Milkotester MASTER MINI User Information Download Page 27

ULTRASONIC PORTABLE MILK ANALYZER 

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Appendix Freezing point determination 

 

1. Methods for determination. 
 
The milk analyzer determines the freezing point of each sample and the 
quantity of added water. The milk analyser does not measure the 
freezing point, but calculates it from the components it depends on. The 
basic components in the milk are water, solids, lactose, FAT, proteins, 
minerals (salts) and acids. The freezing point depends only on the 
diluted in the milk components and quantity of the solvent (in the milk it 
is water). The ultrasonic technology allows direct measurement of FAT, 
proteins, l salts (the soluble components, only influencing the 
freezing point), and the quantity of the solvent in % is determined by 100 
% – total solids %, total solids = lactose % + FAT % + proteins % + salts 
% + acids %.  
Without understanding the meaning of the freezing point – determined or 
shown from the milk analyzer added water result easily may lead to a 
mistake for the value of this parameter. 
 
2. The basic freezing point. 
 
Milk freezes at lower temperature than water. The average freezing point 
of the raw milk in the most regions is at about -0,540

С

. The average 

reading for your region is called “basic” freezing point. 
The freezing point of milk is a “physiological constant”. This does not 
mean that it will not vary. In fact feed, breed, season, time of lactation, 
climate, whether the sample is taken at the beginning, middle or end of 
lactation – all these factors will have an effect on the freezing point of the 
individual sample. This means that there is an average value of all these 
numbers. The more samples used in obtaining this average, the more 
reliable it is as a base. Or the basic freezing point is an average of 
freezing points of milk, taken from many cows. When a laboratory 
checks a producer, it is only comparing the average of the producer’s 
cows against a larger area average. 
The Health authorities establish the basic freezing point or agriculture 
departments in some regions, sometimes by universities, separate dairy 
producers, or their associations. Frequently, tolerances have been 
established on top of a basic freezing point to allow some variations in 
the milk as well as device or operator variations. 
Without mentioning the basic freezing point, the Association of Official 
Analytical Chemists now recommends an upper limit freezing point at -
0,525

C (2,326 standard deviations above the most recently determined 

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Summary of Contents for MASTER MINI

Page 1: ...ing device Model MASTER MINI Fat Solids Non Fat SNF Protein Lactose Water content Temperature C Freezing point Solids Density THE INFORMATION CONTAINED IN THIS MANUAL IS A SUBJECT TO CHANGE WITHOUT NO...

Page 2: ...a leveled and stable surface If it falls or is severely shocked its functional systems may be damaged When plugging the device into the electrical outlet put away the power cord so it does not stay in...

Page 3: ...Preparing the device 9 4 2 Measuring samples 10 4 3 Making correction and calibration 11 4 3 1 Correction 13 4 3 1 Calibration 14 4 4 Settings and options 18 4 5 Connecting to printer 20 5 Cleaning an...

Page 4: ...ntioned types of milk The device has a compact design with a robust structure and a user friendly interface MASTER MINI can analyze three types of milk defined by user The measurement speed is 40 45 s...

Page 5: ...e up view IN THIS CHAPTER Front panel Display Back panel 2 1 Front panel 8 7 9 6 5 1 4 3 2 1 Intake pipette 2 Start knob 3 Operation indicator 4 Arrow DOWN button 5 Arrow UP button 6 ENTER button 7 EX...

Page 6: ...ULTRASONIC PORTABLE MILK ANALYZER www milkotester com 2 2 Back panel 3 1 2 1 Serial port to printer or PC 2 Power in 12V 3 Power switch 5...

Page 7: ...es only once and do not return it to the vessel Samples can be kept for a maximum of 2 days if they are stored at a temperature not exceeding 5 Milk stirring It is a very important condition for recei...

Page 8: ...ermally treated When examining samples taken immediately before analyses and shortly stored the milk is poured several times from vessel to vessel in order to distribute the fat content uniformly To a...

Page 9: ...d stable surface Caution Any sources of hot or cold air can influence the accuracy of the measurements 2 Connect the device to 12V DC power source 220V AC to 12V DC adaptor or 12V DC electrical lighte...

Page 10: ...ou can choose among three types of milk at a time When you choose the desired type of milk you use the UP and DOWN arrow buttons and then turn the knob clockwise until the knob indicator comes to the...

Page 11: ...start measuring anew by turning the knob to the red point By choosing the EXIT button you can start from the very beginning and choose to analyze another type of milk To access the menu press the ENT...

Page 12: ...reduce this inaccuracy due to water in the system please refer to chapter Cleaning and Maintenance section Thorough Cleaning 4 3 MAKING CORRECTIONS AND CALLIBRATION In the process of work with the ana...

Page 13: ...ween the values of the parameter from the reference sample and measured with the analyser Make analyses of the difference received If the received differences are relatively constant value for samples...

Page 14: ...rows and press ENTER to select Correction Calibration Back up or Restore Correction Calibration Back up Restore If you choose correction and press ENTER then use the up and down arrows and press ENTER...

Page 15: ...4 3 2 Calibration MENU Mode Calibration In order to perform calibration of the device for a certain type of milk for example cow milk You need two samples of milk with known values of their parameters...

Page 16: ...me procedure to enter the second and third figure After confirmation of the last figure the cursor goes to the next parameter for entering new values mind that there are 2 two pages of components thus...

Page 17: ...ing the knob counter clockwise to the black point the following message will appear on the display Put Sample High Milk 2 5 and turn to red point Follow the procedure until the 5th measurement After p...

Page 18: ...end of the 5th measurement the calibration procedure is complete Please note Before each sample measurement stir the milk by pouring it from one vessel to another The temperature of the samples should...

Page 19: ...tem info Choose Options and press ENTER System Info Language Time and Date Choose System info Language or Time and Date and press ENTER MILKOTESTER Model MASTER MINI Ver x xx SN XXXXXX MENU Options La...

Page 20: ...wing text appears on the display Set Fr Point 0 520 Press ENTER To Set Use Up and Down arrows to enter the new value and Press Enter to confirm After dialing the last symbol press ENTER to confirm the...

Page 21: ...to work only with printers supplied by Milkotester Ltd We warn you that the unit is not set to work with other types of printers To connect MILKOTESTER MASTER MINI to the serial printer follow the ste...

Page 22: ...s or a considerable number of measurements have been performed the device begins to issue continuing beep sounds At the same time the message Cleaning needed appears on the display Please carry out th...

Page 23: ...to be well stirred up and can remain good for unlimited time After flushing with the solution flush the system with clean water twice by repeating steps 1 and 2 from routine cleaning 5 3 Weekly cleani...

Page 24: ...e Check that there are no air bubbles in the sample Check if after starting measurement milk sample in the sample holder decreases In other case there is damage in the suction system Check if the end...

Page 25: ...rotein Lactose Water content Temperature C Freezing point Solids Density 2 Ranges of measurement Fat from 0 00 to 20 SNF from 3 to 15 Density from 1015 to 10 40 kg m3 Proteins from 2 to 7 Lactose from...

Page 26: ...3 Accuracy Fat 0 1 SNF 0 1 Density 0 3 kg m3 Proteins 0 1 Lactose 0 1 ADDED Water 3 0 Sample Temperature 1o C Freezing point 0 002 o C Solids 0 05 Air temperature from 10 o C to 40 o C Relative humid...

Page 27: ...st regions is at about 0 540 The average reading for your region is called basic freezing point The freezing point of milk is a physiological constant This does not mean that it will not vary In fact...

Page 28: ...es obtained as specified in the METHODS After determination the freezing point of your sample via the milk analyzer the added water is calculated using the following formula 100 int int int Base Calc...

Page 29: ...ct basic freezing point in the device The device s results for added water may give information about doubt of added water in the milk and the exact value of this added water may be determined after a...

Page 30: ...Botev St 4470 Belovo BULGARIA Milkotester MASTER MINI Guarantee period is 1 one year after purchasing date Improper handling transport and storage will invalidate the guarantee Guarantee is void if w...

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