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15

109118-1 Rev. A,10/96

3.3

Maintenance

3.3.1

Meter Maintenance

The Model 440 needs no maintenance except for an occasional
wipe with a damp cloth. The front panel is made of polyester and
is not affected by most solvents. Polyester is known to be affected
by some organic solvents, including toluene, xylene and methyl-
ethyl-ketone. It is good laboratory practice to wipe away any
spillages as soon as they occur.

3.3.2

Electrode Maintenance

CAUTION

Solutions used to clean electrodes must be handled

with the care accorded to toxic or corrosive
substances.

Do not allow the reference chamber of the electrode to dry

out. Always keep it filled with the proper fill solution.

Formation of KCl salt at the tip and side of the electrode is

normal and should be rinsed off with warm water.

Leave the tip of the electrode in an inch (25 mm) of pH 7.0

or 4.0 buffer when it is not being used. Do not leave it in
distilled water. For long term storage follow the electrode
manufacturer's instructions.

If the electrode slope is off or the electrode response has

become sluggish or inaccurate, change the fill solution. If
that does not improve the response then the pH sensing
glass and the junction have probably become coated with
some of the samples being tested.

Test the junction for flow - rinse the tip of the electrode,

blot dry and let the electrode hang in the air for 15
minutes. A proper flowing junction should have KCl salt
crystals forming on it. If none appear, review the following
suggestions for cleaning.

Protein contamination - soak the tip of the electrode for
1-2 hours in a solution of 10% Pepsin and water with
enough Hydrochloric acid added to bring the pH of the
solution to 1.0. Rinse the electrode and soak in pH 7.0
buffer until stable.

3

Summary of Contents for 440 pH Meter

Page 1: ...ded for use by persons knowledgeable in safe laboratory practices If the 440 is not used in accordance with these instructions for use the protection provided by the equipment may be impaired The 440...

Page 2: ...asurements 9 2 6 Temperature Measurements 10 2 7 Changing the Resolution 11 2 8 Chart Recorder 11 2 9 Interfacing via the RS232 Output 12 3 Support Information 3 1 Basic Theory 13 3 2 Operating Hints...

Page 3: ...ories packing sheet for a list of the additional components 3 To attach the electrode arm to the pH meter a The electrode arm can be attached to the left or right hand side Using the screwdriver suppl...

Page 4: ...r lead to the ATC socket 2 If you are using a separate ATC probe connect it to the ATC socket 3 Connect the power supply unit to the DC socket 1 3 Display and Controls DC power supply unit socket ATC...

Page 5: ...value used when setting calibration buffers Also changes display resolution Selects calibration buffers Selects automatic endpoint detection Turns the display off and places the meter in standby mode...

Page 6: ...play and Controls cont 440 Display temperature or slope value automatic or manual temperature compensation slope value displayed calibration buffer indicator auto endpoint is selected main display mod...

Page 7: ...corrected for temperature see Section 2 6 If you are not using an ATC in the system the Model 440 assumes a temperature of 25 C 2 point calibration Place the tip of the electrode in the second buffer...

Page 8: ...hecks the electrode output for stability and automatically freezes the display when the reading appears stable It can be used during calibration and routine measurements Turn auto endpoint on by press...

Page 9: ...cannot be set closer than 2 pH units from each other You also cannot move one buffer value past another For changes on the low end change buffer 1 first and for changes on the high end change buffer 3...

Page 10: ...will show ATC If not the display will show MTC and 25 C Buffer Temperature Correction Table If you use standard buffers listed below the 440 automatically corrects for temperature using the values sh...

Page 11: ...y The REC socket 2 5 mm phone jack provides a voltage proportional to the displayed reading in pH and mV modes The polarity of the output is the same as the polarity of the input signal Approximate Re...

Page 12: ...computers is part number 477758 and can be ordered from your distributor The pin configuration of that connector and Model 440 output protocols are as follows Pin Signal 1 device enable link to pin 5...

Page 13: ...mple The Model 440 measures and converts the resulting minute electrode voltages into a pH reading The response of a pH electrode or its slope is defined by the Nernst equation Electrode response E0 2...

Page 14: ...urate You should be calibrating and measuring at room temperature 5 When transferring from one sample to another always rinse the electrode with distilled water and blot dry Handle the electrode caref...

Page 15: ...warm water Leave the tip of the electrode in an inch 25 mm of pH 7 0 or 4 0 buffer when it is not being used Do not leave it in distilled water For long term storage follow the electrode manufacturer...

Page 16: ...ble 3 4 Problem Solving Most problems are caused by electrode faults rather than by the Model 440 but power fluctuations can corrupt calibration values being held in the meter memory 3 4 1 Meter Test...

Page 17: ...er fails the above test call the number on the back of this manual for warranty and service information 3 4 2 Meter Error Codes Error codes are designed to give the user information on electrode perfo...

Page 18: ...nd reconditioning electrodes Although slope is useful in generally determining when it is time to do maintenance on an electrode response time is by far the critical factor effecting accuracy of measu...

Page 19: ...r Try adding a drop of KCl fill solution to about 5 mL of the sample In most cases it will not change the pH but will give the sample enough ionic strength for the electrode to finish the reading 2 No...

Page 20: ...rating ATC Display LCD display Outputs RS232 Recorder Input Conditions Impedance greater than 1012 ohms Operating Conditions Operating temperature 5 to 40 C Operating humidity max 80 at 35 C non conde...

Page 21: ...tandards UL1262 CSA151 IEC1010 The 440 also complies with the European EMC Directives and therefore carries the CE mark Environmental Compliance The casework components of the 440 are marked with the...

Page 22: ...3 pH Electrode Rinse Sachets 30 packs 471226 Power Supply 100 120V 50 60Hz 1 471228 Power Supply 230V 50Hz 1 477758 RS232C Cable 1 470109 Shorting Test Clip 3 470493 Dot Matrix Printer with Cables 1 W...

Page 23: ...1992 All rights reserved Corning Incorporated Science Products Division Corning New York 14831 USA Telephone 1 800 222 7740 US and Canada 1 607 974 0353 Outside US Fax 1 607 974 0345 430 Rev A 6 96...

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