Jasco P-1010 Hardware/Function Manual Download Page 22

  

10 

Positioning holes

Temperature sensor
fixture

Setscrew

Aperture

絞り機構

8

Front panel

Cell holder

 

Figure 3.1  Sample cell unit (Top view) 

3.2.2  Cleaning the sample cell unit 

(1) For water-soluble sample 

Carefully wipe off spilt sample with gauze or the like.  Wipe off the sample completely 
with gauze wetted with water.  Finally, wipe off moisture with gauze wetted with ethyl 
alcohol and then allow the sample chamber to dry up. 

(2) For non-water-soluble sample 

Carefully wipe off spilt sample with gauze or the like.  Wipe off the sample completely 
with gauze wetted with ethyl alcohol and then allow the sample chamber to dry up. 

3.2.3  Remounting the sample cell unit 

(1) Install the sample cell unit 

1)  Fit  the  positioning  pins  in  the  sample  chamber  into  the  positioning  holes  in  the 
sample cell unit. 

2) Tighten the two setscrews to fix the sample cell to the main unit. 

Make  sure  the  beam  is  incident  on  the  center  of  the  aperture  of  the  aperture 
mechanism according to the following procedure. 

1) Turn ON the 

ʺ″

Power

ʺ″

 switch. 

2) Remove the filter for a while. 

3) Place a piece of white paper in front the cell holder and visually check if the beam 
is incident on the center of the aperture. 

4) Install the cell holder temperature sensor. 

5) Mount the filter in the original position. 

Summary of Contents for P-1010

Page 1: ...P N 0302 0411A April 1999 P 1010 1020 1030 Polarimeter Hardware Function Manual Data Station Type...

Page 2: ...the product is marked with this symbol refer to the instrument manuals to protect the instrument against damage WARNING A WARNING indicates an potentially hazardous situation which if not avoided coul...

Page 3: ...ND CURRENT RATINGS Part No 0822 0102A 2 Warning for GROUND on Figure 1 2 or 3 WARNING MAINS PLUG GROUND PIN OR GROUND TERMINAL MUST BE CONNECTED TO GROUND Part No 0822 0104A Power On Off AC Input T3 1...

Page 4: ...iRM PS AUX1 AUX2 LC Out Temp Control Analog Out Se ri a l GND GND 1 2 Figure 2 Rear panel of P 1020 iRM PS AUX1 AUX2 LC Out Temp Control Analog Out FUSE T 10A 100 120V T 5A 200 240V AC Input Power On...

Page 5: ...sample exceeds 50 the correct optical rotation may not be shown if the sample with the large optical rotation is placed in the sample chamber first In this case use the following procedure 1 Beforeha...

Page 6: ...nown sample 4 After measuring the unknown sample open the sample chamber lid replace the unknown sample with the known sample used above close the lid and measure until the optical rotation stabilizes...

Page 7: ...gnetic compatibility Generic immunity standard Part 1 Residential commercial and light industry IEC1000 4 2 Electromagnetic compatibility for industrial process measurement and control equipment Part...

Page 8: ...r experienced users Before using the instrument please read this instruction manual carefully and make sure you fully understand its contents This manual should be easily accessible to the operator at...

Page 9: ...nder atmospheric pressure of 750 1060hPa 6 Avoid strong magnetic fields and sources of high frequency The instrument may not function properly when near a strong magnetic field or high frequency sourc...

Page 10: ...ON THE USE OF JASCO SOFTWARE COPYING SOFTWARE FOR PURPOSES OTHER THAN BACKUP TRANSFER OR LICENSING OF THE RIGHT TO USE SOFTWARE TO A THIRD PARTY DISCLOSURE OF CONFIDENTIAL INFORMATION REGARDING SOFTWA...

Page 11: ...DENTS BEYOND JASCO S CONTROL INCLUDING NATURAL DISASTERS This warranty does not cover the consumable parts listed below 1 Deuterium lamp tungsten lamp xenon lamp and other light sources 2 Mirrors in t...

Page 12: ...2 Names and Functions of Each Part 5 2 1 Overview 5 2 2 Rear panel 5 2 3 Filter 8 3 Maintenance 9 3 1 Cautions in Use 9 3 2 Cleaning Sample Chamber 9 3 2 1 Dismounting the sample cell unit 9 3 2 2 Cle...

Page 13: ...nter Equipped with Centronics parallel interface Display Liquid crystal panel Language Japanese English Temperature measurement Within cell holder cell sample Temperature measurement range 0 40 C Mini...

Page 14: ...ity Data processing Edit data Statistical calculation average value standard deviation coefficient of variation Other functions Recognizes light source filter External terminal External start External...

Page 15: ...100 115 200 220 and 240 VAC 10 50 60 Hz 530 W 1 3 Hardware Structure Figure 1 1 shows a block diagram of the polarimeter Light from the light source lamp passes through slit S lens L and filter F bef...

Page 16: ...AMP Generator Ref AM P H T AMP Main AMP Servo AMP Accessory Micro Computer Servo Motor G PC RS 232C SO Light source S Slit L Lens F Filter P Polarizer M Modulator A Analyzer PM Photomultiplier tube G...

Page 17: ...mp The lamp is housed here Contains a filter for changing over wavelength Includes the cell holder light beam aperture changer and sensor for temperature measurement The aperture changer can be set at...

Page 18: ...X1 AUX2 LC Out Temp Control Analog Out GND GND 1 2 3 4 5 7 8 9 10 11 6 Figure 2 3 P 1020 rear panel P 1030 rear panel iRM PS FUSE T10A 100 120V T5A 200 240V AC Input Power On Off 50Hz 60Hz Hg Na Seria...

Page 19: ...specified fuse for the voltage is contained here Be sure to match the voltage of the power source being used Enables power to be supplied to the intelligent remote module iRM Connector for connecting...

Page 20: ...ing the left and right ends of the disk pops up the lid of the filter unit The filter must be inserted in a specified direction Insert it by noting the wavelength indication at the top of the filter a...

Page 21: ...a day s measurement turn OFF the Power switch wait for about 15 minutes for the lamp to cool down and then put on the dust cover 3 2 Cleaning Sample Chamber If sample is spilt in the sample chamber wi...

Page 22: ...etely with gauze wetted with ethyl alcohol and then allow the sample chamber to dry up 3 2 3 Remounting the sample cell unit 1 Install the sample cell unit 1 Fit the positioning pins in the sample cha...

Page 23: ...5330 0080 5330 0006 5330 0099 5332 0001 1009 0042A 1009 0043A 1009 0044A 1009 0045A 1009 0059A Sodium lamp Mercury lamp Halogen lamp The glow discharge tube Filter 589nm Filter 578nm Filter 546nm Fil...

Page 24: ...ut 30 minutes 2 Set data mode to optical rotation alpha 3 Set the parameters as follows Lamp WI or Na Wavelength filter 589 nm Integration 5 sec Sample chamber aperture 8 mm Auto meas On Auto print On...

Page 25: ...ees Degrees Degrees Li 6708 Cd 6438 50 51 55 04 50 50 55 05 0 01 0 01 Fe 4384 Fe 4376 126 5 127 2 126 7 127 2 0 12 Zn 6362 56 51 56 45 0 06 Hg 4358 128 49 128 3 0 12 Na 5893 Cu 5782 Hg 5780 Cu 5700 Hg...

Page 26: ...amp into the socket 5 Mount the lid into place 6 Turn the Power switch On and make sure that the instrument operates properly See 3 4 Performance Check for details 3 5 2 Replacing Lamp for P 1020 Repl...

Page 27: ...lamp 2 Take out the Hg lamp from its case and insert it perpendicularly into the socket by aligning the prongs of the lamp with the socket holes 3 Set the lamp selector switch on the rear of the lamp...

Page 28: ...ce the glow discharge tube in the lamp housing Use commercially available glow discharge tube FG 4P 200 volts WARNING The lamp is still very hot after turning the Power switch Off Therefore wait at le...

Page 29: ...ed type and current rating 1 Turn the power switch off and unplug the power cable from the socket 2 Insert a standard driver into the fuse holder on the rear panel Figure 3 4 Then press and turn about...

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