Gilson dispensman Скачать руководство пользователя страница 15

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DISPENSMAN

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USER’S GUIDE

Chapter 8

TROUBLESHOOTING

Valve Sticks

With the dispensing unit screwed on, ensure that the valves are surrounded by 

liquid and that the valve system is easy to move by rinsing it with distilled water 

and/or laboratory cleaning agent. As a last step, rinse with alcohol.

Piston Difficult to Move

Check whether crystals have formed, and if so, carry out intensive cleaning of the 

piston and the cylinder (refer to Chapter 5 

MAINTENANCE

, page 11).

No Liquid Dispensed

 

•  Check that the nozzle switch is set to “Dispense” (0°).

•  Check the suction valve and then clean it, if necessary. 

•  Check the nozzle switch. If it is not clean and operational, clean unit by 

immersing nozzle set in cleaning fluid.

•  Check the discharge tube. If it is not clean and operational, disassemble it, 

and then flush it with cleaning fluid.

No Liquid Aspirated

•  Check the fit of the telescopic tube into the suction valve. It should be firmly 

pressed into the smaller hole of the bottom part of the valve block (please 

refer to figure 6, page 8).

•  Check the volume setting.

•  Check the suction valve and then clean it, if necessary. 

Air Bubbles in Aspirated Liquid

•  Check whether all air has been removed from the instrument, (See Chapter 4 

OPERATION

, page 9). 

•  Check that the reservoir is not empty. 

•  Check the telescopic tube, if necessary slide it to shorten it or replace it in its 

socket.

•  Ensure slow, steady aspiration of reagent.

•  Check the suction valve and then clean it, if necessary. 

Incorrect Volume Dispensed

Calibrate the instrument (See Chapter 7 

CALIBRATION

, page 13).

If any problem persists, please return DISPENSMAN back to your local Gilson 

service center.

Return for Repair

Please clean the instrument carefully, as described in Chapter 6 

CLEANING & STERILIZATION

, page 12. Never send in instruments 

filled with reagents. Returned instruments can only be 

checked and repaired if they have been carefully cleaned and 

decontaminated by the customer. 

Forced opening of the instrument invalidates any warranty claim. Enclose with 

the returned instrument a description of the trouble that has occurred and 

specify which reagents were used. 

Chapter 9

SPECIFICATIONS

DISPENSMAN is a high quality dispenser that offers excellent accuracy and 

precision; it is fully compliant with ISO 8655. 

Each dispenser is inspected and validated by qualified technicians. Gilson 

declares that its manufactured dispensers comply with the requirements of the 

ISO 8655 standard, by type testing. The adjustment is carried out under strictly 

defined and monitored conditions.

MODEL

PART 

NUMBER

VOLUME RANGE

SCALING 

(mL)

MAXIMUM PERMISSIBLE ERRORS

GILSON

ISO 8655-5

SYSTEMATIC 

ERROR (mL)

RANDOM 

ERROR (mL)

SYSTEMATIC 

ERROR (mL)

RANDOM 

ERROR (mL)

DISPENSMAN 2.5 mL

F110101

0.25 – 2.5 mL

0.05

±0.012

 0.002

±0.030

 0.010

DISPENSMAN 5.0 mL

F110102

0.5 – 5 mL

0.10

±0.030

 0.005

±0.030

 0.010

DISPENSMAN 10 mL

F110103

1 – 10 mL

0.20

±0.060

 0.010

±0.060

 0.020

DISPENSMAN 25 mL

F110104

2.5 – 25 mL

0.50

±0.150

 0.025

±0.150

 0.050

DISPENSMAN 50 mL

F110105

5 – 50 mL

1.00

±0.300

 0.050

±0.300

 0.100

Noise During Aspiration and Dispensing

Noise while aspirating or dispensing is acceptable as it is because of the high quality 

suction valve with valve ball.

SPECIFICA

TIONS

NOTICE

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09/11/2017   15:01:15

Содержание dispensman

Страница 1: ...User s Guide EN LT801577_D _UG DISPENSMAN indd 1 09 11 2017 15 01 11 ...

Страница 2: ...LATION 8 Telescopic Tube 8 Bottle Adapter 8 OPERATION 9 Volume adjustment 9 Air Purging 9 Dispensing 10 Anti Drop system 10 MAINTENANCE 11 Disassembly 11 Assembly 11 CLEANING AND STERILIZATION 12 Cleaning 12 Sterilization 12 CALIBRATON 13 TROUBLESHOOTING 14 SPECIFICATIONS 15 SPARE PARTS 16 Spare Parts for Small Volumes 2 5 5 and 10 mL 16 Spare Parts for Large Volumes 25 and 50 mL 16 APPENDIX 17 WA...

Страница 3: ...lve block can rotate 360 therefore the label of the bottle is always visible for your added safety The dispenser has our unique 100 drip free system for your safety at work just turn the nozzle switch to Empty 180 to drain it and prevent uncontrolled flow of liquid The dispenser is fully autoclavable at 121 C and can be completely disassembled for cleaning Each instrument is individually tested an...

Страница 4: ...tube Reflux tube 19 5 6 15 20 7 22 21 12 5 6 7 20 21 22 12 7 16 14 13 17 18 19 18 17 16 15 14 13 12 Figure 1 Nozzle switch and its axle located inside the valve block Figure 2 Valve block without nozzle Figure 3 Valve block top view Figure 4 Aspiration system located under outer housing Figure 5 Valve block bottom view Com Parts After un and not 1 Gil 1 tel 1 pro 1 ca 4 ad 1 ce 1 us LT801577_D _UG...

Страница 5: ...opylene Nozzle switch PP polypropylene Clear components Discharge tube FEP fluorinated ethylene propylene Inside valve block ETFE ethylene tetrafluoroethylene Valve star ETFE ethylene tetrafluoroethylene Cylinder Glass Protective transparent plastic for cylinder PTFE polytetrafluoroethylene Telescopic tube FEP fluorinated ethylene propylene Reflux tube FEP fluorinated ethylene propylene Dark compo...

Страница 6: ...very week and if you want to use DISPENSMAN for another chemical solution or if you do not use it for a longer time The temperature of the dispenser and reagent should not exceed 40 C 104 F The user is responsible for checking that the instrument is suitable for his application The proper and secure function is only guaranteed by using the supplied discharge tube 9 Do not use any other discharge t...

Страница 7: ... the screw base Do not pump before the instrument has been assembled completely and a collecting vessel has been placed underneath Operating Limitations Do not use for PTFE swelling solvents Hydrofluoric acid Chemical solutions that react with platinum iridium alloys Liquids used with DISPENSMAN must not exceed the following limits Liquid Contact Materials The components having direct contact with...

Страница 8: ...be it should reach the bottom of the bottle The reflux tube 22 is already attached to the bigger hole Bottle Adaptor Choose the right adaptor according to your bottle Screw the chosen adaptor on to the extremity of the bottle and screw DISPENSMAN into the adaptor Check the stability of the instrument on the bottle before operating 21 22 Figure 6 Valve block bottom view LT801577_D _UG DISPENSMAN in...

Страница 9: ... to Recycle 90 Set a small volume and dispense until the cylinder 19 is free from air Air purging is performed in a closed circuit for zero loss of reagent Turn the discharge tube back to Dispense 0 Adjust to the desired volume Dispense liquid precisely and carefully until the end of discharge tube 9 is fully filled Without any air in the entire instrument this step will guarantee that the dispens...

Страница 10: ...outer housing to the lowest point The movements should be smooth and constant to achieve an accurate dispense volume Noise while aspirating or dispensing is acceptable as it is because of the high quality suction valve with valve ball Anti Drop System Turn the nozzle switch 7 to Empty 180 The liquid from the discharge tube will now rinse back into the bottle Any further dispensing of liquid is not...

Страница 11: ...he valve block 20 be aware that the valve star 13 and the valve ball 14 might fall out 10 Take the valve star 13 and the valve ball 14 out of the valve block 20 11 Pull the nozzle switch 7 out of the valve block 20 Assembly 1 Push the nozzle switch 7 into the valve block 20 2 Place the valve ball 14 and the valve star 13 into the suction valve Check that the edges of the valve star 13 point upward...

Страница 12: ... on page 11 and clean all components The dispenser should be cleaned daily if used with following chemicals Solutions that tend to crystallize e g salts Inorganic oxidizing solutions e g biuret reagent Sterilization After removal of the reflux tube 22 and the telescopic tube 21 the dispenser can be steam sterilized 121 C 1 bar 20 minutes according to EN ISO 17665 Place the instrument on a cloth an...

Страница 13: ...with the thicker side to the site of the safety bolt Figure 9 5 To recalibrate a volume set too low rotate the calibration tool clockwise To recalibrate a volume set too high rotate the calibration tool counter clockwise 6 Attach the safety bolt to the piston Figure 8 7 Check the volume If the measured volume exceeds the tolerance limits then calibrate the instrument again If the calibration was s...

Страница 14: ...et in cleaning fluid Check the discharge tube If it is not clean and operational disassemble it and then flush it with cleaning fluid No Liquid Aspirated Check the fit of the telescopic tube into the suction valve It should be firmly pressed into the smaller hole of the bottom part of the valve block please refer to figure 6 page 8 Check the volume setting Check the suction valve and then clean it...

Страница 15: ...iant with ISO 8655 Each dispenser is inspected and validated by qualified technicians Gilson declares that its manufactured dispensers comply with the requirements of the ISO 8655 standard by type testing The adjustment is carried out under strictly defined and monitored conditions MODEL PART NUMBER VOLUME RANGE SCALING mL MAXIMUM PERMISSIBLE ERRORS GILSON ISO 8655 5 SYSTEMATIC ERROR mL RANDOM ERR...

Страница 16: ...umes 2 5 5 and 10 mL Spare Parts for Large Volumes 25 and 50 mL DESCRIPTION PART NUMBER Calibration tool F107123 Protective sleeve for discharge tube 25 and 50 mL F107146 9 Discharge tube 25 and 50 mL F107126 22 Reflux tube 40mm l Ø 6mm A Ø 7 mm F107128 21 Telescopic tube 170 330 mm F107134 21 Telescopic tube 250 480 mm F107138 11 Thread adapters made of PP invert GL A45 A32 F107139 11 Thread adap...

Страница 17: ...umene Methyl butyl ether Ammonium sulfate Cyclohexanone Methyl ethyl ketone n Amyl acetate Decane Methyl formate Amyl alcohol 1 Decanol Methyl propyl ketone Aniline Dibenzyl ether Mineral oil Barium chloride Dichlorobenzene Monochloroacetic acid Benzaldehyde Diethanolamine Nitric acid 30 Benzol Diethylamine Nitrobenzene Benzoyl chloride 1 2 Diethylbenzene Oleic acid Benzyl alcohol Diethylene glyco...

Страница 18: ... it is designed Gilson is not responsible for consequential damages resulting from the misuse of this instrument Potassium permanganate Sodium acetate Tetramethylammoniumhydroxide Propionic acid Sodium chloride Triethanolamine Propylene glycol Sodium dichromate Triethylene glycol Pyridine Sodium fluoride Urea Pyruvic acid Sodium hydroxide 30 Zinc chloride 10 Salicylaldehyde Sodium hypochlorite Zin...

Страница 19: ...Notes 19 DISPENSMAN USER S GUIDE NOTES ide LT801577_D _UG DISPENSMAN indd 19 09 11 2017 15 01 15 ...

Страница 20: ...ghts reserved Specifications subject to change without notification errors excepted Reproduction adaptation or translation without prior written permission is prohibited except as allowed under copyright laws LT801577_D _UG DISPENSMAN indd 20 09 11 2017 15 01 15 ...

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