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UltiMate 3000 Series: 

SR-3000 Solvent Rack 

 

Operating Instructions

  

Page

 3 

1.2.2  Safety Precautions 

When working with analytical instrumentation, you must know the potential hazards of 

using chemical solvents.  

  Tip:

 

Before initial operation, make sure that you are familiar with the 

contents of this manual. 
For the safety precautions in French, see section 1.2.3 (

 page 6). 

  

Warning:

  All users of the device must observe the following safety precautions 

and all additional safety precautions in this manual to avoid the 

possibility of personal injury or damage to the device when operating 

the device or carrying out any maintenance or service procedures. 
Observe any warning labels on the device and see the related sections in 

these 

Operating Instructions

 

Protective equipment 

When performing any work on or near the HPLC system, wear personal protective 

equipment (protective clothing, safety gloves, safety glasses) as required by the hazard of 

the mobile phase and sample. For information about the proper handling of particular 

substance and for advice on specific hazards, refer to the material safety data sheet for the 

substance you are using. Observe the guidelines of Good Laboratory Practice (GLP). 
An eyewash facility and a sink should be close to the device. If any substance splashes on 

the eyes or skin, wash the affected area and seek medical attention. 

 

Hazardous substances 

Many organic solvents, mobile phases, and samples are harmful to health. Be sure that 

you know the toxic and infectious properties of all substances that you are using. You 

may not know the toxic or infectious properties of many substances that you are using. If 

you have any doubt about a substance, treat it as if it contains a potentially harmful 

substance. For advice on the proper handling of a particular substance, refer to the Safety 

Data Sheet (SDS) of the manufacturer. Observe the guidelines of Good Laboratory 

Practice (GLP). 
Dispose of waste substance in an environmentally safe manner that is consistent with all 

local regulations. Do not allow flammable, toxic, and/or infectious substances to 

accumulate. Follow a regulated, approved waste disposal program. Never dispose of 

flammable, toxic, and/or infectious substances through the municipal sewage system. 

 

Hazardous gases 

Install the HPLC system in a well-ventilated laboratory. If the mobile phase or sample 

includes volatile or flammable solvents, do not allow them to enter the workspace. If the 

mobile phase or sample includes volatile or flammable solvents, avoid open flames and 

sparks. 

Summary of Contents for SR-3000

Page 1: ...Scientific Dionex UltiMate 3000 Series SR 3000 Solvent Rack Operating Instructions Original Operating Instructions Revision 1 7 Date September 2013 2013 Thermo Fisher Scientific Inc Doc No 4820 3555 4820 3555 ...

Page 2: ...UltiMate 3000 Series SR 3000 Solvent Rack Operating Instructions ...

Page 3: ...l safety of the products was evaluated based on the following standard DIN EN 61010 1 2010 Safety requirements for electrical equipment for measurement control and laboratory use Part 1 General Requirements The Electromagnetic Compatibility EMC of the products was evaluated based on the following standard DIN EN 61326 2006 Electrical equipment for measurement control and laboratory use EMC Require...

Page 4: ...UltiMate 3000 Series SR 3000 Solvent Rack Page II Operating Instructions ...

Page 5: ... 9 1 4 Federal Communications Commission FCC Note 9 2 Installation and Maintenance 11 2 1 General Information 11 2 2 Unpacking 11 2 3 Positioning the Solvent Rack in the UltiMate 3000 System 12 2 4 Inside View 13 2 5 Solvent Reservoirs 14 2 5 1 General Precautions 14 2 5 2 Connecting the Solvent Reservoirs 15 2 6 Routine and Preventive Maintenance 16 3 Technical Information 17 4 Accessories Consum...

Page 6: ...UltiMate 3000 Series SR 3000 Solvent Rack Page ii Operating Instructions ...

Page 7: ...responsibility for any errors that may appear in this document This document is believed to be complete and accurate at the time of publication In no event shall Thermo Fisher Scientific be liable for incidental or consequential damages in connection with or arising from the use of this document The information contained in this document is subject to change without notice All rights reserved incl...

Page 8: ...the instrument against damage Référez vous à ce manuel pour éviter tout risque de blessure à l opérateur et ou protéger l instrument contre tout dommage Label according to the Measures for Administration of the Pollution Control of Electronic Information Products China RoHS guideline if necessary Étiquette China RoHs si nécessaire At various points throughout the manual the following symbols indic...

Page 9: ...ines of Good Laboratory Practice GLP An eyewash facility and a sink should be close to the device If any substance splashes on the eyes or skin wash the affected area and seek medical attention Hazardous substances Many organic solvents mobile phases and samples are harmful to health Be sure that you know the toxic and infectious properties of all substances that you are using You may not know the...

Page 10: ...slip out of their fittings or may not be screwed in This may result in substances spraying out of the open connections In an UltiMate 3000 system some components are made of PEEK This polymer has superb chemical resistance to most organic solvents However it tends to swell when in contact with trichlormethane CHCl3 dimethyl sulfoxide DMSO or tetrahydrofuran THF In addition it is attacked by concen...

Page 11: ...evel monitoring Pump manual The front panel tilts upward When lifting or moving the SRD always lift by the bottom or sides of the instrument This is to avoid damage to the instrument The open front panel door is not designed to carry weight Therefore you shall not place any objects on the open front panel door Do not use the solvent rack in ways other than those described in this manual Keep the o...

Page 12: ...urité des substances que vous utilisez Veuillez respecter des directives des Bonnes Pratiques de Laboratoire BPL Une installation permettant de se laver les yeux ainsi qu un lavabo doivent se trouver à proximité du système Si une substance quelle qu elle soit entre en contact avec vos yeux ou votre peau rincez abondamment la zone affectée à l eau puis Substances dangereuses De nombreux solvants or...

Page 13: ...nts au réservoir de déchets Capillaires électriquement conducteur devrait être mis à la terre Inflammation spontanée des solvants N utilisez aucun solvants avec une température d auto inflammabilité inférieure à 150 C Si une fuite se produit ces solvants peuvent s auto enflammer au contact d une surface chaude Capillaires connecteur capillaires connexions ouvertes Des capillaires en particulier le...

Page 14: ...ccessoires autorisés par Thermo Fisher Scientific Réglez toujours une limite de pression minimum pour le système HPLC Ceci prévient les dommages résultant de fuites ou de long terme fonctionnement à sec de la pompe Activez la surveillance de niveau liquide pour des réservoirs manuel de pompe Lorsque vous soulevez ou l instrument tenez le toujours par le dessous ou par les côtés de l unité Soulever...

Page 15: ...ply with the limits for a Class A digital device pursuant to part 15 of the U S FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instruction manual may cause harmful inte...

Page 16: ...UltiMate 3000 Series SR 3000 Solvent Rack Page 10 Operating Instructions ...

Page 17: ...ge that may have occurred during transit Tips Immediately report any shipping damage to both the incoming carrier and Thermo Fisher Scientific Shipping insurance will compensate for the damage only if reported immediately Keep the original shipping container and the packing material They will provide excellent protection for the solvent rack in case of future transit Shipping the rack in any other...

Page 18: ...individual modules for example as shown in Fig 1 However the arrangement of the system modules depends on the application Fig 1 Module arrangement for an UltiMate 3000 system example If the solvent rack is part of an UltiMate 3000 RSLCnano or Proteomics MDLC system the related system manual provides information about how to arrange the system modules and set up the systems for these applications D...

Page 19: ...vec des réservoirs Important When lifting or moving the solvent rack always lift by the bottom or sides of the unit Lifting the solvent rack by the front panel may damage the front panel door The open front panel door is not designed to carry weight Therefore you should not place any objects on the open door Important Lorsque vous soulevez ou l instrument tenez le toujours par le dessous ou par le...

Page 20: ...tandard the filter frits shipped with the solvent rack are stainless steel frits If the UltiMate 3000 system includes a biocompatible pump NCS 3500RS or NCP 3200RS replace the stainless frits with the frits from the accessories kit of the module To do so unscrew the top part of the filter holder from its bottom part and replace the filter frit When placing the new filter frit into the bottom part ...

Page 21: ...and is not deformed Cut the tubing straight if necessary Use only the original Dionex solvent lines 4 Place the complete assembly in the solvent reservoir 5 Tighten the reservoir cap hand tight Press the retaining guide into the hole in the reservoir cap to ensure that the solvent line is hold in place inside the reservoir Fig 3 Connecting the solvent lines to the reservoir When replacing a solven...

Page 22: ...fic Service for Dionex HPLC Products An RMA Return Material Authorization number is required in order to track your instrument Always use the original packaging and observe the packing instructions when shipping the solvent rack Shipping the rack in anything other than the original packaging will void the warranty For more information see the warranty statement in the terms of sale If the original...

Page 23: ...5 L reservoirs or sixteen 0 5L reservoirs Wetted parts PEEK FEP and ETFE ECTFE Inline filter frit SST PEEK or Titanium Environmental conditions Range of use Indoor use Temperature 10 C to 35 C Air humidity max 80 rel humidity non condensing Pollution degree 2 Dimensions h x w x d 10 x 42 x 51 cm 3 9 x 16 5 x 20 in Emission sound pressure level No emission Weight 3 0 kg 6 6 lbs without reservoirs T...

Page 24: ...UltiMate 3000 Series SR 3000 Solvent Rack Page 18 Operating Instructions ...

Page 25: ...0 0013 Cap to close the holes in the bottle cap 20 Included in 6000 0047 Retaining guide solvent reservoir 4 Included in 6000 0042 1 L solvent reservoir with cap 4 Included in 2270 0012 4 2 Consumables and Spare Parts Description Part No Filter holder top and bottom parts for solvent filter pack of 6 filter holders to be used with all pumps except HPG 3200BX 6268 0115 Filter holder top and bottom ...

Page 26: ...UltiMate 3000 Series SR 3000 Solvent Rack Page 20 Operating Instructions ...

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