Xylem SI Analytics TITRONIC 500, Operating Manual

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TABLE OF CONTENT
1 Technical Specifications of the TITRONIC
®
500 piston burette ......................... 87
Notes to the operating manual ................................................................................................ 87 1.1
Intended Use ........................................................................................................................... 87 1.2
Technical Specifications .......................................................................................................... 88 1.3
1.3.1
Piston burette TITRONIC
®
500 ............................................................................................... 88
Warning and safety information .............................................................................................. 90 1.4
2 Installation and Commissioning........................................................................... 91
Unpacking and setting up ........................................................................................................ 91 2.1
Back panel of the piston burette TITRONIC
®
500 ................................................................... 92 2.2
Connection and installation of the piston burette and the magnetic stirrer TM235 ................. 93 2.3
Installation of the Z 300 Rod Foot Plate (Optional) ................................................................. 93 2.4
Setting the language ............................................................................................................... 94 2.5
Exchangeable head (WA) ....................................................................................................... 95 2.7
2.7.1
Installation of the Interchangeable Unit ................................................................................... 95
2.7.2 Placing and Replacing of the Interchangeable Unit ................................................................ 96
2.7.3 Programming of the titration unit ............................................................................................. 97
2.7.4 Initial Filling or Rinsing of the Entire Interchangeable Unit ..................................................... 99
Installing the burette tip ......................................................................................................... 101 2.8
Replacing the Glass Cylinder and the PTFE Piston ............................................................. 102 2.9
Combination with Accessories and Additional Devices ........................................................ 103 2.10
2.10.1
Connecting a printer .............................................................................................................. 103
2.10.2 Connecting a USB device ..................................................................................................... 103
2.10.3 Connection of analytical balances ......................................................................................... 103
3 Working with the piston burette TITRONIC
®
500 .............................................. 104
Front Keyboard ...................................................................................................................... 104 3.1
Display ................................................................................................................................... 104 3.2
Manual controller ................................................................................................................... 105 3.3
External PC Keyboard ........................................................................................................... 105 3.4
Menu Structure ...................................................................................................................... 106 3.5
Main Menu ............................................................................................................................. 108 3.6
3.6.1
Manual Titration ..................................................................................................................... 108
3.6.2 Dosage .................................................................................................................................. 111
3.6.3 Preparing Solutions ............................................................................................................... 113
4 Method parameters.............................................................................................. 114
Method editing and new method ........................................................................................... 114 4.1
Default method ...................................................................................................................... 115 4.2
Copy Method ......................................................................................................................... 115 4.3
Delete Method ....................................................................................................................... 116 4.4
Change Method Parameters ................................................................................................. 116 4.5
4.5.1
Method type ........................................................................................................................... 116
4.5.2 Result .................................................................................................................................... 117
4.5.3 Formula Editor ....................................................................................................................... 123
4.5.4 Dosing parameter .................................................................................................................. 129
4.5.5 Sample identification ............................................................................................................. 130
4.5.6 Documentation ...................................................................................................................... 131
5 System settings ................................................................................................... 132
Interchangeable Unit - Reagents .......................................................................................... 132 5.1
RS-232 Settings .................................................................................................................... 134 5.2
Date and Time ....................................................................................................................... 136 5.3
Password ............................................................................................................................... 137 5.4
5.4.1
Creation of the first Administrator .......................................................................................... 137
5.4.2 Creation of additional users .................................................................................................. 141
5.4.3 Predefined rights and definable rights................................................................................... 142
5.4.4 Delete of users ...................................................................................................................... 146