Sigma 10208 Operating Manual Download

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Version 04/2008, Rev. 1.18 of 07/06/2012

Translation of the original operating manual

Formatiert:

Englisch (Großbritannien)

Operating Manual

Centrifuge

2-6E

from serial no. 124764

Please retain for later use!

Summary of Contents for 10208

Page 1: ...ersion 04 2008 Rev 1 18 of 07 06 2012 Translation of the original operating manual Formatiert Englisch Gro britannien Operating Manual Centrifuge 2 6E from serial no 124764 Please retain for later use...

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Page 3: ...ht by Sigma Laborzentrifugen GmbH An der Unteren S se 50 37520 Osterode am Harz Germany Phone 49 0 55 22 50 07 0 Fax 49 0 55 22 50 07 12 E mail info sigma zentrifugen de For service please use our ser...

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Page 7: ...perating Manual 15 2 3 Informal Notes on Safety 15 2 4 Safety Instructions for Centrifugation 16 2 4 1 Special Instructions 16 2 4 2 Resistance of Plastics 17 2 5 Prohibited Centrifuging Operations an...

Page 8: ...d Wire Check 26 5 2 Initial Start Up 27 5 2 1 Switching the Centrifuge ON 27 5 2 2 Opening and Closing the Lid 27 5 2 3 Installation of Rotors 28 5 2 4 Installation of Accessories 29 5 2 4 1 Carrier S...

Page 9: ...ifuge cannot be started 39 6 2 3 Centrifuge decelerates during Operation 39 6 2 4 Lid cannot be opened 40 6 2 5 Emergency Lid Release 40 6 2 6 Error Codes 41 6 2 7 Service Contact 42 7 Care and Mainte...

Page 10: ...mum speed for tubes 55 10 2 Graphical Representation of the Rotors 55 11 Appendix 56 11 1 Formulae Mathematical Relations 56 11 1 1 Relative Centrifugal Force RCF 56 11 1 2 Density 56 11 1 3 Speed Gra...

Page 11: ...ed by all persons operating the centrifuge In addition the local rules and regulations for the prevention of accidents must be complied with 1 2 Intended Use Centrifuges are power driven machines that...

Page 12: ...Max kin energy Nm 3 900 480 2 466 1 610 Other parameters Time range Storage locations 10 sec 11 h 59 min short run continuous run 10 Physical data Depth mm Width mm Height mm Weight kg EMC as per EN 6...

Page 13: ...ing oil Part no 70 104 1 tube of grease for load bearing bolts Part no 70 284 Spare fuses Part no 70149 for 220 240 V Part no 70102 for 120 V Documentation Operating manual incl EU Declaration of Conf...

Page 14: ...d emploi Ein Netzverbindung On Power Marche mise sous tension Aus Netzverbindung Off Power Arr t mise hors tension Schutzleiteranschluss Protective earth ground Liaison la terre Erde Earth ground Ter...

Page 15: ...r s importante Fig 2 2 Symbols used in the Operating Manual 2 3 Informal Notes on Safety The operating manual is an integral part of the product Please retain the operating manual throughout the servi...

Page 16: ...must be loaded symmetrically at equal weights Please observe the instructions on the Installation of accessories see 5 2 4 page 29 2 4 1 Special Instructions If liquids with a density 1 2 g cm3 are us...

Page 17: ...e or subject to any warranty claims Only persons who have read and understood the operating manual in whole are authorized to operate the centrifuge see 2 3 Informal Notes on Safety page 15 Keep infor...

Page 18: ...personnel see 6 2 7 Service Contact page 42 2 5 1 Special Hazards Do not open the lid when the rotor is in motion Do not reach into the rotor chamber when the rotor is in motion Do not hold your finge...

Page 19: ...ning of the trunnion pins in the rotor Screw connections Rotors and accessories see 5 2 5 Service Life of Rotors an Accessories page 30 2 7 Instructions for Emergency Situations If an emergency arises...

Page 20: ...rifuge always reach under the centrifuge from the side Install the transport safety device foamed plastic ring into the rotor chamber Transport the centrifuge within suitable packaging and if at all p...

Page 21: ...e side Attention The centrifuge weighs approx 21 kg Please retain the packaging for any possible future transport of the centrifuge 4 1 1 Transport Safety Device The transport safety device this centr...

Page 22: ...ortant to allow sufficient time for drying before the centrifuge can be used again 4 2 2 Connection The operating voltage on the name plate must correspond to the local supply voltage SIGMA laboratory...

Page 23: ...1 Description 5 1 1 Operating Elements Fig 5 1 Total view of the centrifuge Fig 5 2 Rear view of the centrifuge 9 10 11 1 Mains power switch 2 Stop key 3 Lid key 4 Display 5 Lid 6 Start key 7 Left ro...

Page 24: ...Plate 1 Manufacturer and registered office 2 Type name 3 Serial number 4 Max speed 5 Kinetic energy 6 Max density 7 Nominal voltage 8 Input fuse 9 Symbol for special disposal see chapter 8 10 CE mark...

Page 25: ...chronous motor 5 1 4 Operation and Display The display is a hermetically sealed LCD display It is operated by way of two rotary knobs and indicates the operating statuses 5 1 5 Electronic System The m...

Page 26: ...power supply i e the centrifuge cannot be started see 6 2 5 Emergency Lid Release page 40 5 1 6 2 Standstill Monitoring Opening of the centrifuge lid is only possible if the rotor is at a standstill...

Page 27: ...5 2 2 Opening and Closing the Lid The lid can be opened if the centrifuge is at a standstill and if the lid key is illuminated Press the lid key in order to open the lid see 5 3 7 Activating Deactivat...

Page 28: ...own screw clockwise with the supplied rotor wrench with 5 Nm In doing so hold the rotor at its outer rim After frequent use the rotor tie down screw must be loosened by some turns and fastened again T...

Page 29: ...5 2 4 1 Carrier Systems In order to ensure easy handling even if vessels of various sizes are used a carrier system was developed Load the opposite carriers with the same number of vessels and with t...

Page 30: ...form regular checks at least once per month for safety reasons Pay special attention to changes such as corrosion cracks material abrasion etc After 10 years they must be inspected by the manufacturer...

Page 31: ...p Function The softstart function is used to extend the acceleration time whereas the softstop function is used to extend the deceleration time The current combination is shown on the display The stop...

Page 32: ...isplay Fig 5 10 Select the option by pressing or turning the right rotary knob Set will now flash Turn the right rotary knob until the desired duration is displayed Press the right rotary knob in orde...

Page 33: ...he short run The message short run is displayed in the time display Fig 5 11 and the duration of the short run is also displayed When the start key is released the centrifuge decelerates at maximum po...

Page 34: ...d on the display Fig 5 13 Select the option by pressing or turning the right rotary knob Set will now flash Turn the right rotary knob until the desired value is displayed Press the right rotary knob...

Page 35: ...ary knob until the desired value is displayed Press the right rotary knob to confirm the selected value If this is not done the value will be automatically reset to the last setting It is also possibl...

Page 36: ...the right rotary knob until the desired program number is displayed Empty storage location numbers flash Press the right rotary knob to confirm the input The settings are now saved under this program...

Page 37: ...unction the padlock symbol Fig 5 18 will flash Now the centrifuge can be started and stopped but the settings cannot be changed Proceed in the same way in order to deactivate the function The current...

Page 38: ...ignal can be heard at the end of the operation as well as in the event of an error message or imbalance Press the lid key five times and on the fifth time hold it down for approx two seconds Proceed i...

Page 39: ...ly Power cord plugged in and line voltage present Plug in power cord correctly Fuse OK Replace fuse see fig 5 4 name plate page 24 Mains power switch on Switch on power Lid closed Close lid see 6 2 4...

Page 40: ...cy Lid Release In the event of a power supply failure it is possible to manually open the centrifuge lid using two stoppers that are secured with screws They are located on the front of the bottom pan...

Page 41: ...efrigerated centrifuges allow to slow down power off allow to cool down provide better ventilation 46 49 Imbalance error allow to slow down power off eliminate the imbalance 50 59 Lid error press lid...

Page 42: ...ifugen GmbH An der Unteren S se 50 37520 Osterode Germany Tel 49 0 55 22 50 07 84 25 Fax 49 0 55 22 50 07 94 25 E mail service sigma zentrifugen de outside Germany contact our agency in your country A...

Page 43: ...ntrifuge and rotors to intensive UV radiation or thermal stress e g by heat generators 7 1 1 Centrifuge Disconnect the power cord from the socket before cleaning Carefully remove all liquids including...

Page 44: ...with toxic radioactive or pathogenic substances clean them immediately with a suitable decontamination agent depending on the type of contamination Take suitable precautions for your own safety if the...

Page 45: ...signs of corrosion other changes Check the bores of the rotors and multiple carriers Replace any damaged components immediately for your own safety Protect the rotors lid seals and rubber cushions if...

Page 46: ...from the rotor chamber Grease the upper third of the centrifuge chamber with e g Vaseline Then let the rotor rotate for a few minutes at a moderate speed approx 2 000 rpm The glass and metal particles...

Page 47: ...min max time min max cycles Glass tubes 134 138 3 40 Polycarbonate tubes 115 118 30 40 20 Polypropylene tubes 115 118 30 40 30 Teflon tubes 134 138 3 5 100 Aluminum rotors 134 138 3 5 Polycarbonate Po...

Page 48: ...ointments in Germany use the service request form at www sigma zentrifugen de Service Area or contact SIGMA Laborzentrifugen GmbH An der Unteren S se 50 37520 Osterode Germany Tel 49 0 55 22 50 07 84...

Page 49: ...aration is enclosed in the return package we will perform the decontamination at your expense 2 Form for the return of defective parts This form is for the product related data They facilitate the ass...

Page 50: ...l in the enclosed declaration of decontamination Please comply with any other applicable local rules and regulations 8 2 Disposal of the Packaging Use the packaging to return the centrifuge for dispos...

Page 51: ...15020 15023 15024 15039 or Monovettes 9 10 ml 1 set 2 pcs suitable for 11030 11031 11032 11035 11036 13037 Multiple carrier made of plastic for 6 tubes 5 to 15 ml round bottom max 17 19 x 80 105 mm e...

Page 52: ...flat bottom or skirt max 25 31 x 65 95 mm e g Sterilin tube 30 ml Barloworld Scientific Ltd 1 set 2 pcs suitable for 13034 14032 Round carrier for 1 round bottom tube 50 ml max 35 38 x 70 105 mm e g...

Page 53: ...dius 13 9 cm min radius 7 8 cm Warning This rotor may heat up to more than 15 C during long runs of more than 15 minutes or repeated runs at short intervals 3 900 2 364 Adapters plastic vessels and gl...

Page 54: ...4 x 100 mm graduated 2 up to 50 ml in 2 ml increments suitable for 14032 17950 15049 Polycarbonate tube 65 ml 34 x 100 mm graduated 1 up to 50 ml in 1 ml increments suitable for 14032 17950 15100 Cent...

Page 55: ...heir useful volume the volume that is stated for the tube When using glass tubes the maximum value of 4 000 x g must not be exceeded except special high strengh glass tubes please refer to the informa...

Page 56: ...ned by the equation If then the speed or the rotation radius is changed the resulting RCF will be recalculated If the RCF is altered the speed will be adapted accordingly under the consideration of th...

Page 57: ...Version 04 2008 Rev 1 18 of 07 06 2012 page 57 of 65 Translation of the original operating manual Fig 11 1 Speed gravitational field diagram...

Page 58: ...K 12101 5 years 20x 1 15 1 15K 1 15P 1 15PK 12124 5 years 20x 1 15 1 15K 1 15P 1 15PK 12126 5 years 20x 1 15 1 15K 1 15P 1 15PK 9100 15 000 4 15C 4K15C 4 16 4 16K 6 15 6K15 6 16 6 16K without engravin...

Page 59: ...mony trichloride SbCl3 90 1 4 1 4 1 1 1 4 Benzaldehyde C7H6O 100 1 3 4 1 1 3 4 4 1 1 Benzene C6H6 100 3 2 4 1 3 4 4 1 1 Boric acid H3BO3 aqueous 1 3 1 2 1 1 1 Butyl acrylate C7H12O2 100 1 2 4 2 3 4 4...

Page 60: ...4 4 4 1 1 2 3 1 4 Hydrogen peroxide H2O2 3 1 3 1 1 1 1 1 1 3 Hydrogen peroxide H2O2 30 1 4 1 4 1 1 1 1 3 Hydrogen sulfide H2S 10 1 1 1 1 1 1 1 3 1 1 Iodine tincture of I2 1 4 3 1 1 4 4 1 1 Isopropyl...

Page 61: ...O3 10 1 1 2 4 1 1 1 Sodium carbonate Na2CO3 10 1 1 1 1 1 1 3 Sodium chloride NaCl 30 1 1 1 1 1 1 1 1 1 3 Sodium hydroxide NaOH 30 1 1 4 1 1 1 1 1 1 4 Sodium hydroxide NaOH 50 1 1 4 1 1 1 1 1 4 Sodium...

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Page 63: ...g cable 13 Contamination 18 43 44 Continuous heat resistance 46 Continuous run 25 33 Corrosion 16 18 19 29 30 43 44 46 Cost estimate 49 Cracks 19 30 45 Current consumption 12 Damage of the surface 45...

Page 64: ...the lid 27 Operating voltage 22 Operational safety 18 44 Overseas shipping 20 Padlock symbol 37 Parameter 25 56 Parameter error 41 Pathogenic substances 18 43 44 46 Performance data 12 Pivot bearing 4...

Page 65: ...g oil 13 44 45 Solvents 17 43 44 Sound signal 38 39 Spare fuse 13 Spare parts 54 Specialist personnel 48 Storage temperature 12 20 Stress corrosion 45 Structural changes 19 Supply voltage 22 Swing out...

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