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Contents

Safety

Safety Notations

Introduction

About the Instrument

Important Safeguards

Microwave Safeguards

Instrument Safeguards

Compounds Unsuitable for Closed Vessel Microwave

Digestion 3

Instrument Overview

Front and Side View

Back and Side View

Cavity 7

Software Overview

Software Icons

Home Screen

Methods Screen (One Touch and Classic)

System Settings

System Installation

Unboxing 13

System Setup

Perform a Digestion

iPrep Vessel Series

EasyPrep Vessel Series

MARSXpress Vessel Series

MARSXpress Plus Vessel Series

Methods

One Touch Method Creation

Classic Method Creation

Edit Method

Delete Method

Export Method

Import Method

Users

Create User

Edit/Delete User

Auto Login

Password Configuration

Data Management

View, Print, and Export Data

Activity Log

MARS 6 Screenshot Capture

Calibrations

Temperature Verification (iWave Sensors)

Temperature Calibration (iWave Sensors)

Turntable Calibration

Power Test

Power Test

Printer (Optional)

Internal Printer

Software Update

How to Update Software

Routine Maintenance

After Every Use

Daily 36

Weekly 36

Annually 37

As Needed

Troubleshooting

Problems and Possible Solutions

System Specifications

Location Requirements

Electrical Requirements

Environmental Requirements

Содержание MARS 6 iWave

Страница 1: ...MARS 6 iWave Microwave Digestion System Manual...

Страница 2: ...THIS PAGE INTENTIONALLY LEFT BLANK...

Страница 3: ...ods One Touch Method Creation 20 Classic Method Creation 20 Edit Method 20 Delete Method 20 Export Method 21 Import Method 22 Users Create User 23 Edit Delete User 24 Auto Login 24 Password Configurat...

Страница 4: ...Warranty Limited Warranty Information 42 Technical Assistance Applications Support 44 Technical Support 44 Contact Information CEM Corporation Headquarters 45 CEM International Subsidiaries 45 CEM Au...

Страница 5: ...d below NOTE A NOTE is intended to provide emphasis on procedures that may be misinterpreted or overlooked or to clarify confusing situations CAUTION A CAUTION is intended to provide essential informa...

Страница 6: ...nformation including but not limited to training notes and videos application notes software updates and parts can be viewed on CEM s website at www cem com The MARS 6 iWave is designed to be operated...

Страница 7: ...pletion of the cool down time Vent vessels and reseal Restart method from the beginning Allow vessels to cool to completion of the cool down time before opening the microwave door Instrument Safeguard...

Страница 8: ...Hydrazine Ammonium Perchlorate etc Pyrophoric chemicals Hypergolic mixtures Nitric Acid and Phenol Nitric Acid and Triethylamine Nitric Acid and Acetone etc Animal Fats Esters of glycerol capable of...

Страница 9: ...ers 2 Door Handle Permits ease of opening instrument door 3 Internal Printer optional Permits printing of method parameters graphs and or method data 4 Cooling Fan Draws room air past the electronics...

Страница 10: ...s fumes from the microwave cavity 3 Cavity Exhaust Blower Directs air from the microwave cavity to the exhaust outlet at the rate of 3 6 m3 minute 125 ft3 minute 4 External Sensor Port Permits interfa...

Страница 11: ...ntable drive shaft to pass through the cavity floor and engage the Turntable 4 Floor Mat Protects the Teflon Coating on the Floor of the Mars 6 Cavity 5 Door Inerlock 3 door safety interlocks and an i...

Страница 12: ...tware Icons Icon Description Icon Description Icon Description Add Stage Home Run Back Information Save Blower Import Screen Context Menu Delete iWave System Settings Done New Temperature Edit Power T...

Страница 13: ...be copied and the copy can be edited Classic Methods are created by the user and can be edited at any time These methods are typically for users with unique or specialized products that do not have a...

Страница 14: ...ation etc and users Video Visual display to ensure proper system handling and usage Logout Protects the current user s access or prevent unauthorized actions on the current login session Tools System...

Страница 15: ...t Date Time Location for setting the correct date and time Users Manage users passwords and log in preferences Run Adjustments to settings specific to each sample run including data output vessel cool...

Страница 16: ...12 Software Overview Logout Displays logout screen...

Страница 17: ...ed during shipping If the instrument or accessories have damage contact the freight carrier to report the damage and file a damage report Contact your CEM Representative for assistance WARNING If any...

Страница 18: ...at and remove the foam from the top of the system 7 Lift the system from the sides onto bench top near exhaust service two people required Do not place the system in a fume hood 8 Remove the plastic a...

Страница 19: ...acking material for use if returning the instrument to the manufacturer for service System Setup 1 Connect the exhaust hose to back of the system 2 Connect the opposite end of the exhaust hose to a fu...

Страница 20: ...de of the instrument and position it in the ON position 6 When the system is first powered on during the install a Line Voltage message will appear 7 Determine the line voltage from outlet 60 Hz 208 V...

Страница 21: ...ols 9 3 Select the System tab The iWave Temperature s will appear under Status NOTE The Side iWave Temperature C will only appear for the iPrep 16 vessel set 9 4 Ensure sensors are clean and free of d...

Страница 22: ...table drive lug and press Start 10 6 Once the alignment process is complete there will be three 3 possible outcomes Turntable is Aligned proceed with next step Turntable is not aligned It is recommend...

Страница 23: ...ly understand all documentation before operating the instrument iPrep Vessel Series iPrep Vessel Series Manual P N 600856 EasyPrep Vessel Series EasyPrep Vessel Series Manual P N 600962 MARSXpress Ves...

Страница 24: ...ic is the recommend sample type for most samples Contact CEM before selecting any other sample types 6 Select Hold Time and enter in the appropriate hold time 7 If applicable select Sample Prep Notes...

Страница 25: ...instrument 2 Select and hold long touch the method to be exported 3 Select the Screen Context Menu in the upper right corner of the screen NOTE To select multiple methods to export select Multi Select...

Страница 26: ...trument 2 From the Home Screen select Classic or One Touch 3 Select the Screen Context Menu located in the upper right corner of the screen 4 Select Import 5 Select the method to import 5 1 If the met...

Страница 27: ...bottom right corner of the screen 2 Select Settings 3 Select Users 4 Scroll down until Users section appears 5 Select Add User 6 Enter the User Name 7 Assign the User Group Administrators Ability to...

Страница 28: ...n appears 5 Select the Edit icon or Delete icon If Edit is selected make the appropriate changes and select the Save icon If Delete is selected confirm that the user wishes to delete the selected user...

Страница 29: ...he System Settings icon in the bottom right corner of the screen 2 Select Settings 3 Select Users 4 Scroll down to Password Settings and toggle to ON or OFF ON The administrator determines password cr...

Страница 30: ...can be exported and or printed 5 1 To export run data Install a USB in the USB port on the right side of the MARS 6 instrument Select the Export icon to export data 5 2 If the instrument is equipped w...

Страница 31: ...he top right corner 5 The results can be printed or exported by selecting the Print or Export icon s NOTE Activity log has a lot of data and if it is not filtered to a specific user and date range the...

Страница 32: ...on the keyboard to save the screenshot to the USB An on screen notification will appear software version 1 40 4 Press OK to clear the notification 5 Remove USB and plug into a computer 6 The screensho...

Страница 33: ...t the calibrator to warm until the Ready light is illuminated WARNING To prevent the possibility of burns DO NOT touch the heating module or Teflon cover surrounding the heating module 2 Select the Sy...

Страница 34: ...emperature calibration Read and fully understand the AutoCal manual P N 600835 before operation 1 Plug the AutoCal into an electrical outlet close enough to the instrument for it to be placed on the i...

Страница 35: ...the sensor 10 Press Start 11 Wait for a stable reading Repeat the above steps to calibrate the remaining sensor s NOTE The Side iWave Temperature C will only appear for the iPrep 16 vessel set 12 Ver...

Страница 36: ...turntable drive lug and press Start 6 Once the alignment process is complete there will be three 3 possible outcomes Turntable is Aligned No alignment is required Turntable is not aligned It is recom...

Страница 37: ...r and place the thermometer in the beaker 13 2 Stir the water thoroughly for 15 seconds then measure and record the peak temperature reading This is the final temperature Tf 14 To determine the microw...

Страница 38: ...e Print icon is displayed on the screen during method performance or when viewing method information and previous method performance data Replace Printer Paper 1 Lift the printer cover 2 Position the...

Страница 39: ...the MARS 6 USB port 4 Select the System Settings icon in the bottom right corner of the screen 5 Select Tools 6 Select Update Manager 7 Select the available software version and highlight the latest s...

Страница 40: ...l of the acids Dispose of all waste in accordance with all applicable local state and federal health and safety recommendations After Every Use Wipe inside of MARS 6 cavity including temperature senso...

Страница 41: ...ce WARNING Acid can condense and collect inside the blower duct Annually Preventative Maintenance by CEM Certified Technician Contact the CEM Service Department for assistance As Needed If installed r...

Страница 42: ...n fuse Contact CEM Corporation No Microwave Power Instrument door ajar Close MARS 6 door before pressing start Incorrect percentage of power selected View Method section for programming methods Low li...

Страница 43: ...for ventilation Electrical Requirements This instrument conforms to Globally Harmonized EN61010 1 Standard for Safety Requirements for Electric Equipment for Measurement Control and Laboratory Use Pa...

Страница 44: ...This instrument complies with United States Code of Federal Regulations 21CFR Part 1030 10 C for microwave leakage A verification report is on file This instrument complies with FCC Requirements in th...

Страница 45: ...n if full programmed power is applied continuously over a specified period of time ReactiGuard Continuously monitors the cavity and disables the magnetron if disturbances occur inside the cavity TempG...

Страница 46: ...pair or Any other damage caused by purchaser or its agents Responsibilities of Purchaser To ensure warranty coverage the purchaser must Use the instrument according to directions Connect the instrumen...

Страница 47: ...nd the face hereof CEM Corporation shall not be liable for loss of use of instrument or other incidental or consequential costs expenses or damages incurred by the purchaser or any other user This war...

Страница 48: ...Support or email CEM MARS 6 iWave applications support at analytical support cem com Technical Support CEM is proud to provide technical support for the MARS 6 iWave from a team of specially trained...

Страница 49: ...gique de Saclay 4 rue Ren Razel 91892 ORSAY Cedex France Web Address http www cemfrance fr Email info fr cem com Germany CEM GmbH Phone 011 49 2842 9644 0 Fax 011 49 2842 9644 11 Address Carl Friedric...

Страница 50: ...one 353 0 1 885 1752 Address Sky Business Centre 9a Plato Business Park Damastown Dublin 15 Ireland Web Address http www cemmicrowave co uk Email info ireland cem com CEM Authorized Dealers For a comp...

Страница 51: ...THIS PAGE INTENTIONALLY LEFT BLANK...

Страница 52: ...which shall not be reproduced or transferred to other documents or disclosed to others without prior written permission of CEM Corporation CEM iPrep iWave and One Touch are registered trademarks of C...

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