Agilent Technologies 5800 ICP-OES, Руководство пользователя

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Operation
44 Agilent 5800 and 5900 ICP-OES User's Guide

Highlight the wavelength you wish to use from the list of available
wavelengths displayed. Click Add.
NOTE
Alternatively, press CTRL and select the element from the periodic table to add the
primary wavelength for the selected element to your method.
The element will appear in the table with the selected wavelength and default
settings selected.
NOTE
It is recommended to add multiple wavelengths for each element. Similar results for
each wavelength indicate there are no interferences present. If there are different
results, check IntelliQuant for the right wavelength to report.
4 Check that there are no known interferents or other analytical lines close to the
selected analytical line. Their relative intensity will govern how close the lines
can be to each other. For example, if your matrix contains an element that is
not of analytical interest, but is a potential interferent and has a line close to
one of your analytical lines, the concentration of that element in your matrix
will determine whether you need to choose another analytical line.
5 Make any required adjustments to each element including selecting a different
wavelength, entering additional information into the ‘Label’ column, and
selecting the type (choose from analyte, internal standard or interferent).
6 Click Conditions to modify both common settings for the run and settings for
each element. Up to eight different measurement conditions can be used.
7 Click QC to enter the method detection limits, select the QC tests to be used
and which error actions should be performed if an error occurs.
8 Click IEC to enter the concentration of the elements in your analyte and
interferent standards.
9 Click Standards to enter the concentration of the elements in your standards
and select whether to use other options such as Standard Additions or
MultiCal. In addition, also select whether to use the blank in calibrations and
whether to enable reslope.
10 Click Sequence to specify the number of samples, insert QC tests, select the
solution type, edit the sample labels and end of run actions.
11 Click FACT to manually create FACT models or to set the method up to
automatically create them during analysis.
12 If you are using an autosampler, click the ‘Autosampler’ tab to select the racks
and probe depth (if needed). Depending on the autosampler selected, options
may vary.