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behr InKjel P

© behr Labor-Technik 2014

142109

Spare Parts

Description

Art.-Nr.

Round-bottom digestion vessel 250 ml, for sample rack EG 12

B 0021 7959

Round-bottom digestion vessel 500 ml, for sample racks EG 6, EG 4/500

B 0021 8195

Round-bottom digestion vessel 750 ml, for sample rack EG 4/750

B 0021 8218

Glass collector tube for exhaust collector AE 12 (for 12 vessels of 250 ml)

B 0023 1828

Glass collector tube for exhaust collector AE 6 (for 6 vessels of 500 ml)

B 0023 1825

Glass collector tube for exhaust collectors AE 4 (for 4 vessels)

B 0023 1826

Silicone hose 25 mm inner ø, 33 mm outer ø, for the silicone buffers

B 0022 4998

PTFE watch-glass disk 50 mm ø with 13 mm boring (for the suction nozzles)

B 0022 5947

Sample rack for 12 digestion vessels of 250 ml

B 0021 8087

Sample rack for 6 digestion vessels of 500 ml

B 0021 8086

Sample rack for 4 digestion vessels of 500 ml

B 0021 8085

Sample rack for 4 digestion vessels of 750 ml

B 0021 8080

Exhaust collector for 12 digestion vessels

B 0021 8090

Exhaust collector for 6 digestion vessels

B 0021 8089

Exhaust collector for 4 digestion vessels

B 0021 8088

Suction hose, Viton, 2 m

B 0022 4985

Hose clip for the suction hose

B 0023 3672

KjelTabs KT 1 Catalyst Tabs (5 g K

2

SO

4

 + 0.5 g CuSO

4

), 1000 Tabs

B 0021 7934

KjelTabs KT 2 Catalyst Tabs (5 g K

2

SO

4,

 0.15 g CuSO

4

, 0.15 g TiO

2

), 1000 Tabs

B 0021 7938

KjelTabs KT 3 Catalyst Tabs (3.5 g K

2

SO

4

 + 0.4 g CuSO

4

), 1000 Tabs

B 0021 7937

KjelTabs KT 4 Catalyst Tabs, containing selenium (3.5 g K

2

SO

4

 + 3.5 g Se), 1000 Tabs

B 0049 0920

Boiling chips, 100 g

B 0021 7914

Содержание InKjel P

Страница 1: ...142109 InKjel P Digestion Unit User s Manual ...

Страница 2: ...simple guidance For reasons of safety in use of the system please follow all safety warnings carefully These are designated in the text by a warning symbol Additional information which is useful and important for an understanding of the manner of operation of the apparatus is denoted by a stripe in the margin We wish you success in the use of the behr InKjel P digestion unit ...

Страница 3: ...of this appli ance may be performed only by authorized specialist staff Danger glass can break and cause injury In working with glass components observe all appro priate safety precautions Be careful in working with corrosive substances Follow the safety guidance in the pertinent Safety Data Sheets Hazard from toxic gases During the Kjeldahl digestion vapours of sulfuric acid and other toxic gases...

Страница 4: ...e On 9 Using the InKjel P 9 The operating unit 9 The Start menu 10 Configuring the InKjel P to meet your needs 10 Write a heating program 12 Processing samples 13 Maintenance 16 Cleaning the Exhaust Collector 16 Changing the Exhaust Collector Tube 17 Keep your Device Working Reliably as Long as Possible 19 Do Not Use Damaged Vessels 19 Always Use a Scrubber 19 Don t Leave Any Places Empty 19 Avoid...

Страница 5: ...perating safety and reliability and the longest possible service life for your digestion unit Always operate the appliance in accordance with the instructions and data contained in this oper ating manual Modifications to the appliance will result in forfeit of any guarantee claims and can result in serious deficiencies in the unit s operating safety and reliability During the Kjeldahl digestion su...

Страница 6: ... behr InKjel P 142109 Overview of the behr InKjel P Suction hose Exhaust collector Mounting rack Drip pan Sample rack Heating slot with IR radiators InKjel base unit Control unit Mains switch ...

Страница 7: ...ectronic and mechanical modules of this appliance may be performed only by authorized specialist staff Fixing the mounting rack Place the base unit on a level horizontal surface in such a way tha the mounting brackets point to the rear Insert the mounting rack between the mounting brackets from above Do not push them down to the bottom but align the lower edges of the rails with the lower edges of...

Страница 8: ...ion hose to an appropriate scrubbe device e g a behrosog scrub ber See also the instruction manual of the scrubber Hang the exhaust collector into the upper hooks of the mounting rack Connecting to Mains Power Make sure that your local mains voltage corresponds to the voltage specified on the instrument label of your InKjel P Make sure the mains switch on the front of the device is in 0 position P...

Страница 9: ...nu appears once the initialization routine has been com pleted Prog 01 01 START EIN The device is now ready for operation Don t wonder if the start menu appears in German This is the factory setting you ll soon see how to change it see pp 10 11 Using the InKjel P The operating unit You can program and operate your behr InKjel P quite simply using a single button The principle is the same in all ca...

Страница 10: ...ng the button Store the value by pressing the operating button again The Start menu 1 If no program is running but a starting time has been selected the starting time is displayed here This box is otherwise blank 2 Start menu item The temperature program most recently selected starts if this menu item is selected What program this is is1 indicated at bottom left 3 Preheat ON OFF menu item if this ...

Страница 11: ...ct digit appears and then press it If an illogical value is entered such as 26 for the hours or 61 for minutes for example the unit will reject the value and instead jump back to the first digit of the setting Use to move to the next page of this menu Second page Autostart settings START TIME AUTOSTART OFF 11 20 The Autostart settings can be selected on this page You can for example set the unit t...

Страница 12: ...you are currently editing are shown in the top line Program 07 05 for example means the fifth step in Program No 07 In the lines below specify the values for this program step the Heat output in of total output ranging from 1 to 100 and the Time in minutes The unit will then heat at the specified percentage of total heat output for the time specified You can enter the values digit by digit If you ...

Страница 13: ...ater and then to get the sulfuric acid boiling Again in the second step continue heating at a lower heat output for the rest of the time When digesting samples that will release large quantities of gas it may be necessary to have the sample react with the sulfuric acid in the cold at first or to heat up slowly and cautiously For many kinds of sample materials we have prepared application sheets we...

Страница 14: ...t s where it meets the least resistance Also condensate may drip out in the empty places producing caustic fumes and damaging the device Always insert the complete set of sample vessels to make sure scrubbing will work correctly Place the sample rack bearing the samples in the heating cavity Put the exhaust collector on top of the sample rack and switch the exhauster system on Select the Start men...

Страница 15: ...ce Wash your hands with water after contact with the condensate Insert the drip tray after inserting the exhaust collector in the mounting rack Grasp the sample rack using the two red handles Lift the rack carefully together with the exhaust col lector and hang it on the lower hooks of the mounting rack Leave the exhaust collector on the sample rack until the samples have cooled down Once the samp...

Страница 16: ... of breakage of glass Always adhere to your professional association s regulations when handling glass elements Caution there may be sulphuric acid in the exhaust collector It might burn you Adhere to the current Hazardous Sub stances Ordinance If during a digestion the exhaust collector has been contaminated by sample components you can easily clean it Cautiously lay the exhaust collector upside ...

Страница 17: ...collector Lay the exhaust collector to the edge of the desk so one of the red handles comes to lie beneath the desk but make sure the exhaust collector won t slide off the desk The glass collector tube is mounted to the roof of the housing with two pipe clips Two pieces of silicone hose are inserted each between the glass tube and the hous ing and between the glass tube and the pipe clips as buffe...

Страница 18: ...the new collector tube in such a way as for the screwholes to fit on the scre wholes of the housing Screw the pipe clips to the housing again but do not yet tighten them first you need to align the new col lector tube properly Shift the new collector tube in such a way that the exhaust nozzles have the same distance from the housing on both sides Now screw the pipe clips tight ...

Страница 19: ...zzles must reach into the vessels the uppermost disk on the nozzles will rest on the rim of the vessel Adjust the suction flow rate in such a way that the white fumes are sucked off but no vacuum will arise Don t Leave Any Places Empty The suction air current will always go the way of least resistance So if you leave some sample places empty if there is no sample vessel under the suction nozzle th...

Страница 20: ... rise so fast maybe even preparing the sample in the evening and letting it rest overnight before starting the digestion That will sometimes work but it won t always work Some sample materials will start reacting with the sulfuric acid in the cold and the longer it takes the sample to reach digestion temperature the higher the foam will rise In these cases it is better to have the sample come to d...

Страница 21: ...3 mm boring for the suction nozzles B00225947 Sample rack for 12 digestion vessels of 250 ml B00218087 Sample rack for 6 digestion vessels of 500 ml B00218086 Sample rack for 4 digestion vessels of 500 ml B00218085 Sample rack for 4 digestion vessels of 750 ml B00218080 Exhaust collector for 12 digestion vessels B00218090 Exhaust collector for 6 digestion vessels B00218089 Exhaust collector for 4 ...

Страница 22: ...0 x 750 x 440 mm Weight approx 20 kg Time range 0 199 minutes in 1 min steps Heat output range 0 100 in 1 steps Programs max 25 Display LCD Customer Service behr Labor Technik GmbH Spangerstraße 8 D 40599 Düsseldorf Phone Customer service 49 211 7 48 47 17 Telefax 49 211 7 48 47 48 E mail info behr labor com ...

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