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P-OQ1011-3276-J01 

Operational 

Qualification   (OQ) 

 

 

 

 

Automatic Digital   

Refractometer RX-5000i 

 

Apply distilled water on the prism and press “ZERO SET.” Touch “START” and measure the 

distilled water. Wipe the water off the prism. 

 

3-1. Display Test 

 

   After the instrument is turned on, the opening message will be displayed, and then the 

home screen will appear. Make sure that no truncated or garbled letters are found on the 

screen. 

 

3-2. Touch Key Test   

 

1)

 

Touch “HOME” on the measurement screen. Touch “SET UP” to display the set up 

screen. Touch each icon and check the values against the factory default values found 

in the instruction manual. Once the contents of each menu have been checked, return 

to the set up screen.   

2)

 

Touch “HOME” on the set up screen to display the home screen. Touch 

“MEASUREMENT” to return to the measurement screen. 

 

3-3. Error Message Test 

 

   

The measurement screen is currently displayed. 

 

1) Make sure that the prism is clean and touch “ZERO.” “WAITING,” and then “READING” 

will be displayed. “OUT OF WATER” will be displayed and printed. 

2) Make sure that the prism is clean and touch “START.” “WAITING,” and then “READING” 

will be displayed. After a few seconds, “OUT OF RANGE” will be displayed and printed. 

3) Apply the 30.00% Brix standard sucrose solution and touch “ZERO.” “WAITING,” and then 

“READING” will be displayed. A few seconds later, “OUT OF WATER” will be displayed. 

Wipe the solution off the prism. 

4)  Place a round sheet and apply  the solution with 1.585 nD or above, such as 

monobromonaphthalene, on the prism and touch “START.”  “WAITING,” and then 

“READING” will be displayed. A few seconds later, “OUT OF RANGE” will be displayed. 

Wipe the solution off the prism.   

 

   

 

The RX-5000i  is currently in MODE-1.  Program a user scale and check the “OUT OF 

SCALE” error message and WAIT TIME function. 

 

1)

 

Touch “HOME” on the measurement screen to display the home screen. Touch “SCALE” 

and select the uppermost empty row with the smallest scale number on the scale list. 

Touch “EDIT” at the bottom of the screen. The scale-edit screen will be displayed. 

2)

 

Touch the scale number on the upper left corner of the screen. Enter the name of the 

scale in SCALE NAME, using the alphabet & number keys. In this case, type in “Brix050.” 

Touch “USER” from the scale types. Touch “ENTER,” and the user scale data screen will 

appear. 

3)

 

Enter the refractive index in “nD” and the corresponding concentrations in “DATA,” 

using the ten-key pad.

  

 

Содержание RX-5000i

Страница 1: ...strument may not perform to the required specifications if tested in an environment that deviates from the criteria below Performance Test Environment Ambient temperature 15 0 30 0 Relative humidity Below 85 Power supply AC 100V 50 60Hz The RX 5000i should be placed indoors on a level surface such as a desk or table 2 Standard of Evaluation A performance test requires a standard of evaluation Cons...

Страница 2: ...ge to test the accuracy repeatability and span This procedure almost replicates the performance tests executed for calibration purposes The accuracy of the RX 5000i is expressed as 0 0000X for refractive index and 0 0X for Brix 4 Necessary Items 1 Samples distilled water 10 00 Brix standard sucrose solution 30 00 Brix standard sucrose solution 1 51 nD standard liquid round sheets 2 Plastic spoon o...

Страница 3: ...d measure the 1 51 nD standard liquid Record the measurement value in the log sheet 6 Repeat the steps 2 through 5 for 4 times Record the measurement value each time 7 Recorded Data Review the recorded measurement data 1 Cross reference the data recorded on the log sheet and the data printed from the printer 2 The RX 5000i stores the last 500 measurement data Once the maximum memory capacity is re...

Страница 4: ...P OQ1011 3276 J01 4 Operational Qualification OQ Automatic Digital Refractometer RX 5000i 4 Lastly have the operator and an approver sign the report ...

Страница 5: ...ed 3 Let the instrument warm up for at least 20 minutes 4 Set the target temperature TARGET to 20 00 in mode 1 Make sure that the measurement values are displayed in Brix 5 Make sure that the date and time displayed are correct 6 Check the print settings Touch SET UP on the home screen Touch PRINTER and the print settings will be displayed Check the following items to be printed DATE TIME ATAGO RX...

Страница 6: ...RT WAITING and then READING will be displayed After a few seconds OUT OF RANGE will be displayed and printed 3 Apply the 30 00 Brix standard sucrose solution and touch ZERO WAITING and then READING will be displayed A few seconds later OUT OF WATER will be displayed Wipe the solution off the prism 4 Place a round sheet and apply the solution with 1 585 nD or above such as monobromonaphthalene on t...

Страница 7: ...n above connect a printer and turn the power on Turn the power on to the RX 5000i Make sure that the opening message is printed 2 Apply distilled water on the prism and zero set the instrument Make sure that ZERO SET END is printed 3 Measure the 30 00 Brix standard sucrose solution Make sure that the sample number measurement values in nD and Brix and measurement temperature are displayed The item...

Страница 8: ...NTER 5 SAVING will be displayed on the screen The data have successfully been copied to the USB drive once COMPLETED is displayed 6 Disconnect the USB drive from the instrument and connect it to a PC to check the contents 4 Publication to Operational and Performance Qualification Test Results Report Record the function test items on the Operational and Performance Qualification Test Results Report...

Страница 9: ...ard liquid 1st measurement 2nd measurement 3rd measurement 4th measurement Average Margin of error Standard of evaluation 0 05 Brix 0 00006 nD accuracy 2 Function Test Results Items Results Switch Power switch Screens and icons Home screen Set up screen ZERO icon START icon Display Opening message Date and time Display Messages ZERO SET END OUT OF WATER OUT OF RANGE OUT OF SCALE Output 1 Printer U...

Страница 10: ...P OQ1011 3276 J01 10 Operational Qualification OQ Automatic Digital Refractometer RX 5000i yyyy mm dd yyyy mm dd Operator Signature Approver Signature ...

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