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Stirring Fluid Loss Manual
100031980
Revision F
20
5
Operation
This section gives detailed instructions on operating the instrument. The following
sections describe how to
•
Pre-test the Instrument
•
Load the Sample Chamber
•
Pre-heat the Sample Chamber
•
Start the Stirring Fluid Loss Test
•
End the Stirring Fluid Loss Test
•
Disassemble and Clean the Equipment
•
Reassemble the Equipment
5.1
Pre-test the Instrument
1.
Arrange sample chamber (also called reservoir, cylinder, or test cell) parts for
assembly. Check all O-rings for nicks, abrasions, cement debris and brittleness.
Replace damaged O-rings.
2.
Lubricate threads and O-rings with heavy grease to make cleanup easier after
testing is complete.
3.
Check the filter screen for plugging or holes in the support plate.
4.
Spin the paddle and shaft, listen for grinding sound, and feel for tightness. Refer
to Section 7 Troubleshooting and Maintenance for servicing, if required.
5.
Screw paddle cap assembly in one end of the sample chamber and hand-tighten.
Paddle cap assembly should be as nearly flush as possible with chamber end.
6.
Insert sample chamber (open end first) into the heating jacket.
7.
Rotate the chamber slowly clockwise to ensure the notches engage the screws on
heating jacket end.
8.
Make sure the nitrogen pressure port on the sample chamber points away from
you. If not, lift chamber slightly and rotate it a half turn, and recheck.
9.
Swing locking plate into position to hold chamber in heating jacket. Use hand
knob to tighten.
10.
Attach supply pressure line that is coiled on heating jacket mount to the coupling
on the side of the paddle cap assembly. Hand-tighten only.
11.
To release heating jacket, pull the red knob and rotate the heating jacket 180
degrees. Pushing the knob latches the heating jacket in its new position.
12.
Rotate the paddle shaft to same position as flexible drive shaft.
13.
Attach flexible drive shaft into position and hand-tighten the flexible shaft collar.
Summary of Contents for 210194
Page 39: ...Stirring Fluid Loss Manual 100031980 Revision F 39 Figure 8 1 Stirring Fluid Loss Assembly...
Page 44: ...Stirring Fluid Loss Manual 100031980 Revision F 44 Figure 8 3 Mainframe Assembly Front View...
Page 45: ...Stirring Fluid Loss Manual 100031980 Revision F 45 Figure 8 4 Mainframe Assembly Rear View...
Page 50: ...Stirring Fluid Loss Manual 100031980 Revision F 50 Figure 8 7 Chamber Assembly...
Page 52: ...Stirring Fluid Loss Manual 100031980 Revision F 52 Figure 8 8 Manifold System Water Nitrogen...