 CLEANING AND STERILIZATION 12 Cleaning 12 Sterilization 12 CALIBRATON 13 TROUBLESHOOTING 14 SPECIFICATIONS 15 SPARE PARTS 16 Spare Parts for Small Volumes 2 5 5 and 10 mL 16 Spare Parts for Large Volumes 25 and 50 mL 16 APPENDIX 17 WA...

Страница 3: ...lve block can rotate 360 therefore the label of the bottle is always visible for your added safety The dispenser has our unique 100 drip free system for your safety at work just turn the nozzle switch to Empty 180 to drain it and prevent uncontrolled flow of liquid The dispenser is fully autoclavable at 121 C and can be completely disassembled for cleaning Each instrument is individually tested an...

Страница 4: ...tube Reflux tube 19 5 6 15 20 7 22 21 12 5 6 7 20 21 22 12 7 16 14 13 17 18 19 18 17 16 15 14 13 12 Figure 1 Nozzle switch and its axle located inside the valve block Figure 2 Valve block without nozzle Figure 3 Valve block top view Figure 4 Aspiration system located under outer housing Figure 5 Valve block bottom view Com Parts After un and not 1 Gil 1 tel 1 pro 1 ca 4 ad 1 ce 1 us LT801577_D _UG...

Страница 5: ...opylene Nozzle switch PP polypropylene Clear components Discharge tube FEP fluorinated ethylene propylene Inside valve block ETFE ethylene tetrafluoroethylene Valve star ETFE ethylene tetrafluoroethylene Cylinder Glass Protective transparent plastic for cylinder PTFE polytetrafluoroethylene Telescopic tube FEP fluorinated ethylene propylene Reflux tube FEP fluorinated ethylene propylene Dark compo...

Страница 6: ...very week and if you want to use DISPENSMAN for another chemical solution or if you do not use it for a longer time The temperature of the dispenser and reagent should not exceed 40 C 104 F The user is responsible for checking that the instrument is suitable for his application The proper and secure function is only guaranteed by using the supplied discharge tube 9 Do not use any other discharge t...

Страница 7: ... the screw base Do not pump before the instrument has been assembled completely and a collecting vessel has been placed underneath Operating Limitations Do not use for PTFE swelling solvents Hydrofluoric acid Chemical solutions that react with platinum iridium alloys Liquids used with DISPENSMAN must not exceed the following limits Liquid Contact Materials The components having direct contact with...

Страница 8: ...be it should reach the bottom of the bottle The reflux tube 22 is already attached to the bigger hole Bottle Adaptor Choose the right adaptor according to your bottle Screw the chosen adaptor on to the extremity of the bottle and screw DISPENSMAN into the adaptor Check the stability of the instrument on the bottle before operating 21 22 Figure 6 Valve block bottom view LT801577_D _UG DISPENSMAN in...

Страница 9: ... to Recycle 90 Set a small volume and dispense until the cylinder 19 is free from air Air purging is performed in a closed circuit for zero loss of reagent Turn the discharge tube back to Dispense 0 Adjust to the desired volume Dispense liquid precisely and carefully until the end of discharge tube 9 is fully filled Without any air in the entire instrument this step will guarantee that the dispens...

Страница 10: ...outer housing to the lowest point The movements should be smooth and constant to achieve an accurate dispense volume Noise while aspirating or dispensing is acceptable as it is because of the high quality suction valve with valve ball Anti Drop System Turn the nozzle switch 7 to Empty 180 The liquid from the discharge tube will now rinse back into the bottle Any further dispensing of liquid is not...

Страница 11: ...he valve block 20 be aware that the valve star 13 and the valve ball 14 might fall out 10 Take the valve star 13 and the valve ball 14 out of the valve block 20 11 Pull the nozzle switch 7 out of the valve block 20 Assembly 1 Push the nozzle switch 7 into the valve block 20 2 Place the valve ball 14 and the valve star 13 into the suction valve Check that the edges of the valve star 13 point upward...

Страница 12: ... on page 11 and clean all components The dispenser should be cleaned daily if used with following chemicals Solutions that tend to crystallize e g salts Inorganic oxidizing solutions e g biuret reagent Sterilization After removal of the reflux tube 22 and the telescopic tube 21 the dispenser can be steam sterilized 121 C 1 bar 20 minutes according to EN ISO 17665 Place the instrument on a cloth an...

Страница 13: ...with the thicker side to the site of the safety bolt Figure 9 5 To recalibrate a volume set too low rotate the calibration tool clockwise To recalibrate a volume set too high rotate the calibration tool counter clockwise 6 Attach the safety bolt to the piston Figure 8 7 Check the volume If the measured volume exceeds the tolerance limits then calibrate the instrument again If the calibration was s...

Страница 14: ...et in cleaning fluid Check the discharge tube If it is not clean and operational disassemble it and then flush it with cleaning fluid No Liquid Aspirated Check the fit of the telescopic tube into the suction valve It should be firmly pressed into the smaller hole of the bottom part of the valve block please refer to figure 6 page 8 Check the volume setting Check the suction valve and then clean it...

Страница 15: ...iant with ISO 8655 Each dispenser is inspected and validated by qualified technicians Gilson declares that its manufactured dispensers comply with the requirements of the ISO 8655 standard by type testing The adjustment is carried out under strictly defined and monitored conditions MODEL PART NUMBER VOLUME RANGE SCALING mL MAXIMUM PERMISSIBLE ERRORS GILSON ISO 8655 5 SYSTEMATIC ERROR mL RANDOM ERR...

Страница 16: ...umes 2 5 5 and 10 mL Spare Parts for Large Volumes 25 and 50 mL DESCRIPTION PART NUMBER Calibration tool F107123 Protective sleeve for discharge tube 25 and 50 mL F107146 9 Discharge tube 25 and 50 mL F107126 22 Reflux tube 40mm l Ø 6mm A Ø 7 mm F107128 21 Telescopic tube 170 330 mm F107134 21 Telescopic tube 250 480 mm F107138 11 Thread adapters made of PP invert GL A45 A32 F107139 11 Thread adap...

Страница 17: ...umene Methyl butyl ether Ammonium sulfate Cyclohexanone Methyl ethyl ketone n Amyl acetate Decane Methyl formate Amyl alcohol 1 Decanol Methyl propyl ketone Aniline Dibenzyl ether Mineral oil Barium chloride Dichlorobenzene Monochloroacetic acid Benzaldehyde Diethanolamine Nitric acid 30 Benzol Diethylamine Nitrobenzene Benzoyl chloride 1 2 Diethylbenzene Oleic acid Benzyl alcohol Diethylene glyco...

Страница 18: ... it is designed Gilson is not responsible for consequential damages resulting from the misuse of this instrument Potassium permanganate Sodium acetate Tetramethylammoniumhydroxide Propionic acid Sodium chloride Triethanolamine Propylene glycol Sodium dichromate Triethylene glycol Pyridine Sodium fluoride Urea Pyruvic acid Sodium hydroxide 30 Zinc chloride 10 Salicylaldehyde Sodium hypochlorite Zin...

Страница 19: ...Notes 19 DISPENSMAN USER S GUIDE NOTES ide LT801577_D _UG DISPENSMAN indd 19 09 11 2017 15 01 15 ...

Страница 20: ...ghts reserved Specifications subject to change without notification errors excepted Reproduction adaptation or translation without prior written permission is prohibited except as allowed under copyright laws LT801577_D _UG DISPENSMAN indd 20 09 11 2017 15 01 15 ...

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