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15

Evaporate

Note: 

Changes made to methods cannot be undone. Overwritten 

data will be lost.

Set Up a Method

Before setting up a method, read "Determine Optimal 
Evaporation Conditions" on page 6. A
lso make sure that 
desired evaporation settings are defined, see "Evaporation 
Settings" on page 9.

To set up a method, proceed as follows:

1.  Select 

Method mode

 from the Evaporation Modes view, see 

Figure 25.

2.  Press the 

Method 

button in the appearing Evaporate view, 

see Figure 26, to access the methods.

3.  The Methods view dialog opens, see Figure 27.

Note:

 There are 10 default methods per manifold 

configuration. To access them, make sure to configure the 
correct manifold settings for the method, see "Common 
Settings" on page 8
.

4.  Select the method of choice and press the 

Edit

 

method 

button, see Figure 27.

Note:

 All methods can be reset to their default values, see 

"System Information" on page 10.

5.  In the Evaporation Parameters view (see Figure 28), enter 

the desired evaporation parameters and press the 

Edit 

name 

button to enter the desired name, see "Evaporation 

Parameters" on page 15.

6.  When done, press 

Save

.

Note:

 Once a method has been saved, its previous settings 

cannot be recovered.

7.  In the Methods view, press 

OK 

to return to the Evaporate 

view, see Figure 27.

Figure 25.

 The Evaporation Modes view.

Figure 26.

 The Evaporate view where methods can be accessed. In 

this view, the Flow Step Method is selected, as displayed on the Method 

button.

Figure 27.

 The Methods view where the method to be run or modified 

can be accessed. 

Evaporation Parameters

The evaporation parameters are displayed in the Evaporation 
Parameters view, see Figure 28. Four time segments can be 
configured: 

Step 1 – Step 4

 .

To change a setting, proceed as follows:

1.  Press the button for the setting to be configured; 

Time

Gas flow

Gas temperature

Plate temperature

 and 

Plate 

height

, see Figure 28.

Note:

 If the plate height button is continuously pressed 

down, it will change color to red. In this mode, pressing 
the 

Up and Down

 arrows will elevate and lower the lift, see 

Figure 29.

2.  Press the 

Up and Down 

arrows to change the setting step 

by step. Alternatively, press the 

Open numpad 

button to 

open the numeric keypad and enter numbers, see Figure 
28.

Содержание TurboVap 96 Dual

Страница 1: ...Patent Pending Biotage 2021 Title Truncated if Neccessary Page 1 TurboVap 96 Dual User Manual...

Страница 2: ...8 Define System Settings 8 Common Settings 9 Evaporation Settings 10 Network and Firmware 10 System Information 10 Warnings in the Software 11 Prepare the System 11 Replace the Manifold 11 Set the Pr...

Страница 3: ...s manifolds with 24 48 or 96 nozzles to allow for processing of up to 96 samples in each cabinet The left and right cabinet can perform simultaneous evaporation runs with varying size well plates vary...

Страница 4: ...he door is closed the evaporation run will resume To determine the correct plate height for an evaporation run see Determine Optimal Evaporation Conditions on page 6 Evaporation To provide consistency...

Страница 5: ...the Manifold on page 11 according to the chosen well plate Available manifolds TurboVap manifold with 24 gas nozzles TurboVap manifold with 48 gas nozzles TurboVap manifold with 96 gas nozzles Differe...

Страница 6: ...radation of analytes may be observed Do not allow samples or solvents to boil The evaporation time of samples decreases with increasing sample cleanliness The presence of sample detritus or particulat...

Страница 7: ...plate Usually setting the temperature of the plate heater 0 20 C above the gas temperature allows for enhanced evaporation uniformity Use of the plate heater minimizes cross contamination of samples w...

Страница 8: ...ifying and calibrating the touch screen 1 Mode Mode selection Press to select mode 2 Common Settings Press to change common settings 3 Evaporation Settings Press to change evaporation settings 4 Netwo...

Страница 9: ...as temperature Tick the box to wait for the gas temperature to reach the set value before starting an evaporation Wait for plate temperature Tick the box to wait for the plate temperature to reach the...

Страница 10: ...ress the Reset Settings button to reset all settings in Common settings Evaporation Settings and Network and Firmware to their default values Calibrate Touch Press the Calibrate Touch button to calibr...

Страница 11: ...ure 17 Ensure that the manifold is held in position while the last screw is removed 3 With a steady grip remove the manifold Note Do not hold the manifold by the nozzles as this might bend the nozzles...

Страница 12: ...Time Mode Evaporate for a set period of time 4 Method Mode Evaporate using a predefined method 5 Split to left and right OR Join left and right The left and right cabinets operate independently OR The...

Страница 13: ...splay shows that the left side is ready to start the orange Start button is active and the right side is running an evaporation the blue Pause button and the red Stop button are active To perform a Ti...

Страница 14: ...ode In the Join left and right mode the left and right cabinets operate the same evaporation run with the same parameters see Figure 23 Figure 23 Temp Step Method 96 run in Join left and right mode Du...

Страница 15: ...utton to enter the desired name see Evaporation Parameters on page 15 6 When done press Save Note Once a method has been saved its previous settings cannot be recovered 7 In the Methods view press OK...

Страница 16: ...ers view where the evaporation parameters or the method name can be edited or a method can be copied Figure 29 Press and hold the Plate height button then move the lift by pressing the Up and Down arr...

Страница 17: ...an alarm sounds If operating each cabinet separately then the LED lights in each cabinet will turn green independently The Evaporation Finished dialog appears on the screen see Figure 34 The alarm co...

Страница 18: ...l risk for burn damage Open the cabinet door The well plate will descend Carefully remove the well plate or rack Be careful not to come in contact with the nozzles See Figure 35 Note The lift will ret...

Страница 19: ...ly dampened with isopropanol or ethanol 3 When the system has been cleaned connect the power cord and turn on the system Clean the Interior of the System Warning Never clean the surface where the mani...

Страница 20: ...following is recommended a For polar analytes chose solvent combinations with a high aqueous content e g an 80 20 solution of water and methanol b For lipophilic analytes chose solvent combinations wi...

Страница 21: ...plied by Biotage Incorrect fuses will void the warranty of the system and creates a potential fire hazard and a risk of personal injury 1 Turn off the system and disconnect the power cord 2 Using a fl...

Страница 22: ...into Storage Warning Ensure not to bend any of the nozzles If a nozzle is bent it is recommended that the manifold is replaced 1 Remove and clean the manifolds as described on page 20 2 Place the man...

Страница 23: ...er Temperature on page 7 Check that the sample is not left too long on the plate heater after the evaporation is completed Check that the gas flow is not too high and causing splashing see Determine t...

Страница 24: ...crew 1 Consumables Part No Description Qty 121 5201 Collection Plate 350 uL Square 50 121 5202 Collection Plate 1 mL Square 50 121 5203 Collection Plate 2 mL Square 50 121 5213 Collection Plate 2 mL R...

Страница 25: ...25 Notes Notes...

Страница 26: ...art Number 418001 B 2021 Biotage All rights reserved No material may be reproduced or published without the written permission of Biotage Information in this document is subject to change without noti...

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