Koehler K41100 Operation And Instruction Manual Download Page 25

 

 
 
 
 

K41100

 

5.2.1.2 Removing carbon deposits from the oven

  

 
The  outlet  at  the  base  of  the  oven  may  be  a  point  for  deposits  of 
carbon, which by accumulation could block the oven exhaust.  

To  avoid  total  blockage  of  the  oven,  it  is  preferable  to  clean  this  part  regularly, 
using the cable supplied.  

 

To do this:  

 

 With the oven cold and disconnected from the  

 

power supply, remove the condensates container.  

 Remove the insulating cover and the metal cover  

 

of the oven.  

 Pass the cable through the oven mouth and push  

 

out through the exhaust  
pipe.  

 With a backwards and forwards movement,  

 

orientating the cable in all directions, clean the pipe  

 

by removing all deposits of carbon.  

 
 


  Check  the  condition  of  the  flue  pipe  and  its  extension.  Perform  the  same  

 

operation in the case of deposits of carbon.  

5.2.2 Checking the oven temperature  

To  check  the  oven  temperature,  a  control 
thermocouple must be placed in the oven.  
For  this  purpose,  the  cover  has  a  hole  blocked  with  a  
small  stud.  This  hole  allows  inserting  a  thermo-couple  
to  monitor  and  measure  the  oven  temperature.  This  
stud  is  simply  forced  into  the  hole.  By  pushing  it  can  
be ejected.  
If the oven temperature is not satisfactory, it is 
recommended to check the calibration of the oven 
thermo-couple (see Para. Calibration).  

5.2.3 Monitoring the gas flows  

To monitor the gas flows, it vital to start a no-load test.  
Calibration  of  gas  flow  rates  must  be  performed  using  the  abacus  received  with  the 
appliance.  

 

For guidance, for a flow rate of 150 ml/min, the flow meter should be  

 

regulated at 20.62 mm and for a flow rate of 600 ml/min, at 58.20 mm.  

 Always refer to the abacus received with the appliance.  

 

 

 

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Summary of Contents for K41100

Page 1: ...nue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis I...

Page 2: ......

Page 3: ...in conformance with the applicable standards set forth in this certification Specifications ASTM D4530 This unit is tested before it leaves the factory to ensure total functionality and compliance to...

Page 4: ......

Page 5: ...nnectors 13 3 3 Starting up 14 4 USE OF THE APPLIANCE 15 4 1 Description of the temperature regulator 15 4 2 Starting a test 15 4 3 Interruption of a test 18 4 4 Alarm 19 4 4 1 Alarm during a test 19...

Page 6: ...hed 7 Disconnect the appliance from the mains power when it is not in use Never pull on the cable to disconnect it from the mains Take hold of the plug and remove it from the power socket 8 Allow the...

Page 7: ...a month in order to check satisfactory condition of pipes and their fastenings In the case of an incident that could result in damage to the appliance excess gas pressure abnormal heating of the appli...

Page 8: ...to an appliance of which the defect is the result of incorrect use connection to an unsuitable electricity supply absence of ground an act of vandalism or caused by the forces of nature thunder flood...

Page 9: ...respected scrupulously to avoid any physical injury or damage to your appliance Maintenance Supplies important information concerning the maintenance of your appliance Remark Provides useful advice f...

Page 10: ...tandard ASTM D 4530 Cooling of oven Accelerated by injection of compressed air for forty minutes Gas connections at the rear of the Instant connections dia 4 mm for appliance nitrogen and dia 8 mm for...

Page 11: ...K41100 2 3 Description of the appliance 2 3 1 Front panel 8 30...

Page 12: ...K41100 2 3 2 Rear Panel 9 30...

Page 13: ...K41100 2 3 3 Accessories I 10 30...

Page 14: ...er transport or unpacking must not be commissioned To avoid risks of condensation the appliance must be left at room temperature for several hours before it is powered on 3 2 Appliance connections Dep...

Page 15: ...nterfere with the test by modifying the flow rates and causing leaks through the hot cover of the oven From the side of the appliance take the cover handling hook and the sample vial see photo opposit...

Page 16: ...nnection of a pipe Simply push the pipe totally home in the connector The connection and leak tightness are made instantaneously 3 2 1 2 Disconnection of a pipe Press the push button on the outside of...

Page 17: ...e When the temperature regulator is powered on for three seconds it runs a series of automatic tests After each sequence the display shows the temperature measured on the upper display and displays OF...

Page 18: ...ed by the test Reminder It is vital to be familiar with the standards concerning the tests to be initiated Reminder The installing and removal of samples after the tests requires working with a hot ov...

Page 19: ...f the test Check that the oven outlet is not blocked by carbon deposits see Para Maintenance Place the vial holder in the oven using the tool supplied see photo Replace the oven cover with the tool pl...

Page 20: ...Cooling with compressed air for forty minutes Entry of nitrogen in the oven high flow rate 5 End of test Switch off heating and gas supply During the test check that the nitrogen flow rates are corre...

Page 21: ...the RUN LED goes out To put the program on hold press the key the RUN LED goes out and the HOLD LED lights up HOLD is indicated on the lower display The temperature regulator will remain in this stat...

Page 22: ...st If a test is in progress the safety device will switch the regulator to HOLD the RUN LED goes out and the HOLD LED comes on HOLD is indicated on the lower display The temperature regulator will rem...

Page 23: ...regulator to manual mode the AUTO LED goes out and the MAN LED lights up When the oven is cold the regulator reverts to wait mode In the case of an alarm it is always necessary to investigate the caus...

Page 24: ...ded running the cleaning cable through to clean off any deposits see next paragraph 5 2 General maintenance Depending on the number of analyses and the type of samples used periodic maintenance is nec...

Page 25: ...rform the same operation in the case of deposits of carbon 5 2 2 Checking the oven temperature To check the oven temperature a control thermocouple must be placed in the oven For this purpose the cove...

Page 26: ...a doubtful result it is appropriate to Check the condition of the cover after the test If leaks have occurred at that location there will be traces on the cover Also check there are no deposits on th...

Page 27: ...couple Insulating cover Glass vial 2 ml Glass vial 16 ml Pressure gauge Brass condensates container Glass condensates container Condensates container seal Flow Meter Air electro valve Nitrogen electro...

Page 28: ...K41100 8 ANNEXES 8 1 Flow meter abacus 25 30...

Page 29: ...26 30...

Page 30: ...EUROTHERM 24 08 1 2 3 4 static relay r elais statiq ue 2A L r elay N 1A 10A 1B l og ic AA AB 2 1 LA LB LC BY DATE V V 2A 2B 2C 2D 3A 3D heater chauffe temperature sensor thermocouple Tc nitr og en azo...

Page 31: ...2 50 KPa solenoid valve lectrovanne NITROGEN solenoid valve lectrovanne valve low flow vanne petit d bit flowmeter d bitm tre manometer BY DATE SIMON M 18 04 05 28 30 Furnace Four Furnace Four KOEHLE...

Page 32: ...mensions 7 Display 14 16 17 18 19 E END 17 Extension 3 12 16 22 24 F Flow 2 11 12 17 22 23 24 25 Flue 12 16 22 24 G Gas 7 Gloves 4 15 21 24 Goggles 4 15 21 H HOLD 18 19 Holder 12 16 24 Hood 4 12 15 16...

Page 33: ...1 23 Seal 21 24 Smoke 4 12 15 Stud 22 Switch 14 17 19 20 T Temperature 2 4 7 11 14 15 16 17 18 19 22 24 Test 2 3 4 11 12 14 15 16 17 18 19 20 21 22 23 Thermocouple 7 Tube 13 V Valve 16 24 Vial 7 12 16...

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