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Section 6  

Operation

Caution

Do not use in the presence of flammable or combustible materials

or explosive gases. Do not use in the presence of pressurized or sealed
containers - fire or explosion may result, causing death or severe injury. 

s

Caution

Do not heat any substance above a temperature which will cause

it to emit toxic fumes - death or severe injury may result. 

s

If it is necessary to set temperature before loading oven, push the power
switch ON and note that the power switch light is lit. Rotate the
thermostat knob to approximate the desired setting. The heater status lamp
will be steadily lit until the chamber temperature approaches the
thermostat setting. Wait several heat cycles until the temperature has
stabilized.

Check the thermometer and rotate the thermostat knob clockwise to raise
the set point, or counterclockwise to lower it. After oven temperature has
stabilized, check the temperature again and make further thermostat
adjustments until the thermometer consistently shows the desired
operating temperature. Push the power-switch OFF and allow the oven to
cool down, or, if a batch is ready, the oven can be loaded immediately.

The thermometer can be removed and put back after loading if that is
more convenient. Note that the thermometer sensing element must be in
direct contact with a shelf for an accurate reading.

For best results, distribute the load evenly in the chamber, at least 1 inch
away from chamber walls and resting directly on the shelves. DO NOT
PLACE FLAMMABLE SOLVENTS OR VAPORS in the oven and avoid
spilling acids. Be careful not to heat substances above their autoignition
temperatures.

While the oven door is open, apply high temperature vacuum grease to the
door gasket. Close the door and push the power switch ON. If oven
temperature was not previously set, review above at “TEMPERATURE
CONTROL” to set the desired operating temperature.

Vacuum Oven

6-1

VWR Collection

Temperature Control

Loading the Oven

Summary of Contents for 89508-426

Page 1: ...User Manual VWR Collection Models 89508 426 and 89508 428 Vacuum Oven Operating and Maintenance Manual 7006291 Rev 0...

Page 2: ...7 13 Original ccs REV ECR ECN DATE DESCRIPTION By Preface Vacuum Oven i Models covered in this manual Catalog Numbers Model Numbers Voltage Feature Size cu ft 89508 426 6291 120V Dial thermometer 0 7...

Page 3: ...stments and maintenance must be performed by qualified service personnel s Material in this manual is for information purposes only The contents and the product it describes are subject to change with...

Page 4: ...equipment that has been put on the market after 13 August 2005 This product is required to comply with the European Union s Waste Electrical Electronic Equipment WEEE Directive 2002 96 EC It is marke...

Page 5: ...rol 6 1 Loading the Oven 6 1 Unloading the Oven 6 2 Purging the Chamber with Inert Gas 6 2 Releasing the Vacuum 6 2 Maintaining Proper Vacuum Level 6 2 Routine Cleaning 7 1 Maintenance 7 1 Care and Cl...

Page 6: ...t helps maintain temperature uniformity effectiveness Temperature is controlled by a hydraulic thermostat and can be read on the dial thermometer The chamber of the unit is not designed for exposure t...

Page 7: ...conformance with local electrical codes It is most important that the user follow installation instructions exactly as written Failure to do so is likely to lead to improper operation erroneous calibr...

Page 8: ...rmometer Type Bimetallic dial type range from 0 C to 300 C in 5 C increments Chamber Dimensions 89508 426 10 W x 12 D x 10 H 25 x 30 x 25 cm 89508 428 14 W x 20 D x 14 H 36 x 51 x 36 cm Overall Dimens...

Page 9: ...onditions Indoor use only Operating 15 C to 40 C Humidity 20 to 80 Voltage Fluctuation 10 of nominal Installation Category II overvoltage in accordance with IEC 664 Pollution Degree 2 in accordance wi...

Page 10: ...must call for a damage inspection promptly s Place the unit where it will be operated away from drafts and wide variations in ambient temperature It should be near a power source that matches the uni...

Page 11: ...ded outlet If a plug must be installed use only the 3 prong grounded type rated for the unit load requirements and matching the power outlet Make sure the green ground wire is secured to the plug grou...

Page 12: ...ature A permanently set bimetallic thermostat not on the panel limits oven temperature at 250 C should the control thermostat fail 3 Vacuum Gauge Displays chamber level to 30 inches of mercury 4 Vacuu...

Page 13: ...has stabilized check the temperature again and make further thermostat adjustments until the thermometer consistently shows the desired operating temperature Push the power switch OFF and allow the o...

Page 14: ...vacuum with an inert gas Connect 1 4 inch ID tubing to the hose connector marked VENT and connect the other end of the tubing to the regulator at the inert gas source Start the gas flowing at no more...

Page 15: ...et with a solution of water and mild soap or detergent to clean off surface dirt marks or smudges Keep the vents clear of dust for free air circulation This will add to the service life of components...

Page 16: ...lm or coating However if free oxygen is not available due to scale or contamination buildup the metal surface may become vulnerable to rusting and corrosion as well as pitting But by maintaining neutr...

Page 17: ...nd the stainless steel surface cleaned with mild soapy water followed by a clean water rinse Anti fungal and anti bacterial additives are permissible to use as long as the pH of the aqueous solution i...

Page 18: ...n to soak the surface affected until rust and scale is loosened Immediately follow with a clean water rise Citric acid based cleaners Bathroom tub and tile cleaners A mixture of 20 nitric acid and 1 5...

Page 19: ...n Consult your staff chemist to determine what would be best for your stainless steel product and laboratory s Apply a high quality vacuum grease to the door gasket frequently especially before initia...

Page 20: ...Check the vacuum vent valve order a replacement if it is leaking Won t vent or evacuate Check for open fittings large leaks Check vacuum vent valve replace if bad Check tubing fittings for obstructio...

Page 21: ...VWR International LLC Radnor Corporate Center Building One Suite 200 100 Matsonford Road Radnor Pennsylvania 19087 United States 610 386 1700 www vwrsp com...

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