Koehler K44100 Operation And Instruction Manual Download Page 5

K441XX Automatic Non-Woods Metal Noack Evaporative Apparatus  

Operation and Instruction Manual 

 

K441XX-Manual 

- 4 - 

1.3 Instrument 

Specifications 

 

Model: 

K44100 
K44190 

Electrical 

Requirements:  

 
115V ±15%, 60Hz 
220V ±15%, 50/60Hz  

Test Temperature 

Range: 

 
225°C to 275°C 

Measurable 

Temperature Range: 

 
0°C to 320°C 

Temperature 

Resolution: 

 
0.01°C 

Temperature 

Accuracy: 

 
± 0.2°C 

Maximum Ambient 

Temperature: 

 
35°C 

Relative Humidity: 

80% 

Heating Power: 

420W 

Repeatability / 

Reproducibility: 

 
According to ASTM 
D5800 or better 

Dimensions: 

(L x W x H, in.(cm)) 

15.75 x 17.72 x 17.72  
(40 x 45 x 45) 

Net Weight:  

48.5 lbs (22kg) 

 
 

2  Safety Information and Warnings 

 

Safety Considerations. 

The use of this 

equipment may involve 

hazardous 

materials and 

operations. This manual does not purport to address 
all of the safety problems associated with the use of 
this equipment. It is the responsibility of any user of 
this equipment to investigate, research, and 
establish appropriate safety and health practices and 
determine the applicability of regulatory limitations 
prior to use. 
 

 

DO NOT

 allow unauthorized persons to access 

the analyzer. 

 

 

STAY ALERT! 

Do not operate this unit while 

under the influence of medication, alcohol, or 
drugs. 

 

Equipment Modifications and Replacement 
Parts: 

Any modification or alteration of this 

equipment from that of factory specifications is not 
recommended and voids the manufacturer warranty, 
product safety, performance specifications, and/or 
certifications whether specified or implied, and may 
result in personal injury and/or property loss. 

Replacement parts must be O.E.M. exact 
replacement equipment. 

 

Chemical Reagents Information: 

Chemicals and 

reagents used in performing the test may exhibit 
potential hazards. Any user must be familiarized 
with the possible dangers before use. We also 
recommend consulting the Material Data and 
Safety Sheet (MSDS) on each chemical reagent 
for additional information. MSDS information can 
be easily located on the internet at 
http://siri.uvm.edu or http://www.sigma-
aldrich.com. 
 

Disposal of the Instrument 

Please note the crossed out symbol of a trash can 
on the instrument (please see symbol below).  This 
indicates that the product must be disposed of 
separate from waste at the end of its operational 
life. The user that intends to dispose of this 
equipment must contact the manufacturer to 
ensure proper disposal. 

 

 

 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 

Summary of Contents for K44100

Page 1: ...mia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis Instrumen...

Page 2: ...1...

Page 3: ...Packing List 5 3 2 Unpacking 5 3 3 Installation 5 3 4 Additional Accessories Required for Running Tests 5 3 5 Optional Accessories Available 5 4 Descriptions 6 4 1 Piping Diagram 6 4 2 Instrument Cont...

Page 4: ...s manual should also be used in conjunction with applicable published laboratory procedures Information on these procedures is given in section 1 2 1 1 Koehler s Commitment to Our Customers Providing...

Page 5: ...to access the analyzer STAY ALERT Do not operate this unit while under the influence of medication alcohol or drugs Equipment Modifications and Replacement Parts Any modification or alteration of thi...

Page 6: ...shipping container and equipment Do not return goods to Koehler without written authorization 3 3 Installation Equipment Placement Place the instrument on a firm surface in a secure area 1 Connect th...

Page 7: ...6 4 Descriptions 4 1 Piping Diagram Figure 1 Piping Diagram...

Page 8: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 7 4 2 Instrument Controls and Connections Figure 2 Top Front Left Side View...

Page 9: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 8 Figure 3 Top Left Back Side View Figure 4 Analyzer Complete with Assembled Glassware Set...

Page 10: ...bration date Figure 7 Calibration Screen 4 On the left side of the screen a graph shows the calibration curve along with the selected probe s value in both C and volts 5 On the right side of the scree...

Page 11: ...emperature Control via PT100 probe in the Heating Block Bath Method B Temperature Control via PT100 probe in the Crucible 4 Select the set point temperature for the test based on the selected method S...

Page 12: ...egulate the aspiration vacuum to 2 mbar by slowly closing the bleed valve halfway and regulating the vacuum regulator on the analyzer s side in order to reach 20 0 2mm on the inclined manometer 2mbar...

Page 13: ...for 30 minutes NOTE WHILE REMOVING THE CRUCIBLE AND PLACING IT IN THE WATER BATH MAKE SURE THE SAMPLE DOES NOT SPLASH THE CRUCIBLE S COVER 7 After 30 minutes carefully dry the outside of the crucible...

Page 14: ...e operator to select the sample o Press the Load Analysis Button in between the two arrows to view the analysis Figure 13 Results Browser Main Screen If the final weight has not been introduced a ques...

Page 15: ...hler Representative as each printer has different characteristics and specific drivers Touching the Show Details button causes the analysis to reload and the data to be displayed second by second on t...

Page 16: ...test is run clean the Woullf bottles and pipes Each time a test is run clean the heating jacket Periodically clean the vacuum filter 7 2 Replacement Parts Some instrument parts may need to be replaced...

Page 17: ...rize the return of the product to the factory The sole responsibility of Koehler Instrument Company and the purchaser s exclusive remedy for any claim arising out of the purchase of any product is the...

Page 18: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 17 Notes...

Page 19: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 18 Notes...

Page 20: ...K441XX Automatic Non Woods Metal Noack Evaporative Apparatus Operation and Instruction Manual K441XX Manual 19 Notes...

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