Bruker NMR 400 89 Ascend DNP User Manual Download Page 42

Page: 42 / 106

ZTKS0243 / Z31993 / 03

Troubleshooting

6.2

Problem

6.2.1

During Transportation

6.2.2

During Assembling

Continued on next page

Indicator

Possible reason

Solution

Tilt Watch / Shock
Watch activated.

Careless

transportation.

Accept delivery with
reservation.

Remark the extent of
damage in the trans-
portation documents.

Start complaint process.

Approved

Customer

Personnel

Visible damage.

Careless

transportation.

Accept delivery with
reservation.

Remark the extent of
damage in the trans-
portation documents.

Start complaint process.

Approved

Customer

Personnel

Indicator

Possible reason

Solution

Ceiling height too
low for assembling
on magnet stand.

Site does not meet
the required
conditions.

Choose another site that
meets the required
conditions.

Bruker Service

Ceiling height too
low for inserting the
Helium Level Sensor

Site does not meet
the required
conditions.

Insert the Helium Level
Sensor before mounting the
magnet stand.

Bruker Service

Helium bore tube
and radiation shield
are not concentric.

Alignment is not
correct.

Check fixation of the align-
ment rods.

Bruker Service

Summary of Contents for NMR 400 89 Ascend DNP

Page 1: ...Version Innovation with Integrity 400 89 Ascend DNP 03 User Manual NMR ...

Page 2: ...d trademarks of their respective holders This manual was written by Peter van Bommel June 2013 Bruker Corporation Faellanden Switzerland ZTKS0243 Z31993 03 For further technical assistance on the NMR Magnet System please do not hesitate to contact your nearest BRUKER dealer or contact us directly at BRUKER BioSpin AG Industriestrasse 26 CH 8117 Faellanden Switzerland Phone 41 44 825 91 11 FAX 41 4...

Page 3: ...3 ZTKS0243 Z31993 03 0 Contact 9 1 Introduction 11 2 Safety 13 3 Transportation 29 4 Assembling 35 5 Operation 37 6 Troubleshooting 41 7 Maintenance 57 8 Disassembling 59 A Appendix 61 ...

Page 4: ...4 ZTKS0243 Z31993 03 ...

Page 5: ...Intended Use 16 2 4 3 Safety Devices 17 2 4 4 Spare Parts 17 2 4 5 Signs and Labels 18 2 4 6 Technical Risks 18 2 5 Personal Protective Equipment 24 2 6 Description of Signs and Labels 25 2 7 Safety Devices 26 2 8 Behavior in Danger and Emergency Situations 28 2 9 Fire Department Notification 28 3 Transportation 29 3 1 Safety 29 3 2 Packaging 29 3 2 1 Disposal 30 3 3 Transport Inspection 30 3 4 Tr...

Page 6: ...During Energizing and Shimming 48 6 2 5 During Operation of the Magnet Stand 50 6 2 6 During Standard Operation 52 6 2 7 During De energizing and Warming up 54 6 3 Troubleshooting Work 55 6 3 1 After a Quench 55 7 Maintenance 57 7 1 Safety 57 7 2 Cleaning 58 7 3 Maintenance Timetable 58 8 Disassembling 59 8 1 Safety 59 A Appendix 61 A 1 Warning Signs 63 A 2 Figures 65 A 3 Tables 67 A 4 Glossary Ab...

Page 7: ...7 ZTKS0243 Z31993 03 ...

Page 8: ...8 ZTKS0243 Z31993 03 π ...

Page 9: ...dustriestrasse 26 CH 8117 Faellanden Switzerland Phone 41 44 825 91 11 Fax 41 44 825 96 96 http www bruker com E mail service bruker ch Please refer to the Model No Serial No and Internal Order No in all correspondence regarding the NMR system or components thereof ...

Page 10: ...10 ZTKS0243 Z31993 03 Contact ...

Page 11: ... of the technology The manufacturer assumes no liability for damages resulting from non compliance with the instructions and all applicable documentation use for purposes not intended not sufficiently approved persons arbitrary changes or modifications and use of not approved spare parts or accessories 1 3 Customer Service Technical support is provided by Bruker Service via telephone or e mail For...

Page 12: ... The isolators in the magnet stand absorb floor vibrations Different heights and isolators are available optionally The nitrogen turrets 4 connected with the nitrogen flow system 6 and the heat exchangers 5 are the interface to the nitrogen vessel The nitrogen fill in turret is marked with a green label The helium turrets 8 9 connected with the helium flow system 7 are the interface of the helium ...

Page 13: ...nel As a result of professional training by Bruker Service Personnel experience and knowledge of applicable regulations these persons are qualified to perform the specific tasks on the magnet system and its components assigned to them in this manual Approved Customer Personnel are qualified to identify possible hazards and risks associated with the tasks assigned to them and to perform all possibl...

Page 14: ...truction plates The customer has to ensure the intended use of the magnet system The customer has to inform the local fire brigade about the special risks of the magnet system and how to react in the event of an incident The customer must clearly define the responsibilities for operation and maintenance The customer must ensure that all employees working with the magnet system have read and unders...

Page 15: ...a hazardous situation which if not prevented will result in death or serious injury WARNING Indicates a hazardous situation which if not prevented could result in death or serious injury CAUTION Indicates a hazardous situation which if not prevented may result in moderate or minor injury NOTICE Hazard which could result in property damage ...

Page 16: ...Work must only be carried out by approved persons with applicable qualifications The necessary qualifications are specified in the beginning of the relevant chapter In case of doubt contact Bruker Service Contact information see page 9 of this document WARNING Risk of damage to life and limb by incorrect use of the magnet system Incorrect use of the magnet system can lead to life threatening situa...

Page 17: ...devices Do not remove safety devices Check the operational reliability of the safety devices before working on the magnet system WARNING Risk of injury and property damage from using incorrect or defective spare parts and accessories Incorrect or defective spare parts can cause serious injuries They may cause damaging malfunctioning and the destruction of the magnet system Thus Only use original e...

Page 18: ...health Duration of exposure 8 h day above the limit of 200 mT can cause damage to health Ferromagnetic tools in the magnetic field are significantly hazardous Disks and electronic devices may be damaged Thus Mark the magnetic field of more than 0 5 mT 5 Gauss before start up Keep people with active medical implants away from the 0 5 mT 5 Gauss area The permanent workplace of employees must be outs...

Page 19: ...gents are extremely cold Contact with liquid or gaseous cryogenic agents will lead to cold burns Contact with the eyes may cause blindness Refer to Warning Low Temperature on page 21 Thus Only use cryogenic agents in well ventilated rooms In case of doubt ask Bruker Service Wear an oxygen monitor on the body during service and maintenance work Prevent any skin contact with liquid or gaseous cryoge...

Page 20: ...at and further equipment The helium or the nitrogen vessel of the cryostat may get sealed off due to ice formation inside the helium or the nitrogen turrets in case of non compliance with the instruction given in this manual This may lead to overpressure and damage of the helium or the nitrogen vessel Manipulations of components with gas under pressure may lead to injury and property damage Thus I...

Page 21: ...e sensitive components such as O rings from contact with liquid cryogenic agents WARNING Risk of injury from spontaneous ignition and explosion caused by liquid oxygen Pure oxygen condenses on extremely cold metal pieces Together with oil it may ignite spontaneously In case of fire the pure oxygen may cause an explosion Thus Do not smoke near the magnet system Do not use open flames near the magne...

Page 22: ...em on your own WARNING Risk of damage to life and limb caused from heavy weights Lifting heavy weights is life threatening due to falling or moving parts Thus Do not stay or work under a lifted magnet system All lifting equipment in use must be approved to carry the weight Do not use damaged lifting equipment Do not use lifting equipment without updated check tag Lifting only with approved qualifi...

Page 23: ...the boxes in an upright position Do not tilt the boxes Prevent crossing thresholds even if they are only a few millimeters high Clean the transportation way before moving the box Unpack shortly before assembling The contents or further equipment must be protected from rain and other bad weather conditions during transportation Exclusively move the cryostat in its original box Do not remove the tig...

Page 24: ...t with extremely cold liquids or surfaces and for protection from injury caused by rough edges Protective Clothes Used to protect the body from injury caused by contact with extremely cold liquids or surfaces and for protection from wounds Safety Shoes Used to protect the feet from injury from falling of heavy objects An anti slip sole protects from injury caused by slipping and falling on slipper...

Page 25: ... the identified area of 0 5 mT 5 Gauss and are not allowed to enter these areas Prohibition sign No watches or electronic devices Watches and electronic devices may be damaged in the identified area of 0 5 mT 5 Gauss Prohibition sign No credit cards or other magnetic memory Credit cards and magnetic memory may be damaged in the identified area of 0 5 mT 5 Gauss Prohibition sign Do not touch Do not...

Page 26: ...the magnet system is equipped with the following safety devices Figure 2 1 Safety Devices of the Cryostat with 2 Helium Turrets 1 Drop off Plate 2 One way Valve of the nitrogen vessel 3 Safety Valve of the nitrogen vessel 4 One way Valve of the helium vessel 5 Quench Valves ...

Page 27: ...n case of an accidental overpressure in the nitrogen vessel the safety valve will release the pressure smoothly Drop off Plate The drop off plate 1 is a safety device of the RT vessel If the vacuum breaks the drop off plate will open In case of an accidental overpressure in the RT vessel the drop off plate will release the pressure smoothly One way Valves The one way valves of the nitrogen flow sy...

Page 28: ...Burns Help the injured persons to lie down comfortably in a warm room Loosen all clothing which could prevent blood circulation in the injured area Pour large quantities of warm water over the affected parts Cover the wound with dry and sterile gauze In case of contact of liquid cryogenic agents with the eyes rinse thoroughly with clean water Call for medical assistance 2 9 Fire Department Notific...

Page 29: ...ctions in this chapter and to inform these persons before 3 2 Packaging WARNING Heavy Weights see page 22 CAUTION Transportation see page 23 Figure 3 1 Packaging without surrounding panels The cryostat is supplied in a wooden box on a pallet It is secured inside with straps against tilting and moving Accessories such as the flow systems level sensors and bore tubes are in the side compartment of t...

Page 30: ... Shock Watch Tilt Watch on the boxes show if the boxes were kicked or tilted during transportation Checks Shock Watch Follow instructions on the label Tilt Watch Follow instructions on the label In case of damage Accept delivery with reservation Make a documentation of all observable damage and add it to the transportation documents Start complaint process Contact Bruker Service before installatio...

Page 31: ... side 1 Check the route of transport for the minimal height and width 2 Check sufficient floor capacity on the route of transport In case of doubt ask a stress analyst 3 Check sufficient carrying capacity while using an elevator 4 Position the forks between the bars of the box as shown in the figure Make sure the side towards the operator is the one with the labels on it Figure 3 3 Transportation ...

Page 32: ...marked eyelets as attachment points for the lifting equipment 2 Use all eyelets for the lifting equipment Figure 3 5 Instruction Label for Lifting Equipment 3 Follow the instructions on the label on top of the cryostat This label gives important information about correct attachment and transportation 4 Check for correct fastening of the lifting equipment before lifting the cryostat 5 Make sure tha...

Page 33: ...s in a closed dry and dust free room Store the boxes upright Do not tilt the boxes Do not unpack the supplied boxes Prevent mechanical vibrations to the boxes Storage temperature 5 40 C Storage humidity less than 50 23 C 3 7 Disposal For disposal after the life cycle please contact Bruker Service for further information For contact information see page 9 of this document ...

Page 34: ...34 ZTKS0243 Z31993 03 Transportation ...

Page 35: ...35 ZTKS0243 Z31993 03 4 Assembling 4 1 Safety Approved Persons Bruker Service only ...

Page 36: ...36 ZTKS0243 Z31993 03 Assembling ...

Page 37: ... Z31993 03 5 Operation 5 1 Safety Approved Persons Bruker Service Approved Customer Personnel WARNING Magnetic Field see page 18 Cryogenic Agents see page 19 Electricity see page 19 Gas under Pressure see page 20 ...

Page 38: ... delay is over 8 Switch the persistent switch heater OFF 9 Wait until the persistent switch heater delay is over 10 Set the output current to 0 A at the Sweep Power Supply 11 Wait until the output current is 0 A 12 Save the set output current to an applicable file for the next sweep procedure 13 Switch the Sweep Power Supply OFF WARNING Risk of a quench see page 20 if currents at the Sweep Power S...

Page 39: ...with a magnet stand with pneumatic isolators Set the magnet stand into operation by switching the pneumatic controller to UP position Figure 5 2 Stop the Magnet Stand For any work at the magnet system like maintenance or refill of cryogenic agents stop the magnet stand by switching the pneumatic controller to DOWN position ...

Page 40: ...40 ZTKS0243 Z31993 03 Operation ...

Page 41: ...immediately For contact information see page 9 of this manual 6 1 Safety Approved Persons Bruker Service Approved Customer Personnel Personal protective equipment Protective goggles Protective gloves Protective clothes Safety shoes WARNING Magnetic Fields see page 18 Cryogenic Agents see page 19 Electricity see page 19 Gas under Pressure see page 20 Spontaneous Ignition and Explosion see page 21 ...

Page 42: ...ion 2 Remark the extent of damage in the trans portation documents 3 Start complaint process Approved Customer Personnel Indicator Possible reason Solution By Ceiling height too low for assembling on magnet stand Site does not meet the required conditions Choose another site that meets the required conditions Bruker Service Ceiling height too low for inserting the Helium Level Sensor Site does not...

Page 43: ... line Check pumping unit and pumping line A vacuum less than 10 6 mbar must be reached with a closed sealing plug Replace if necessary Bruker Service Room temperature bore tube has scratches or dust on the sealing surfaces Check sealing surfaces on the room temperature bore tube No scratches and no dust should be visible Bruker Service Moisture in the RT vessel Pump and flush the RT vessel several...

Page 44: ...es too quickly Transfer pressure too high Stop cooling Adjust correct transfer pressure Bruker Service Vacuum in RT vessel does not reach 5 x 10 5 mbar in 48 hours O rings may be leaky Check and clean O rings and slots replace O rings if necessary of the Vacuum Valve of the drop off plate of the reduction and sealing flanges of the bottom plate a Bruker Service O rings may be frozen due to contact...

Page 45: ...liquid nitrogen using the precooling tube 3 Check with the dipstick to be sure that the helium vessel is completely empty no liquid nitrogen or frozen nitrogen Bruker Service After some intervals of flushing it is not possible to reach a vacuum in the range of 1 mbar The globes in the quench valves are not fitting correctly in the O rings and thus the quench valves are leaky 1 Stop pumping 2 Remov...

Page 46: ...ewar Bruker Service The transfer pressure in the transportation dewar is too low Increase the transfer pressure Bruker Service The transportation dewar is leaky no transfer pressure built up Check the transportation dewar for leakage Re tighten all connections Bruker Service The siphon or the helium transfer line are blocked with ice Check the siphon and helium transfer line for blockages remove i...

Page 47: ...h 100 after cooling down Empty transpor tation dewar helium transfer stopped Refill or replace transportation dewar Bruker Service The Helium Level Sensor is disturbed by the transfer line s extension piece 1 Stop the liquid helium transfer 2 Remove the transfer line 3 Measure the helium level after some minutes without the transfer line Bruker Service After cooling down the helium boil off is hig...

Page 48: ...vice Connector or cables defective Clean connectors or replace cables if necessary Bruker Service Setting of sense voltage fails The main coil heater switch is OFF The main coil switch is not opened Switch the main coil heater to ON and check the main coil heater current to be adjusted correctly Bruker Service The main coil heater current is not correct The main coil switch is not opened Adjust ma...

Page 49: ...ing Replace the Power Supply Bruker Service The main coil switch can not be closed on field The helium level is too low for energiz ing The main coil switch is not covered with liquid helium Never try to energize the magnet with less than the minimum level during ener gizing in the helium vessel Bruker Service The Power Supply is defective The main current is oscillating Replace the Power Supply B...

Page 50: ... DOWN position Switch pneumatic controller to UP position Approved Customer Personnel Magnet system has direct mechanical contact with the floor via accessories or cables Identify and eliminate contact point Arrange cables in loose S or U shapes Approved Customer Personnel If the problem is still not solved contact Bruker Service Approved Customer Personnel Magnet system has physical contact to th...

Page 51: ...correctly Stop the pneumatic isolators Check the leveling of the cryostat Bruker Service Defective leveling valve Replace leveling valve or isolator Bruker Service Defective mem brane of an isolator Replace leveling valve or isolator Bruker Service Magnet system achieves working position jerkily Piston is not centric or touching its casing Align magnet stand Bruker Service Audible loss of gas Defe...

Page 52: ... suspension tubes are blocked with ice Blow in warm helium gas carefully through an applicable tube Do not insert it more than 600 mm from the top of the helium turrets Bruker Service The helium boil off is too high The Helium Level Sensor is permanently on service mode or used often Switch off Helium Level Sensor Reduce frequency of helium level measurement during measuring of the helium level an...

Page 53: ...oved Customer Personnel RT vessel is wet and cold Vacuum reduced Contact Bruker Service immediately Approved Customer Personnel Not correct helium level warning out of MICS Helium Level Sensor defective Contact Bruker Service immediately Approved Customer Personnel Helium level at constant level no change during days Helium Level Sensor defective Contact Bruker Service immediately Approved Custome...

Page 54: ...t the control cable to the current lead and to the Power Supply correctly Bruker Service The switch Main Coil OFF Shim Coil is not on the Shim Coil position Switch Main Coil OFF Shim Coil on the Shim Coil position Bruker Service High helium flow after breaking vacuum Remaining cryogenic agents in the vessels Remove liquid cryogenic agents Bruker Service Vacuum still remains after 12 hours Vacuum V...

Page 55: ...m If destroyed close the socket with the supplied plug to prevent air from entering the helium flow system or vessel 6 Remove probe and shim system to prevent icing of the shim system 7 Check the nitrogen turrets for icing 8 Start the refill with liquid helium as soon as possible after the quench within one hour after the quench refer to the supplied Refilling Procedure 9 Contact Bruker Service im...

Page 56: ...56 ZTKS0243 Z31993 03 Troubleshooting i If the quench occurs unattended or helium transfer was not possible within one hour after the quench it is recommended to warm up the system to 90 K ...

Page 57: ...page 9 of this document 7 1 Safety Approved Persons Bruker Service Approved Customer Personnel Personal protective equipment Protective goggles Protective gloves Safety shoes WARNING Magnetic Field see page 18 Cryogenic Agents see page 19 Electricity see page 19 Gas under Pressure see page 20 Low Temperatures see page 21 Spontaneous Ignition and Explosion see page 21 ...

Page 58: ...ry according to the supplied Refilling Procedure respecting the warn ings and instructions given there Record the filling session Deviation from estimated consumption may be used for identification of troubles In this case contact Bruker Service Approved Customer Personnel weekly Cryostat Check the nitrogen level Refill liquid nitrogen if necessary according to the supplied Refilling Procedure res...

Page 59: ...59 ZTKS0243 Z31993 03 8 Disassembling 8 1 Safety Approved Persons Bruker Service only ...

Page 60: ...60 ZTKS0243 Z31993 03 Disassembling ...

Page 61: ...61 ZTKS0243 Z31993 03 A Appendix Warning Signs Figures Tables Glossary Abbreviations Technical Data Index ...

Page 62: ...62 ZTKS0243 Z31993 03 Appendix ...

Page 63: ...s under Pressure 20 Heavy Weights 22 Intended Use 16 Key Word and Symbol 15 Low Temperatures 21 Magnetic Field 18 Persons 16 Quench 20 Safety Devices 17 Signs and Labels 18 Slippage 21 Spare Parts 17 Spontaneous Ignition and Explosion 21 Caution Incorrect Transportation 23 Key Word and Symbol 15 Notice Key Word and Symbol 15 ...

Page 64: ...64 ZTKS0243 Z31993 03 Appendix ...

Page 65: ...igure 6 1 Quench Picture 55 Figure A 1 Dimension Cryostat Front View 72 Figure A 2 Dimension Cryostat Top View 74 Figure A 3 Nitrogen Level Graph 76 Figure A 4 Helium Level Graph 77 Figure A 5 Nitrogen Level Sensor 78 Figure A 6 Helium Level Sensor 79 Figure A 7 Characteristic Curve PT 100 80 Figure A 8 Characteristic Curve IBT 81 Figure A 9 Fringe Field Plot 83 Figure A 10 Current Lead 55 pins 85...

Page 66: ...66 ZTKS0243 Z31993 03 Appendix ...

Page 67: ...ristic Values IBT 81 Table A 9 Specification of the Magnet 82 Table A 10 Fringe Field Values 83 Table A 11 Specification of the Sweep Coil 84 Table A 12 Resistance at Room Temperature 93 Table A 13 Sweep Current Lead Resistance refer to Figure A 11 94 Table A 14 Heater Currents 94 Table A 15 Sweep Power Supply Settings 94 Table A 16 Energizing Assignment and Currents 95 Table A 17 Magnetic Center ...

Page 68: ...68 ZTKS0243 Z31993 03 Appendix ...

Page 69: ...yostat is not energized Dewar Any kind of package used for transporting cryogenic agents like liquid helium or nitrogen Pressure Cylinder Any kind of package used for transporting gaseous agents with a pressure up to 200 bar Magnet System The collective of all parts necessary for the intended use The superconducting magnet inside the cryostat is energized Abbreviations Description ACD Automatic Co...

Page 70: ...70 ZTKS0243 Z31993 03 Appendix ...

Page 71: ...plate Address of the Manufacturer Magnet System Identifier Type Identification Number Magnet Identifier Serial Number Year of Construction Cryostat Identifier Specification Helium Vessel Specification Nitrogen Vessel Specification Vacuum Chamber Weight total empty full Value Unit Minimum surrounding temperature 7 C Maximum surrounding temperature 38 C Maximum relative humidity up to 31 C 80 Maximu...

Page 72: ...72 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Dimensions Cryostat Front view Figure A 1 Dimension Cryostat Front View ...

Page 73: ...e 795 mm H1 Height Cryostat bottom plate to top flange 1205 mm H2 Height Cryostat minimum height for transportation 1604 mm H3 Height Cryostat bottom plate to flow system 1763 mm S Height Magnet Stand floor to bottom plate 950 mm M1 Distance magnetic Center to bottom flange refer to Table A 17 page 96 M2 Distance magnetic center to top flange refer to Table A 17 page 96 Table A 2 Dimension Cryosta...

Page 74: ...scend DNP Top view Figure A 2 Dimension Cryostat Top View Dimensions Cryostat Value Unit W1 1236 mm W2 1116 mm D3 1 1 Keep at least an additional free space of 1 5 m around the magnet system for service 1375 mm Table A 3 Dimensions Cryostat Top View ...

Page 75: ...volume 104 l Nitrogen evaporation rate 270 ml h Nitrogen hold time1 16 days Helium vessel total volume 101 l Helium refill volume 82 l Helium evaporation rate sweep coil persistent mode 23 ml h Helium hold time1 sweep coil persistent mode 1 Maximum time intervall between two fillings 150 days Helium refill volume after Quench cool down and refill 150 l Table A 4 Cryogenic Agents ...

Page 76: ...76 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Nitrogen Level Graph Figure A 3 Nitrogen Level Graph ...

Page 77: ...77 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Helium Level Graph Figure A 4 Helium Level Graph ...

Page 78: ...rret 6 lights display the nitrogen level Nitrogen Level Sensor Material No Value Unit Level Sensor Type Z122404 12 1126 860 Diameter 12 mm Overall length 1126 mm Active length 860 mm Table A 5 Nitrogen Level Sensor Figure A 5 Nitrogen Level Sensor Nitrogen Level at more than 90 70 90 50 70 30 50 10 30 Schedule Refill less than 10 Refill immediately ...

Page 79: ...or Material No Value Unit Level Sensor Type Z58103 1500 874 Overall length 1500 mm Active length 874 mm Calibration 0 Calibration resistor Z53168 violet 177 Ω Calibration 100 Calibration resistor Z28628 black 15 Ω Table A 6 Helium Level Sensor Figure A 6 Helium Level Sensor 1 Pin Side 2 Solder Side 3 Pin connector 4 Active length 5 Sensor tube 6 Superconductor ...

Page 80: ...the magnets during cooling and warming up of the magnet system PT 100 i Measure the resistance with a maximum current of 1 mA Temperature Unit Resistance Unit Room Temperature 293 K 107 8 Ω 273 K 100 0 Ω 250 K 91 0 Ω 200 K 71 1 Ω 150 K 50 9 Ω 100 K 30 0 Ω Liquid Nitrogen 77 K 20 1 Ω Table A 7 Characteristic Values PT 100 Figure A 7 Characteristic Curve PT 100 ...

Page 81: ...Resistance with a maximum current of 0 1 mA Temperature Unit Resistance Unit Room Temperature 300 K 220 Ω Liquid Nitrogen 77 K 265 Ω 40 K 300 Ω 20 K 350 Ω 10 K 420 Ω 8 K 450 Ω 6 K 500 Ω 5 K 540 Ω Liquid Helium 4 2 K 575 Ω Table A 8 Characteristic Values IBT Figure A 8 Characteristic Curve IBT ...

Page 82: ...he coils of the magnet can be energized and de energized Persistent Mode In the persistent mode the electricity is flowing exclusively within the magnet The circuit has no connection to the outside The magnetic field cannot be switched off Technical Data Magnet Value Unit Proton frequency 400 MHz Central field 9 39 T Coil inductance 59 5 H Magnetic energy 527 9 kJ Maximum drift rate 0 01 ppm h 4 H...

Page 83: ...Unit R max Unit Z max Unit 200 mT 0 26 m 0 42 m 5 0 mT 0 54 m 0 82 m 3 0 mT 0 62 m 0 92 m 1 0 mT 0 87 m 1 23 m 0 5 mT 1 10 m 1 50 m 0 2 mT 1 52 m 1 99 m 0 1 mT 1 93 m 2 47 m 0 05 mT 2 45 m 3 09 m max magnetic field B0 at access point 418 mT max field gradient dB dz at access point 6 9 T m Table A 10 Fringe Field Values ...

Page 84: ...er supply The sweep coil can be energized and de energized Sweep Coil Persistent Mode In the persistent mode the sweep current lead is mounted but the electricity is flowing exclusively within the sweep coil Technical Data Sweep Coil Value Unit Sweep coil strength 37 8 G A Maximum sweep coil current range 20 A Maximum sweep coil field 750 G Helium evaporation rate sweep coil driven mode 20 A 1500 ...

Page 85: ...85 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Current Lead Figure A 10 Current Lead 55 pins ...

Page 86: ...86 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Sweep Current Lead Figure A 11 Sweep Current Lead 55 pins ...

Page 87: ...87 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Wiring Diagram Magnet Figure A 12 Wiring Diagram Magnet refer to Figure A 9 ...

Page 88: ...88 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Wiring Diagram Magnet Control Figure A 13 Wiring Diagram Magnet Control ...

Page 89: ...S0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Wiring Diagram Magnet Diagnostic and Temperature Sensors Figure A 14 Wiring Diagram Magnet Diagnostic and Temperature Sensors temperature sensors diagnostic ...

Page 90: ...d DNP Shorting Plug Remove the shorting plug before inserting the current lead or the sweep current lead 1 Shorting Plug Tool for fitting and removing the shorting plug 2 Shorting Plug 3 Shorting Plug view from pin side Figure A 15 Shorting Plug 55 pins ...

Page 91: ...S0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Sweep Current Lead Mounting Device Insert the sweep current lead after removing the current lead Figure A 16 Sweep Current Lead Mounting Device M 16 socket ...

Page 92: ...92 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP This page is intentionally left blank ...

Page 93: ...19 PIN Con CONTROL Z Heater Ω From To PIN C D E F PIN B G J K 10 PIN Con SHIM 10 PIN Con SHIM Shim Coils Ω From To PIN T High current Con 19 PIN Con CONTROL High Current to Sense Ω From To High current Con High current Con Main Coil Ω From To PIN U High current Con 19 PIN Con CONTROL High Current to Sense Ω From To PIN T PIN U 19 PIN Con CONTROL 19 PIN Con CONTROL Sense Sense Ω From To PIN C PIN S...

Page 94: ...Pin Sweep Sweep Coil Heater Ω From To B J C D G H F K A E 10 Pin Sweep 10 Pin Sweep Sweep Coil to Heater Ω Table A 13 Sweep Current Lead Resistance refer to Figure A 11 Heater Currents Value Unit Main heater current A Shim heater current A Table A 14 Heater Currents Sweep Power Supply settings Value Unit Persistance switch PS heater current 0 08 A Maximum output current 20 A Current ramp rate 0 2 ...

Page 95: ...ing the Z2 shim heater must be permanently ON Energizing Currents A Sense voltage mV Remarks Bruker Test Site 0 to to to to to Overshoot 0 _ _ of final current to Overshoot 50 10 Minutes break at overshoot current Overshoot to Final Current 50 Total energizing time min Rate of current ramp down with magnet in persistent mode A min 20 Table A 16 Energizing Assignment and Currents ...

Page 96: ...ter from top flange M2 mm Table A 17 Magnetic Center Cycling Assignment and Shim Currents Value Unit Time between energizing and cycling h Time between cycling and shimming h Current rate A h Z Shim current A Z2 Shim current A Z3 Shim current A X Shim current A Y Shim current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current A Frequency change due to cycling kHz Date and S...

Page 97: ...er Test Site Value Customer Site 1 Value Customer Site 2 Unit Magnet main current A Z Shim current A Z2 Shim current A Z3 Shim current A X Shim current A Y Shim current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current A Frequency range due to Z2 Shim Hz h Date and Signature Table A 19 Energizing Currents ...

Page 98: ... Ascend DNP Deenergizing Assignment and Currents _ _ _ _ _ _ _ _ _ _ _ Deenergizing Currents A Sense voltage mV Remarks Bruker Test Site to to to 0 through external diodes Total deenergizing time min Table A 20 De energizing Assignment and Currents ...

Page 99: ...99 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Nitrogen Refill Report Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature ...

Page 100: ...100 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Nitrogen Refill Report Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature ...

Page 101: ...101 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Helium Refill Report Helium level before refill Helium level after refill Refill Volume l Date Time Signature ...

Page 102: ...102 ZTKS0243 Z31993 03 Technical Data MS 400 89 Ascend DNP Helium Refill Report Helium level before refill Helium level after refill Refill Volume l Date Time Signature ...

Page 103: ...ryogenic Agents 18 19 Cryostat 12 26 D Disturbances 50 Drop off Plate 27 E Electricity 19 Emergency 28 Emergency Exit 25 F Fire Department 28 First Aid for Cold Burns 28 I Identification Plate 71 Intended Use 16 L Liability 11 Low Temperatures 21 M Magnetic Center 96 Magnetic Field 18 O One way Valves 27 ...

Page 104: ... Clothes 24 Protective Gloves 24 Protective Goggles 24 Q Quench 20 55 Quench Valve 27 R Rescue Equipment 28 S Safety Devices 26 Safety Shoes 24 Safety Valve 27 Shock Watch 30 Slippage 21 Spontaneous Ignition 21 T Tilt Watch 30 Tilting 22 Transportation 23 W Warranty 11 ...

Page 105: ... History List Index Date Alteration Type 00 August 2011 First release 01 September 2012 Update and released fringe field data and related directives 02 February 2013 Update Magnetic Center 03 June 2013 New layout front and rear page ...

Page 106: ...Bruker Corporation info bruker com www bruker com Order No ZTKS0243 Z31993 03 ...

Search results

Summary of Contents for NMR 400 89 Ascend DNP

Reviews:

Related manuals for NMR 400 89 Ascend DNP

Brands by name

Popular brands

Bruker NMR 400 89 Ascend DNP, User Manual

Search results

Summary of Contents for NMR 400 89 Ascend DNP

Reviews:

Related manuals for NMR 400 89 Ascend DNP

Brands by name

Popular brands