Anton Paar TTK 600, Справочное руководство

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8 Performing a Measurement
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9. Open the gas tight compartment (4) by pulling
down the closing mechanism (2).
10.Insert the sample holder (1) into the fixing ring of
TTK 600 by pushing the sample holder loader
(3) inwards.
11.Fix the sample holder (1) to the fixing ring by the
use of the Torx screw (6) on the sample holder
loader. To do so, use the constant force Torx
screw driver that was delivered with the instru-
ment. Screw in till the first click occurs.
12.Pull back the sample holder loader (3).
13.Close the gas tight compartment by pushing in
the closing mechanism.
14.Sample is now ready for the experiment.
In order to remove the sample from TTK 600, pro-
ceed as follows:
1. Open the gas tight compartment (4) by pulling
down the closing mechanism.
2. Push the sample holder loader (3) inwards.
3. Use the torx screw (6) on the sample holder
loader to unscrew the sample holder from the
fixing ring of the instrument.
4. Insert the sample to the gas tight compartment
by pulling back the sample holder loader(3).
5. Close the gas tight compartment by pushing in
the closing mechanism.
6. Remove the antechamber from TTK 600 by
unscrewing the two mounting screws.
7. Bring the sample back to the glove box if neces-
sary.
8.4.6 Mounting and Use of the Battery Sam-
ple Holders
Before mounting the battery sample holder, ensure
that the chamber is mounted on the adapter in the
correct position for the sample holder which will be
used. Details for the mounting of the adapter can be
found in chapter 4.3.
Battery Sample Holder (Reflection):
Fig. 59: Reflection sample holder
To mount the battery sample holder (reflection), pro-
ceed as follows:
1. Insert the sample holder in the groove of the
sample holder fixing ring (1) while guiding the
cable of the Pt100 (2) behind the heating/cool-
ing block.
2. Use the Torx screw driver that was delivered
with the instrument to fix the sample holder to
the fixing ring by tightening the screw (3) until
the first click of the Torx screw driver occurs
(corresponds to a force of 1.1 Nm).
3. Connect the Pt100 to the Pt100 plug connector
(4).
4. Connect the electrode cable to the electrode
connector in the housing of TTK 600 (5).
5. Close the lid of the TTK 600.
6. Switch on the heater of CCU 100.
To align the sample in the beam, the standard I1/2
method can first be used (see chapter 6.2). If the X-
ray tube and detector are correctly aligned, the sur-
face of the sample holder should first block the X-ray
NOTICE
If vacuum has been applied during the experi-
ments before, always bring the instrument back
to ambient pressure before you try to open the
gas tight compartment.
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