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5 Putting into operation

21

Melting Point M-565 Operation Manual, Version F

• Glass window

• Glass window with glass holder

• Install the glass window with glass holder on

the front side of the heating block.

• Press the glass holder down.

• Install the cover.

Accessories

• Place the melting point capillaries in the hole of the housing. The second hole is a reservoir for

used capillaries.

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Summary of Contents for M-565

Page 1: ...Melting Point M 565 Operation Manual 093256F en...

Page 2: ...the right to make changes to the manual as deemed necessary in the light of experience espe cially in respect to structure illustrations and technical detail This manual is copyright Information from...

Page 3: ...ommissioning 20 5 2 1 Unpacking and installation 20 5 2 2 Connecting to a PC with MeltingPoint Monitor software 22 5 2 3 Power connection 22 5 2 4 Calibration 22 Read this manual carefully before inst...

Page 4: ...n without pre registered boiling point method 38 6 3 3 Creating a method 40 6 3 4 Adjusting parameters during a determination 40 6 3 5 Printout 41 6 4 Calibration 42 6 4 1 Calibration principle 42 6 4...

Page 5: ...e explained in section 2 1 1 Reference documents For more information regarding melting point refer to the corresponding literature The Laboratory Assistant 94187 Melting Point M 560 Operating Manual...

Page 6: ...m an overview of the dangers which can develop when operating the instrument Personnel without this training or persons who are currently being trained require careful supervision This Operation Manua...

Page 7: ...ks to users property and the environment can arise when the instrument is used carelessly or improperly The manufacturer has determined residual dangers emanating from the instrument if the instrument...

Page 8: ...applying to the instrument must be strictly followed Duty of maintenance and care The operator is responsible for ensuring that the instrument is operated only in a proper manner and that maintenance...

Page 9: ...pe of delivery Check the scope of delivery according to the order number NOTE For detailed information on the listed products see www buchi com or contact your local dealer 3 1 1 Standard accessories...

Page 10: ...Cleaning tool 051978 A A B B A Boiling point tubes 10 units 019697 B Boiling point capillaries 10 units 051850 User management activation code 11066387 Protective cover 051935 Compaction wire 036721...

Page 11: ...Table 3 2 Optional accessories Product Order number MeltingPoint Monitor software with license 11055332 Sample Loader M 569 051997 Verification set M 560 M 565 3 substances benzil p anisic acid phenol...

Page 12: ...roduct Order number Compact keyboard German CH 029509 Compact keyboard English USA 029508 Serial dot matrix printer including ribbon paper roll and cables 11055438 Ribbon for printer 044306 Paper roll...

Page 13: ...Manual Version F Table 3 2 Optional accessories cont Product Order number IQ OQ After installation OQ For repeat use For further information please contact your local affiliate or distributor IQ OQ M...

Page 14: ...g point at 0 5 C min up to 250 C 0 3 C 250 C to 400 C 0 3 C to 0 5 C Repeatability melting point at 0 5 C min 0 1 C Accuracy boiling point at 1 0 C min up to 400 C 0 5 C Repeatability boiling point at...

Page 15: ...able methods for boiling point 50 Compliant with Pharmacopeia methods PH EUR USP and JP NOTE Temperature measuring accuracy refers to pharmacopoeia melting point 3 3 Materials used Table 3 4 Materials...

Page 16: ...one sample Samples can be observed through the lens or on the color display Detection principle of the Melting Point M 565 e a b c d f g a glass capillary tube b sample c camera d temperature sensor...

Page 17: ...is constantly transferred from the heating block to the sample For pure substances the thermodynamic melting point can be approached by multiplying the ther modynamic correction factor by the square r...

Page 18: ...than the expected boiling point The sample is put into the heating block as soon as the start temperature is reached A delay time allows the equilibrium between sample oven temperature and sample temp...

Page 19: ...tilation returns to idle screen d 3 Select and Set buttons e Rotary knob for navigation in the menu and for select characters f Display Fig 4 4 Front view RS232 PS 2 USB b c d e a f a Mains plug b PS...

Page 20: ...measure chemical substances For safety reasons and to ensure sufficient cooling in the electronic compart ment of the unit must be placed at least 30 cm away from rear walls or other objects No contai...

Page 21: ...Glass window with glass holder Install the glass window with glass holder on the front side of the heating block Press the glass holder down Install the cover Accessories Place the melting point capi...

Page 22: ...onnection to the software In the administrator mode the connection is possible 5 2 3 Power connection ATTENTION Make sure that the voltage of the socket corresponds to the voltage given on the type pl...

Page 23: ...pparatus Use supplied calibration substances only The calibration mode is described in section 6 4 Calibration 6 1 Basic operating principles WARNING The heating oven can reach temperatures up to 400...

Page 24: ...ts for all actions The corresponding symbol is displayed during all processes Melting Point Boiling Point Calibration Tools 6 1 2 Display during a process or in menus a b c a Shows where you are and g...

Page 25: ...t determination Settings menu Result indication numeric result Result indication replay 6 1 3 Entering text Text can be entered by using the rotary knob or an external keyboard Rotary knob Turn the ro...

Page 26: ...the results can be wrong Use the following items Product Order number Melting point capillaries 100 units 017808 Melting point capillaries 1000 units 001759 Fig 6 1 Melting point capillaries 6 2 1 Sa...

Page 27: ...of 4 5 mm is recommended for precision measurements To ensure compa rable results it is important to fill all three capillary tubes to the same height and to compact the substance well in the tubes u...

Page 28: ...heating for details on entering text see 6 1 3 This request can be switched off by chang ing the setting Sample ID request see 6 5 Insert samples and press START to start the deter mination To registe...

Page 29: ...tomatically if a printer is connected Back Turns back to the result menu Sample Switches between sample left middle and right Play Replays recorded video automatically Rotary knob Changes temperature...

Page 30: ...is also possible to store parameter sets as methods To enter the method menu press Method To create a new method press Options New then OK Enter a method name To finish press Save Adjust a parameter a...

Page 31: ...ting parameters during a determination NOTE Measuring parameters can be modified during preheating or a determination This function is possible only if enabled by the setting Param adj during meas see...

Page 32: ...oint Melting range is convenient for substances with a wide melting range The thermodynamic melting point should be used for special application only For detailed information see Section 4 1 1 In the...

Page 33: ...sample center g Curve sample right h General information i Signature of person making the determination NOTE The Average is calculated on the basis of the temperature values with two positions after...

Page 34: ...to 15 This value can be used for most of substances Threshold This value is needed only for melting range determination The default value is set to 15 This value can be used for 80 of sub stances If...

Page 35: ...n F a b c d e f g h i Printout a Instrument type b Determination parameters c Automatically detected results d Manual results e Curve sample left f Curve sample center g Curve sample right h General i...

Page 36: ...r sample at three different temperature ramping rates 0 2 0 5 1 0 C min Plot the resulting melting points versus the square root of their corresponding temperature ramping rate mp pharmacopoeia vs gra...

Page 37: ...f Curve sample left g Curve sample center h Curve sample right i General information j Signature of person making the deter mination NOTE The Average is calculated on the basis of the temperature valu...

Page 38: ...liquid sample We recommend using a syringe for simple filling Insert a boiling point capillary into the boiling point tube with its open thick end down Put the sample immediately into the heating bloc...

Page 39: ...instrument has reached the start temperature Press START to start the determination and follow the instructions on the screen The instrument requests a sample ID during preheating for details on ente...

Page 40: ...START to measure again with the identical measuring parameters 6 3 3 Creating a method NOTE The process of creating a boiling point method is identical that used to create a melting point method see 6...

Page 41: ...rted or the instrument is switched off 6 3 5 Printout a b c d e f Printout a Instrument type b Determination parameters c Automatically detected results d Manual results e General information f Signat...

Page 42: ...an MSDS material safety data sheet The calibration set contains the following substances 4 Nitrotoluene approx 52 C Diphenyl acetic acid approx 148 C Caffeine approx 237 C Potassium nitrate approx 33...

Page 43: ...e rotary knob The pharmacopoeia melting point is written on the certificate of analysis Press Save Follow the instructions on the display After each run the current result is indicated Press START to...

Page 44: ...name of the substance with starting the lowest melting point used for the calibration Set the melting point value for the substance using the rotary knob Enter the Lot number for the substance used E...

Page 45: ...e Results caffeine f Results potassium nitrate g General information h Signature of person making the calibration NOTE The Average is calculated on the basis of the temperature values with two positio...

Page 46: ...urrent date is now indicated under Last verification NOTE FOR USER MANAGEMENT Can only be accessed in the administrator level 6 5 Settings SysInfo Test Test Functional test of the instrument To per fo...

Page 47: ...ch result contained is shown with a graphic Calibration interval 0 36 months default 12 months BUCHI recommends calibration or verification after 12 months using the calibration set and the verifica t...

Page 48: ...able or disable the automatic detection If disabled stop tempera ture of method is the end of the determination Statistic Enable or disable the statistic If disabled mean value and standard deviation...

Page 49: ...6 Operation 49 Melting Point M 565 Operation Manual Version F 6 5 1 Test protocol a b c a Power supply voltage b Values for sample brightness c Signature of person carrying out the test...

Page 50: ...6 Operation 50 Melting Point M 565 Operation Manual Version F 6 5 2 SysInfo protocol a a Setting parameters...

Page 51: ...int M 565 Operation Manual Version F b c d e f b Correction values for calibration c Camera position values d Color values Factory default settings e Date of the factory tests f Signature of the perso...

Page 52: ...between melting point and boiling point 2 Access to the following parameters start temperature heating rate and end temperature 3 Selection of methods but no editing and deleting 4 No access to chang...

Page 53: ...e spare parts used should be carried out only with the prior written permission of the manufacturer 7 1 Housing Check the housing of your melting point instrument for defects controls plugs The housin...

Page 54: ...ing it Remove the cover Follow the instructions mentioned below on the use of the cleaning tool 051978 If a melting point capillary is broken and is stuck in the heating block use the cleaning tool Or...

Page 55: ...atic printout in the settings Bad cable connection Check cable connection Printer switched OFF Switch ON printer No paper Replace paper roll Baud rate settings of printer faulty See section 8 1 1 No m...

Page 56: ...replace if necessary Driver not found Device connected for the first time Install recommended driver Table 8 3 Warning messages Warning number Possible cause Remedy Warning 01 Calibration outdated Ca...

Page 57: ...The following setting should be selected 1 2 3 4 5 7 8 9 10 ON 6 OFF 8 2 Customer service Only authorized service personnel are allowed to perform repair work on the instrument They have comprehensiv...

Page 58: ...iohazard Remove all dangerous substances from the instrument and clean it thoroughly Store and transport the instrument in its original packaging WARNING Electrical hazard Always remove the power cord...

Page 59: ...g any spare parts To ensure optimum system performance and reliability use only genuine BUCHI consumables and spare parts for maintenance and repair Prior written permission of the manufacturer should...

Page 60: ...ly to cause harmful interference in which case users will be required to correct the interference at their own expense Fran ais Cet appareil a t test et s est av r conforme aux limites pr vues pour le...

Page 61: ...11 Declarations and requirements 61 Melting Point M 565 Operation Manual Version F...

Page 62: ...n zh India BUCHI India Private Ltd IN Mumbai 400 055 T 91 22 667 75400 F 91 22 667 18986 india buchi com www buchi com in en Indonesia PT BUCHI Indonesia ID Tangerang 15321 T 62 21 537 62 16 F 62 21 5...

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