Koehler K44100 Operation And Instruction Manual Download Page 6

K441XX Automatic Non-Woods Metal Noack Evaporative Apparatus  

Operation and Instruction Manual 

 

K441XX-Manual 

- 5 - 

3 Getting 

Started 

 

3.1 Packing 

List

 

 

  Automatic Non-Woods Metal Noack Evaporative 

Apparatus 

  Evaporation Crucible for Procedure B 

  PT100 Probe for Crucible 

  Test Ball (10) 

  Nozzle Cleaner  

 Crucible 

Holder 

 Protective 

Gloves 

 Hook 

Wrench 

 Pliers 

 Operation 

Software 

 

3.2 Unpacking 

 

Carefully unpack and place the instrument and 
accessories in a secure location. Inspect the unit for 
damage. If any damage is found, keep all packing 
materials and immediately report the damage to the 
carrier. We will assist you with your claim, if 
requested. When submitting a claim for shipping 
damage, request that the carrier inspect the shipping 
container and equipment. Do not return goods to 
Koehler without written authorization. 
 

3.3 Installation 

 

Equipment Placement:

 Place the instrument on a 

firm surface in a secure area.  

 

1.  Connect the cord cable from the analyzer to 

a network that conforms to the electric safety 
specifications 

 
2. Set up glassware as described in the 

procedure section 

 
3.  Turn ON the analyzer 

 

3.4  Additional Accessories Required for 

Running Tests 

 

Part Number 

Description 

K44100-1 

Glassware Accessory Set 

Includes:  

2L Glass Bottle (2) 
Rubber Stopper (4) 
Glass Delivery Tubes 
Silicon Connection Tubing 

K44100-2 

Stand for glass bottles w/ 
inclined manometer, 0-50 
mmH

2

K44100-3 

Noack Reference Oil, RL223,1L 

KLA-DB-KIT 

Set of Connectors and Cables  

KLA-PT100-CAL 
 

Calibration Decade Box – 
PT100 Simulator  

 

3.5  Optional Accessories Available 

 

Part Number 

Description 

K44100-SFW 

Noack Evaluation Software 

K44100-14 

Noack Reference Oil, RL208, 1L 

 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 

Summary of Contents for K44100

Page 1: ...mia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis Instrumen...

Page 2: ...1...

Page 3: ...Packing List 5 3 2 Unpacking 5 3 3 Installation 5 3 4 Additional Accessories Required for Running Tests 5 3 5 Optional Accessories Available 5 4 Descriptions 6 4 1 Piping Diagram 6 4 2 Instrument Cont...

Page 4: ...s manual should also be used in conjunction with applicable published laboratory procedures Information on these procedures is given in section 1 2 1 1 Koehler s Commitment to Our Customers Providing...

Page 5: ...to access the analyzer STAY ALERT Do not operate this unit while under the influence of medication alcohol or drugs Equipment Modifications and Replacement Parts Any modification or alteration of thi...

Page 6: ...shipping container and equipment Do not return goods to Koehler without written authorization 3 3 Installation Equipment Placement Place the instrument on a firm surface in a secure area 1 Connect th...

Page 7: ...6 4 Descriptions 4 1 Piping Diagram Figure 1 Piping Diagram...

Page 8: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 7 4 2 Instrument Controls and Connections Figure 2 Top Front Left Side View...

Page 9: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 8 Figure 3 Top Left Back Side View Figure 4 Analyzer Complete with Assembled Glassware Set...

Page 10: ...bration date Figure 7 Calibration Screen 4 On the left side of the screen a graph shows the calibration curve along with the selected probe s value in both C and volts 5 On the right side of the scree...

Page 11: ...emperature Control via PT100 probe in the Heating Block Bath Method B Temperature Control via PT100 probe in the Crucible 4 Select the set point temperature for the test based on the selected method S...

Page 12: ...egulate the aspiration vacuum to 2 mbar by slowly closing the bleed valve halfway and regulating the vacuum regulator on the analyzer s side in order to reach 20 0 2mm on the inclined manometer 2mbar...

Page 13: ...for 30 minutes NOTE WHILE REMOVING THE CRUCIBLE AND PLACING IT IN THE WATER BATH MAKE SURE THE SAMPLE DOES NOT SPLASH THE CRUCIBLE S COVER 7 After 30 minutes carefully dry the outside of the crucible...

Page 14: ...e operator to select the sample o Press the Load Analysis Button in between the two arrows to view the analysis Figure 13 Results Browser Main Screen If the final weight has not been introduced a ques...

Page 15: ...hler Representative as each printer has different characteristics and specific drivers Touching the Show Details button causes the analysis to reload and the data to be displayed second by second on t...

Page 16: ...test is run clean the Woullf bottles and pipes Each time a test is run clean the heating jacket Periodically clean the vacuum filter 7 2 Replacement Parts Some instrument parts may need to be replaced...

Page 17: ...rize the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product is the...

Page 18: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 17 Notes...

Page 19: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 18 Notes...

Page 20: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 19 Notes...

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