Perkin-Elmer Lambda 11 Operation And Parameter Description Download Page 17 | Manualshive

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Summary of Contents for Lambda 11

Page 1: ...l service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE INSPECTION Remotely inspect equipment before purchasing with our interactive website at www instraview com LOOKING FOR MORE INFORMATION Visit us on the web at www artisantg com for more information on ...

Page 2: ...s Spectrometer Operation and Parameter Description Part Number B050 9912 Publication B2157 10 Release 3 0 Oct 94 UV Vis NIR Spectroscopy Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 3: ...ed by law Release History The information contained in this document is subject to change without notice This document contains proprietary information that is protected by copyright All rights are reserved No part of this document may be reproduced in any form whatsoever or translated into any language without the prior written permission of the Perkin Elmer Corporation or one of its subsidiaries...

Page 4: ... 2 3 Selecting an Application 2 3 2 4 Changing Parameters 2 4 2 5 Assigning the Mn Keys 2 5 2 6 Changing the Wavelength 2 6 2 7 Autozero and Background Correction 2 7 2 8 Running a Sample 2 8 2 8 1 Running an Application 2 8 2 8 2 Quick Sample Run 2 9 2 9 Print 2 10 2 9 1 Print Key Functions 2 10 2 10 Date and Time 2 11 2 11 Wakeup 2 12 B2157 10 Release 2 0 C 1 Artisan Technology Group Quality Ins...

Page 5: ...essages Printed by the Printer 4 4 Chapter 5 Help Messages Appendix 1 Accessories A1 2 A1 2 Al 3 Peltier Accessories A1 2 1Application 903 Peltier A1 3 A1 2 2Application 920 Peltier Calib A1 4 A1 2 3Cell Changers Al 6 Illustrations 1 1 Lambda 11 Operating Controls 1 1 1 2 Example of a Standby Display a 1 2 Al l Setting Accessory Parameter C 2 82157 10 Release 3 0 Artisan Technology Group Quality I...

Page 6: ...s important safety information Please read this information carefully before you install the instrument and observe the recommendations at all times Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 7: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 8: ...s that must be followed by the user to ensure safe operation and to maintain the instrument in a safe condition Before using this instrument it is essential to read the manual carefully and to pay particular attention to any advice it contains concerning potential hazards that may arise from the use of the instrument This advice is intended to supplement not supersede the normal safety code of beh...

Page 9: ...circumstances wo1 o1 Warning We use the term WARNING to inform you about situations that could result in personal injury to yourself or other persons Details about these circumstances are in a box like this one WARNING co1 o1 Caution We use the term CAUTION to inform you about situations that could result in serious damage to the instrument or other equipment Details about these circumstances are ...

Page 10: ... hand is likely to expose live parts Capacitors inside the instrument may still be charged even if the instrument has been disconnected from all voltage sources Safety Information Electricity To ensure satisfactory and safe operation of the instrument it is essential that the green yellow lead of the line power cord is connected to true electrical earth ground If any part of the instrument is not ...

Page 11: ...ted for further adjustment maintenance or repair this must only be done by a skilled person who is aware of the hazard involved Use only fuses with the required current rating and of the specified type for replacement Do not use makeshift fuses or short circuit the fuse holders Whenever it is likely that the instrument is no longer electrically safe for use make the instrument inoperative and secu...

Page 12: ...nce with the manufacturer s recommendations and local safety regulations Waste Disposal Waste vessels may contain acidic or organic solutions and small amounts of the elements that were analyzed If these materials are toxic you may have to treat the collected effluent as hazardous waste Refer to your local safety regulations for proper disposal procedures Deuterium lamps are maintained under reduc...

Page 13: ... Never gaze into the deuterium lamp Always wear UV absorbing protective glasses when the spectrometer top cover is open Radio Frequency This equipment generates radio frequency energy and if not installed and used properly i e in strict accordance with the instruction manual may cause harmful interference to radio communications S 6 B2157 10 Release 2 0 Artisan Technology Group Quality Instrumenta...

Page 14: ...ancias aparecen en recuadros como este We use the term CAUTION to warn you about situations that could result in serious damage to the instrument or other equipment Details about these circumstances are in a box like this one Nous utilisons le terme CAUTION pour vous prevenir de situations qui peuvent provoquer des serieux dommages ä l instrument ou a un autre equipement Tous details ä propos des ...

Page 15: ...s Switch OFF the spectrometer computer and printer and remove the line power connectors before you alter or make any new electrical connections WARNING Mettez le spectrometre l ordinateur et l imprimante en position OFF et ä enlevez les cables secteur avant de faire les moindres connexions electriques Spegnere lo spettrofotometro il computer la stampante e togliare l alimentazione principale prima...

Page 16: ...Preface mmm Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 17: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 18: ...functions and a list of the applications available on the Lambda 11 Installation Maintenance and System Description providing specific information on setting up and maintaining your Lambda 11 Operation and Parameter Description containing information on the operation of Lambda 11 This manual is the Operation and Parameter Descriptionmanual It describes the operation of the instrument and provides ...

Page 19: ...We use the term CAUTION to inform you about situations that could result in serious damage to the instrument or other equipment Details about these circumstances are in a box like this one CAUTION Note A note indicates important supplementary information Failure to follow this information could typically lead to incorrect analytical results or a deterioration in instrument performance Other useful...

Page 20: ...Introduction Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 21: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 22: ... single beam instrument intended for routine UV Vis analysis The parameters and entries to operate the instrument are entered through the keyboard and the information is shown on the display 82157 10 Release 2 0 1 1 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 23: ...igure 1 2 Example of a Standby Display The measurement range is from 0 T to 100 T or from 3 000A to 3 000 A If you obtain a value outside this range adjust the sample concentration dilute the sample or check that the beam is not obstructed Actual Wavelength 1 2 Keyboard CIO 0 10 ID C PR NT AUTOZERO QOTO APPUCAT1014 RUN STOP CO Lc CD O c D O oe ENTER 0 1 2 B2157 10 Release 2 0 Artisan Technology Gr...

Page 24: ...nt status Autozero refer to Section 2 7 page 2 7 To change the wavelength Starts or stops an application Calls up an application in turn Calls up a specified application when used with the numerical keys APPLICATION reassigns application to Me refer to Section 2 5 page 2 5 Numerical keys Decimal point APPLICATION saves an application to Mn Minus used to a enter negative numerical values b select t...

Page 25: ...1 4 82157 10 Release 2 0 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 26: ...Operation Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 27: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 28: ... has switched off before pressing the next key in the sequence This allows the software to complete the calculations and the motors to move the optics to their required setting 82157 10 Release 2 0 2 1 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 29: ...allow the lamps to warm up and stabilize This is normally sufficient for short analysis runs For longer analysis runs and higher stability allow two hours warm up time See also WAKEUP Section 2 11 page 2 12 2 Wait for the initialization phase 3 The display shows the last application used prior to shutdown 500 Onm 0 050ABS 2 SCAN 2 2 Shutdown 1 Remove samples from instrument 2 Press APPLICATION to ...

Page 30: ...each the application you require Type the application number and press APPLICATION to call up a particular application Press 0 and then APPLICATION to call up the previous application Press one of the CD keys to call up an application previously assigned to that key B2157 10 Release 2 0 2 3 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 31: ...y Parameters are in a loop i e you continue to the next parameter in turn when you press the ENTER key 4 Some parameters contain options Press to select your desired option Options are in a loop i e you continue onto the next option in turn when you press the O key 5 Press ENTER to exit the option loop and confirm the selection and move to the next parameter display 6 When you have set all the par...

Page 32: ...Section 2 3 page 2 3 2 Press 0 and then APPLICATION The following is an example of the display shown Use to select Mn number COPY APPLIC TO M1 2 SCAN 3 Press 0 to select the desired number You can return to standby by pressing CD 4 Press ENTER to confirm 5 Check the application is saved to the CD The following is an example of the display shown Wavelength Reading 250run 0 0000ABS 0 Number 1 SCAN A...

Page 33: ...ng the numeric keys 3 Press ENTER to confirm 4 Wait until the instruments sets the new wavelength or 1 Type the required wavelength 2 Press Coro x The following display is shown WAVELENGTH 500 Onm Entered value shown here ENTER 3 Wait until the instruments sets the new wavelength The new wavelength is now set and you can continue with your analysis 2 6 B2157 10 Release 2 0 Artisan Technology Group...

Page 34: ...ixed wavelength measurements an autozero is performed Performing an autozero in standby does not affect the autozero in the application Background correction sets the baseline to 0 A 100 T etc over a preselected wavelength range When you press AuTozERo at the start of a run in a scan application a background correction is performed Note You must perform autozero at the start of an application and ...

Page 35: ...s refer to Section 2 4 page 2 4 and list Chapter 3 page 3 1 4 Press RuNisrop to start the application The following is an example of the display shown SCAN SMPL 1 RUN STOP OR AUTOZERO 5 If you require autozero press AuTozERo if not then proceed to step 6 You must perform an autozero at the start of a run and at regular intervals during the analysis run 6 Place the sample in the sample holder 7 Clo...

Page 36: ... Press GoTo x and select the required wavelength refer to Section 2 6 page 2 6 3 Place blank solution in the cell holder or use air as blank 4 Close the sample compartment cover 5 Press AUTOZERO 6 Place the sample in the sample holder 7 Close the sample compartment cover 8 Press PRINT The absorbance or T reading and wavelength is then printed out To change from absorbance to T use the Timedrive ap...

Page 37: ... on the top line of the display Press0 then PRINT to print out the parameters of the actual application Press 0 then PRINT to print out a directory of the applications available Press then PRINT to print out the help message for the actual application Press 0 then PRINT for a line feed Press O then PRINT for a form feed Presss then PRINT to print out the cell holder temperature shown on the displa...

Page 38: ...s ENTER to confirm and move to next parameter 5 Type in the date using the numeric keys year month day e g 930509 6 Press ENTER to confirm and move to next parameter 7 Press 0 to select the day only with realtime clock e g Monday Tuesday etc 8 Press ENTER to confirm and move to next parameter 9 Type in the time using the numeric keys hours minutes 24 hour clock e g 0955 1326 10 Press ENTER to conf...

Page 39: ...te are set in the realtime clock 2 Call up WAKEUP application 901 refer to Section 2 3 page 2 3 3 Press ENTER DATE 000000 ENTER 4 Type in the date you wish to use the WAKEUP function using the numeric keys year month day e g 930509 5 Press ENTER to confirm and move to next parameter TIME 0000 ENTER 6 Type in the time you wish the lamps to switch on using the numeric keys hours minutes 24 hour cloc...

Page 40: ... to next standby and return to Press APPLICATION to exit the wakeup application without changing any parameters 12 Press RUNisTOP to start the wakeup application Both lamps go off e g WAKE UP AT 930509 0655 Date Time year month day hours minutes 13 Leave the power switch switched on To exit the wakeup application press RUN stop again and the display returns to standby Both lamps go on 82157 10 Rel...

Page 41: ...OFF The lifetime of the deuterium lamp will be markedly reduced if it is switched on and off frequently 3 Press ENTER to confirm and move to next parameter LAMP VIS ON TO SELECT ENTER 4 Use 0 to select Vis lamp ON or OFF 5 Press ENTER to confirm and move to next parameter 6 Press RUNisTOP to activate The selected lamp goes out and the instrument returns automatically to standby Press APPLICATION t...

Page 42: ...signed to the 0 keys This serves as a reminder of the default applications Standard Overlay 0 co 0 0 0 0 S ENTER 1 J There is also a Lambda 11 Bio blank overlay on which you can write the applications you have assigned to the Mn keys Use a marker with ink that can be erased by wiping with a soft cloth moistened with alcohol 82157 10 Release 2 0 2 15 Artisan Technology Group Quality Instrumentation...

Page 43: ...2 16 82157 10 Release 2 0 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 44: ...Applications and Parameters Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 45: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 46: ... nm FACTOR 1 0 RESPONSE 1 s LAMP UV VIS CYCLES 1 CYCLE TIME 0 04 min GRAPHICS PLOT YES ORD MAX 1 000 ABS ORD MIN 0 000 ABS SCALE 20 mm min PRINT DATA NO 2 Scan Scans a spectrum ORDINATE MODE ABS WAV MAX 900 0 nm WAV MIN 200 0 nm SPEED 960 nm min SMOOTH 0 nm LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT YES ORD MAX 1 000 ABS ORD MIN 0 000 ABS SCALE 50 0 nm cm OVERLAY NO PRINT DATA YES THRE...

Page 47: ... 0 CUR FIT LINEAR FACTOR 1 0 RESPONSE 1 s LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min PRINT DATA YES PLOT REFS NO PRINT REFS NO 5 Calibration Concentration Quantitative analysis measurement after calibration using up to 8 references Different calibration curve fitting techniques available MODE ABS WAV 1 500 0 nm OF REFERENCES 3 CONC UNIT C REF 1 1 0 C REF 2 2 0 C REF 3 3 0 C REFERENCES NEW VALUE 1 0 ...

Page 48: ... REF 2 2 0 C REFERENCES NEW VALUE 1 0 1 VALUE 2 0 2 CUR FIT LINEAR FACTOR 1 0 RESPONSE 1 s LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min PRINT DATA YES PLOT REFS NO PRINT REFS YES 8 Three Reference Concentration Quantitative analysis using 3 references for calibration Different calibration curve fitting techniques available MODE ABS WAV 1 500 0 nm OF REFERENCES 3 CONC UNIT C REF 1 1 0 C REF 2 2 0 C REF...

Page 49: ...spectrum fast scan speed ORDINATE MODE ABS WAV MAX 900 0 nm WAV MIN 200 0 nm SPEED 2880 nm min SMOOTH 0 nm LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT YES ORD MAX 1 000 ABS ORD MIN 0 000 ABS SCALE 50 0 nm cm OVERLAY NO PRINT DATA NO 11 Absorbance Scan Scans absorbance spectra ORDINATE MODE ABS WAV MAX 900 0 nm WAV MIN 200 0 nm SPEED 960 nm min SMOOTH 0 nm LAMP UV VIS CYCLES 1 CYCLE TIME...

Page 50: ...m LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT YES ORD MAX 1 0 ABS ORD MIN 0 000 ABS SCALE 20 0 nm cm OVERLAY NO PRINT DATA YES THRESHOLD 0 1 ABS 14 Vis Scan Scans absorbance spectra between 900 nm and 400 nm ORDINATE MODE ABS WAV MAX 900 0 nm WAV MIN 400 0 nm SPEED 960 nm min SMOOTH 0 nm LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT YES ORD MAX 1 000 ABS ORD MIN 0 000 ABS SCALE...

Page 51: ...HOLD 0 1 ABS 16 Cycle Wavelength Successive measurement of one sample at different Program up to 8 wavelengths Measures changes in sample absorption at different wavelengths over a period of time ORDINATE MODE ABS WAVELENGTHS 1 WAV 1 260 0 nm FACTOR 1 1 0 RESPONSE 1 s LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT NO PRINT DATA YES Parameters in bold can be changed the others cannot be cha...

Page 52: ...INT DATA YES 18 Difference Difference of absorbance readings of wavelength pairs One wavelength pair may be entered ORDINATE MODE DIF CONC UNIT DIF WAVELENGTHS 2 WAV 1 360 0 nm WAV 2 418 5 nm FACTOR 1 1 0 FACTOR 2 1 0 RESPONSE 1 s LAMP UV VIS CYCLES 1 CYCLE TIME 0 01 min GRAPHICS PLOT NO PRINT DATA YES Parameters in bold can be changed the others cannot be changed B2157 10 Release 2 0 3 7 Artisan ...

Page 53: ...when the Peltier accessory is installed PELTIER OFF TEMPERATURE 25 0 C CALIB MODE NO 906 Printer Config To configure the instrument for the type of printer used Options for printer type are AUTO INTERNAL EPSON LQ EPSON EX FX PRINTER ON YES PRINTER AUTO GAP 4 COLOUR ON YES PLOT HEADER YES 920 Peltier Calib Enter target temperature for Peltier thermostatted cell holder This application only shows wh...

Page 54: ...on on or off Used with the sipper accessory CALIB MODE NO INTERN EXTERN Calibration Mode to select Perkin Elmer INTERNAL temperature sensor or other EXTERNAL temperature 1 sensor or switch off NO CALIB MODE Shows only in Peltier calib application CALIB TEMP 10 0 C to 55 0 C Calibration Temperature This temperature is measured with an external temperature sensor Refer to Appendix A1 2 2 page A0 4 S...

Page 55: ...r printer or plotter is connected CONC UNIT I C g L mg L mg mL mg dL µg µg mL mol mmol nmol pmol ppm ppb RAT DIF Concentration Unit defines the concentration unit used for the run C is any concentration unit g L is gram per liter mg L is milligram per liter mg mL is milligram per milliliter mg dL is milligram per deciliter µg is microgram tg mL is microgram per milliliter mol is mole mmol is milli...

Page 56: ...s an intercept on the measured value axis to compensate for background interferences CYCLES 1 to 99 Sets the number of times the sample will be scanned or measured CYCLE TIME 0 002 to 999 99 The time between the start of one cycle to the start of the next DAY MONDAY to SUNDAY Sets the day only with realtime clock DATE YYMMDD Sets the date in numerals Year Month Date FACTOR GAP or 0 00001 to 9999 9...

Page 57: ...dinate mode in which the measurements are made ABS is absorbance T is transmittance CONC is concentration units D1 is first derivative D2 is second derivative D3 is third derivative D4 is forth derivative RAT is ratio of absorbances DIF is difference of absorbances ORDINATE MODE ABS T CONC Dl D2 D3 D4 RAT DIE OVERLAY YES NO Prints spectra from the same batch onto the same graphics plot when activa...

Page 58: ...nts are made The number 1 is shown for the first reference solution 2 for the second 3 for the third etc OF REFERENCES 1 to 8 You can enter the number of reference solutions RESPONSE 1s Response time defined as the time a signal requires to reach 98 of full scale deflection after a jumpwise change This function suppresses noise SAMPLE TIME 0 1 to 99 9 Time min during which the sample is aspirated ...

Page 59: ...e Option Description SPEED 30 240 960 2880 nm min Select the scan speed With slow scan speed in derivative mode it may take up to a minute before the instrument starts a scan This is to allow the motors to move the filters etc to the correct position STIRRER ON OFF Turns the stirrer on or off Used with the 13 cell changer TEMPERATURE 15 0 c to 45 0 C To enter the temperature of the Peltier cell ho...

Page 60: ...to select WI DELTA ABS Correction for an offset baseline by measuring at two wavelengths Measured value Av1 A 2 Wl W2 X 3 WL ANLYS Correction for a sloping baseline by measuring at three wavelengths A Measured value Am A A w w3 A W2 W3 K3 W3 W1 W2 82157 10 Release 3 0 3 15 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 61: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 62: ...Error Messages Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 63: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 64: ...de leading up to the error This error is shown when the instrument operating software crashes A full reset is then automatically carried out After the instrument is reset one of the following messages is shown on the second line of the display BATTERY LOW TIMER FAIL RS232 IRQ FAIL TIMER IRQ FAIL make a note of this message Press the APPLICATION key to continue after the system error has been displ...

Page 65: ...teps you made leading up to this message Press the APPLICATION key to continue after this error has been displayed If you cannot continue call your Perkin Elmer office and inform them of the error and the steps you made leading up to the error This error is shown after changing the instrument software or after a full reset All the saved applications are deleted Make a note of the steps you made le...

Page 66: ...ergy is detected NO ENERGY Check The sample compartment that nothing is blocking the beam The lamps for loose connection or lamp burnt out For defective detector ERROR This error is shown when not enough energy is received from NO ENERGY UV LAMP the UV lamp Check The sample compartment that nothing is blocking the beam The lamps loose connection lamp burnt out For defective detector ERROR NO ENERG...

Page 67: ...rences non linearity of the references is so or Change Curve Fit Algorithm great that you cannot fit a curve to them using the present curve fit algorithm Check that the references are prepared correctly or try a different curve fit Two Different Solutions with same ABS absorbance Value Change Curve Fit Algorithm No Peaks Detected Change Threshold Value This message is printed when two samples of ...

Page 68: ...Help Messages Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 69: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 70: ...e at different up to 8 wavelengths 4 Factor Concentration Quantitative analysis without calibration Absorbance at specific wavelength is multiplied by a factor to give concentration of analyte 5 Calibration Concentration Quantitative analysis Calibration using up to 8 references Different calibration curve fitting techniques available 6 One Reference Concentration Quantitative analysis using one r...

Page 71: ...nce spectra 12 Transmittance Scan Scans transmittance spectra 13 UV Scan Scans absorbance spectra between 400 nm and 200 nm 14 VIS Scan Scans absorbance spectra between 900 nm and 400 nm 15 Repetitive Scan Scans the same sample repetitively 16 Cycle Wavelength Program Successive measurement of one sample at different up to 8 wavelengths Measures changes in sample absorption at different wavelength...

Page 72: ...ay 902 Lamp Configuration To switch off the lamp not in use 903 Peltier To enter the desired temperature for the Peltier cell holder 920 Peltier Calib To enter the desired temperature for the Peltier cell holder and compensate for temperature differences between the Peltier element and the measurement cell 82157 10 Release 2 0 5 3 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 ...

Page 73: ...5 4 82157 10 Release 2 0 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 74: ...Appendix Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 75: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 76: ...acturing site If you order this accessory PCB at a later date field installation should only be performed by your Perkin Elmer service engineer or similarly qualified and authorized person We strongly recommend that you do not attempt to install this PCB yourself On the following pages is given information specific to using the accessory with the Lambda 11 spectrometer Additional information is gi...

Page 77: ...AL for manual operations e g with single cell holders or with Peltier single cell holder CELL for operations with cell changers e g with the five six eight nine Peltier and thirteen cell changers The instrument automatically recognizes which cell changer SIPPER for operations with sippers The instrument automatically recognizes which sipper Al 2 82157 10 Release 3 0 Artisan Technology Group Qualit...

Page 78: ... ENTER 4 e g Set required temperature TEMPERATURE 25 0 C Last confirmed tempera ture ENTER 26 0 Selected temperature 5 Press RuNisTop to start the application Allow 10 minutes for the temperature to equilibrate 6 When the cell holder temperature has reached equilibrium press RUNisroP to return to the standby display The Peltier temperature control continues to function You are now ready to start a...

Page 79: ...equired temperature e g TEMPERATURE 2 5 0 C I Last confirmed tempera ture ENTER 2 6 0 Selected temperature 5 Press ENTER 6 Set calib e g mode to NO CALIB MODE NO TO SELECT ENTER 7 Press RUNisTOP to start the application Allow 10 minutes for the temperature to equilibrate When EXTERN check temperature at your sensor see step 10 8 Press RuNisroa 9 Then CALIB MODE press ENTER repeatedly until the par...

Page 80: ...r reading 13 Enter the temperature reading from the external temperature sensor 14 Press RuNisToP to start the application The following display appears e g Wait until temperature equilibrium is reached SPL temperature at the sample cell holder OPT temperature at the Perkin Elmer sensor only when connected 15 When the cell holder temperature has reached equilibrium press RUNisroP to return to the ...

Page 81: ...angers Appendix 1 A 1 2 3 Cell Changers With the cell changer accessories an extra parameter appears e g You must enter the location in the cell changer of the cell or cells to be measured A1 6 82157 10 Release 2 0 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 82: ...Index Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 83: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 84: ... Calib Mode 3 9 A1 4 Temp 3 9 A1 5 Calibration concentration 3 2 Cell Changers A1 6 Location A1 6 Celli 7 3 10 Ce115 3 9 Ce116 3 9 Ce118 3 9 Ce118 13 3 10 Ce119 3 10 Clock 24 hour 2 11 2 12 internal 2 11 realtime 2 11 2 12 Color 3 10 Conc unit 3 10 Concentration variable 3 4 Controls 1 1 Cur fit 3 11 Cycle wavelength program 3 6 Cycles 3 11 Cycletime 3 11 B2157 10 Release 3 0 In 1 Artisan Technolo...

Page 85: ...t 3 11 H Help messages 5 1 5 4 Keyboard 1 2 Keys 1 3 application 1 3 assigning the M 2 5 autozero 1 3 CE 1 3 2 5 enter 1 3 goto 1 3 2 6 M 1 3 2 3 2 15 minus 1 3 numeric 1 3 point 1 3 print 1 3 2 10 run stop 1 3 L Lamp 3 12 configuration 2 14 3 8 warm up 2 2 M Measurement range absorbance 1 2 transmittance 1 2 Mode 3 12 In 2 82157 10 Release 3 0 Artisan Technology Group Quality Instrumentation Guar...

Page 86: ...uration 3 8 Print data 3 13 Print refs 3 13 R Range 3 9 See also Measurement range Ref 3 13 Refs 3 13 of 3 13 Repetitive scan 3 6 Response 3 13 S Safety chemicals S 5 electricity fuses S 4 radio frequency S 6 UV radiation S 6 Safety Information S 1 Sample quick run 2 9 running a 2 8 Sample Time 3 13 Scale 3 13 Scan 3 1 autozero in 2 7 Shutdown 2 2 Smooth 3 13 Speed 3 14 Standby autozero 2 7 return...

Page 87: ...eference concentration 3 3 Threshold 3 14 Timedrive 3 1 Transmittance scan 3 5 Two reference concentration 3 3 U User Documentation P 1 conventions P 2 Installation Maintenance and System Description P 1 Operation and Parameter Description P 1 Quick Reference P 1 UV scan 3 5 V Value 3 14 Vis scan 3 5 In 4 B2157 10 Release 3 0 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURC...

Page 88: ... supplies through the Supplies Catalog for Ultraviolet Visible and Fluorescence Spectroscopy and Polarimetry To place an order request a free catalog or ask for information If you are located within the U S call toll free 1 800 762 4002 8 a m to 8 p m EST Your order will be shipped promptly usually within 24 hours If you are located outside of the U S call your local Perkin Elmer sales office Arti...

Page 89: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 90: ...0 17 61 D 88647 Überlingen Bundesrepublik Deutschland Tel 07551 810 Perkin Elmer Ltd Post Office Lane Beaconsfield Bucks HP9 1QA England Tel Beaconsfield 0494 676161 ISO 9001 ALL ANALYTICAL INSTRUMENTS AND SYSTEMS MANUFACTURED BY PERKIN ELMER ARE CERI IVIED UNDER THE QUALITY REQUIREMENTS OF ISO 9001 CFHTI FIII Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg ...

Page 91: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 92: ...l service in house repair center WE BUY USED EQUIPMENT Sell your excess underutilized and idle used equipment We also offer credit for buy backs and trade ins www artisantg com WeBuyEquipment REMOTE INSPECTION Remotely inspect equipment before purchasing with our interactive website at www instraview com LOOKING FOR MORE INFORMATION Visit us on the web at www artisantg com for more information on ...

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