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disassembled or opened, cleaned with a small brush, and at the same time, use a vacuum cleaner
to absorb the dust in each part. For the negative high-voltage power cord of the photomultiplier
tube, the high-voltage cords and connectors of the computer monitor, use gauze moistened with
a little absolute alcohol to carefully wipe off the carbon and dust.
For the dust removal of the instrument, the help of electronic instrument repair professionals. If
the user or manager of the instrument does not understand the structure of the instrument, do
not move it easily to avoid accidents. The dust removal should be carried out before stopping and
turning off the power supply.

2.2 Power Supply and Auxiliary Material Configuration
2.2.1 Stable Power Supply System

In order to ensure the safe operation of the ICP-AES, the power supply line must have a large
enough capacity, otherwise the voltage drop of the line during the operation of the instrument is
too large, which will affect the life of the instrument. As a precision measuring instrument, it also
needs a relatively stable power supply, and the change in power supply voltage generally does
not exceed ±1%, If it exceeds this range, you need to use a precision purified AC power supply, as
the general voltage stabilizer generates clipping when the voltage is high, it causes electric pulses,
which affects the work of electronic computers, microprocessors and phase sensitive amplifiers,
and causes malfunctions. The continuous sine wave power supply can ensure the normal
operation of these electronic circuits. The power supply circuit of the instrument should be
obtained separately from the distribution board of the power supply transformer. Try not to
share a power supply line with large motors, large ventilators, air conditioners, muffle furnaces
and other large electrical equipment. In order to avoid large fluctuations in the voltage of the
power supply line when these electrical equipment are started, resulting in unstable operation of
the instrument. Generally, the ground wire resistance of the spectrometer should be less than 4Ω,
and the computer ground wire resistance should be less than 0.25Ω(ASTM) to prevent mutual
interference.
In the operation of the instrument, the operator should always pay attention to the change of the
power supply voltage, and you cannot work under over-voltage or under-voltage for a long time.
When the instrument works under over-voltage, the life of the tube will be greatly
shortened(below 20% of the normal life). If working under the condition of insufficient voltage,
the temperature of the electron tube filament is too low, it will also easily cause the aging of the
electron emission material, and also shorten the life of the electron tube. Large fluctuations of
the power supply voltage during the operation of the instrument will also cause the instability of
the output power of the high-frequency generator, which will have a great impact on the
measurement results. Therefore, the quality of the power supply must be guaranteed.

2.2.2 Power Requirements

DW-TY-9900 ICP-AES needs AC single-phase 220V/50Hz power supply. If the voltage fluctuation is
greater than ±1V, it needs to be equipped with 10KVA precision purification AC regulated power
supply(output accuracy

±1%, response time ˂ 20-80ms). The power requirements of each part

are as follows:

DW-TY-9900 ICP-AES host

: single-phase AC(220±1)V/50Hz, 2kVA(The wire cross section is not

less than 4mm

2

).

Microcomputer system

:single-phase AC(220±1)V/50Hz, 500VA

Cooling water tank

:single-phase AC(220±1)V/50Hz, 1.5kVA

Содержание DW-TY-9900

Страница 1: ...manual DRAWELL INTERNATIONAL TECHNOLOGY LIMITED Chongqing Center Suite 2605 Building No 11 Shiyou Road No 1 Yuzhong District Chongqing China Tel 0086 023 63268643 Shanghai Office Suite 1101 Lane561 X...

Страница 2: ...iary Material Configuration 4 2 2 1 Stable Power Supply System 4 2 2 2 Power Requirements 4 2 2 3 Grounding Requirements 5 2 2 4 Gas Requirements 5 2 2 5 Cooling Water Requirements 5 2 2 6 Exhaust Req...

Страница 3: ...ucts include chemical reagents inorganic materials cosmetics oil gasoline diesel lubricating oil C5 and other synthetic gasoline raw materials oleic acid petroleum catalysts urea solutions 8 Food and...

Страница 4: ...nts to ensure the accuracy and sensitivity of the instrument 3 Small matrix effect 99 of the samples do not need to separate the matrix 4 Wide measurement range analysis from ultra micro to constant 5...

Страница 5: ...a generally the room temperature is required to be maintained at a fixed temperature between 25 3 and the temperature change should be less than 1 h If the ambient humidity is too high optical compone...

Страница 6: ...pply transformer Try not to share a power supply line with large motors large ventilators air conditioners muffle furnaces and other large electrical equipment In order to avoid large fluctuations in...

Страница 7: ...ng the smart cooling water tank add 35 liters of distilled or purified water to the PVC water tank of the cooling water tank 2 2 6 Exhaust Requirements The gas exhausted by the plasma chamber is mainl...

Страница 8: ...9900 ICP AES from left to right are main ICP power socket ground wire cooling water inlet and outlet two parts plasma gas and carrier gas inlets Fig 1 Fig 3 1 Schematic diagram of the installation po...

Страница 9: ...w direction it is open Plasma gas and carrier gas inlet in the picture they are respectively connected to the argon cylinder with a 6 PU tube through an oxygen pressure reducing regulator Fig 3 2 Circ...

Страница 10: ...her is the serial port for communication with the computer The power port is directly connected to the 220V power socket and the serial port needs to be connected to the RS232 interface on the back of...

Страница 11: ...Trainees should carefully read the operating instructions understand the functions of the various knobs of the instrument and be familiar with the operating methods and steps of the instrument and the...

Страница 12: ...ealing ring 2 Sets 1 big 2 small 9 Waste bottle 2 Pcs 10 Torch clamp 2 Pcs 11 Temperature controlled cooling circulating water tank 1 Set 12 Exhaust system 1 Set Axial Fan 13 Host power cord waterproo...

Страница 13: ...joint 4 Pcs 27 Direct connection 2 Pcs 6 28 Tee 2 Pcs 6 29 Argon cylinder pressure relief valve outlet connector 2 Pcs Stainless steel quick coupling with trachea 30 Copper plate copper rod and copper...

Страница 14: ...y scan change level of light to find zero light select the building method After the analysis of the capillary into the next measurement method of peak search of the standard peak active the looking f...

Страница 15: ...cts of the title bar shows the current method name the figure shows the ICP Analysis HG The second line is the menu bar A total of six drop down menu options daily use of measurement including three d...

Страница 16: ...15 In the new method enter the method name The following window appears determined...

Страница 17: ...16 OK displays the following window...

Страница 18: ...ach element needs its own standard input is enter the value you are prepared and STDHIGH STDLOW value your configuration or converted units completed in the daily analysis we need only follow the step...

Страница 19: ...18 attenuation measurement standards measure the sample Selection Method...

Страница 20: ...19 Double click or select the following points to determine Measurement automatic searching for peak peak with the preparation of standard solution actively look for a good looking peak...

Страница 21: ...20 Automatic peak search...

Страница 22: ...tenuation measurement in the analysis using standard solutions prepared from standard to high attenuation as shown below The first method requires the establishment of the future does not need automat...

Страница 23: ...22 Measurement standards in the analysis and measurement of the sample analysis sample to select multiple windows Testing standards...

Страница 24: ...23...

Страница 25: ...24 After you finish testing the standard point of exit to save Test sample...

Страница 26: ...25 Historical database free to choose to print to analyze data hold down the Ctrl key point to print the number...

Страница 27: ...26 Test results and historical data...

Страница 28: ...onals can make the sample case tracing the edit icon in the View view of spectrum The line spectrum is easily to identify whether the interference see the letter back ratio can be set to automatically...

Страница 29: ...nd that there is a lot of dirt at the nozzle or the center channel is blocked It needs to be used 1 1 acid soaking for 2 hours and then rinsed with pure water and dried 8 Whether the atomizer enters t...

Страница 30: ...g if the power is frequently on and the main control board is likely to burn if it rains and thunders 5 2 Precautions for Turn On Off Before turn on the measurement you need to make various preparatio...

Страница 31: ...on the working coil such as the torch the high voltage power supply must be turned off or the ICP power supply 2 When performing maintenance on the power box the operator must shut it down for 30 minu...

Страница 32: ...tactor is damaged or the auxiliary contact wiring is disconnected falling off etc Replace the contactor or restore the normal connection after finding the wiring fault High voltage cannot be turned on...

Страница 33: ...ite re ignite after preloading gas Air leakage at the junction of pipe and atomizer Tighten the connector if the atomizer is damaged contact the manufacturer for replacement Insufficient tube power Re...

Страница 34: ...pipe connecting the ICP and the water tank Open the ICP back shell Open the high frequency box and gradually remove the parts connected to the tube After changing the tube install it again Reconnect...

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