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Bruker Ascend 400'54, User Manual

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Bruker Ascend 400'54 User Manual Download Page 75

75

ZTKS0173 / Z31990 / 04

Technical Data MS 400‘54 Ascend ULH

_ _ _

ʹ

_ _ _

ʹ

_ _ _ _

9.17

Magnetic Center

Magnetic Center

Value

Unit

Distance magnetic center from top flange (MCT)

mm

Distance magnetic center from bottom flange (MCB)

mm

Shimsystem Offset (SO)

see 

Figure 9.11:

 and refer to the supplied Test Protocol AST

mm

Table 9.19:  Magnetic center

Figure 9.11: Magnetic center and shimsystem offset (SO)

MC

Magnetic Center

MCT

Magnetic Center from Top Flange

MCB

Magnetic Center from Bottom Flange

SO

Shimsystem Offset

This p

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Summary of Contents for Ascend 400'54

Page 1: ...Version Innovation with Integrity 400 54 Ascend ULH 04 User Manual NMR...

Page 2: ...rks of their respective holders This manual was written by Renate Petry August 30 2017 Bruker Corporation Faellanden Switzerland ZTKS0173 Z31990 04 For further technical assistance on the NMR Magnet S...

Page 3: ...4 3 Safety Devices 15 2 4 4 Spare Parts 15 2 4 5 Signs and Labels 16 2 4 6 Technical Risks 16 2 5 Personal Protective Equipment 22 2 6 Description of Signs and Labels 23 2 7 Safety Devices 24 2 8 Beha...

Page 4: ...53 7 2 Cleaning 53 7 3 Maintenance Timetable 54 7 4 Maintenance free Components 54 8 Disassembly 55 8 1 Safety 55 9 Technical Data MS 400 54 Ascend ULH 57 9 1 Environmental Conditions 57 9 2 Identific...

Page 5: ...urrents 77 9 20 Deenergizing Assignment and Currents 77 9 21 Current Lead 79 9 21 1 Wiring Diagram Magnet 80 9 21 2 Wiring Diagram Magnet Control and Shims 81 9 21 3 Wiring Diagram Magnet Diagnostic a...

Page 6: ...6 ZTKS0173 Z31990 04 Table of Contents...

Page 7: ...asse 26 CH 8117 Faellanden Switzerland Phone 41 44 825 91 11 Fax 41 44 825 96 96 http www bruker com E mail 2nd level support bbio bruker com Please refer to the Model No Serial No and Internal Order...

Page 8: ...8 ZTKS0173 Z31990 04 Contact...

Page 9: ...of the technology The manufacturer assumes no liability for damages resulting from non compliance with the instructions and all applicable documentation use for purposes not intended not sufficiently...

Page 10: ...The isolators in the magnet stand absorb floor vibrations Different heights and isolators are available optionally The nitrogen turrets 4 connected with the nitrogen flow system 7 and the heat exchang...

Page 11: ...nnel As a result of professional training by Bruker Service Personnel experience and knowledge of applicable regulations these persons are qualified to perform the specific tasks on the magnet system...

Page 12: ...ruction plates The customer has to ensure the intended use of the magnet system The customer has to inform the local fire brigade about the special risks of the magnet system and how to react in the e...

Page 13: ...ymbol and signal word indicates a potentially hazardous situation which could result in death or serious injury unless avoided CAUTION This combination of symbol and signal word indicates a possibly h...

Page 14: ...ork must only be carried out by approved persons with applicable qualifications The necessary qualifications are specified in the beginning of the relevant chapter In case of doubt contact Bruker Serv...

Page 15: ...evices Do not remove safety devices Check the operational reliability of the safety devices before working on the magnet system WARNING Risk of injury and property damage from using incorrect or defec...

Page 16: ...ealth Duration of exposure 8 h day above the limit of 200 mT can cause damage to health Ferromagnetic tools in the magnetic field are significantly hazardous Disks and electronic devices may be damage...

Page 17: ...ents are extremely cold Contact with liquid or gaseous cryogenic agents will lead to cold burns Contact with the eyes may cause blindness Refer to Warning Low Temperature on page 21 Thus Only use cryo...

Page 18: ...tat and further equipment The helium or the nitrogen vessel of the cryostat may get sealed off due to ice formation inside the helium or the nitrogen turrets in case of non compliance with the instruc...

Page 19: ...sensitive components such as O rings from contact with liquid cryogenic agents WARNING Risk of injury from spontaneous ignition and explosion caused by liquid oxygen Pure oxygen condenses on extremel...

Page 20: ...em on your own WARNING Risk of damage to life and limb caused by heavy weights Lifting heavy weights is life threatening due to falling or moving parts Thus Do not stay or work under a lifted magnet s...

Page 21: ...the boxes in an upright position Do not tilt the boxes Prevent crossing thresholds even if they are only a few millimeters high Clean the transportation way before moving the box Unpack shortly befor...

Page 22: ...ntact with extremely cold liquids or surfaces and for protection from injury caused by rough edges Protective Clothes Used to protect the body from injury caused by contact with extremely cold liquids...

Page 23: ...to enter these areas Prohibition sign No watches or electronic devices Watches and electronic devices may be damaged in the identified area of 0 5 mT 5 Gauss Prohibition sign No credit cards or other...

Page 24: ...he magnet system is equipped with the following safety devices Figure 2 1 Safety Devices of the Cryostat with 2 Helium Turrets 1 Drop off plate 2 One way valve of the nitrogen vessel 3 Safety valve of...

Page 25: ...of an accidental overpressure in the nitrogen vessel the safety valve will release the pressure smoothly Drop off Plate The drop off plate 1 is a safety device of the RT vessel If the vacuum breaks t...

Page 26: ...urns Help the injured persons to lie down comfortably in a warm room Loosen all clothing which could prevent blood circulation in the injured area Pour large quantities of warm water over the affected...

Page 27: ...tions in this chapter and to inform these persons before 3 2 Packaging WARNING Heavy Weights see page 20 CAUTION Transportation see page 21 Figure 3 1 Packaging without surrounding panels The cryostat...

Page 28: ...Shock Watch Tilt Watch on the boxes show if the boxes were kicked or tilted during transportation Checks Shock Watch Follow instructions on the label Tilt Watch Follow instructions on the label In ca...

Page 29: ...side 1 Check the route of transport for the minimal height and width 2 Check sufficient floor capacity on the route of transport In case of doubt ask a stress analyst 3 Check sufficient carrying capac...

Page 30: ...use the marked eyelets as attachment points for the lifting equipment 2 Use all eyelets for the lifting equipment Figure 3 5 Instruction Label for Lifting Equipment 3 Follow the instructions on the la...

Page 31: ...in a closed dry and dust free room Store the boxes upright Do not tilt the boxes Do not unpack the supplied boxes Prevent mechanical vibrations to the boxes Storage temperature 5 40 C Storage humidit...

Page 32: ...32 ZTKS0173 Z31990 04 Transportation...

Page 33: ...33 ZTKS0173 Z31990 04 4 Assembly 4 1 Safety Approved Persons Bruker Service only...

Page 34: ...34 ZTKS0173 Z31990 04 Assembly...

Page 35: ...Z31990 04 5 Operation 5 1 Safety Approved Persons Bruker Service Approved Customer Personnel WARNING Magnetic Field see page 16 Cryogenic Agents see page 17 Electricity see page 17 Gas under Pressure...

Page 36: ...ith a magnet stand with pneumatic isolators Set the magnet stand into operation by switching the pneumatic controller to UP position Figure 5 2 Stop the Magnet Stand For any work at the magnet system...

Page 37: ...age 7 of this manual 6 1 Safety Only approved persons should perform the troubleshooting tasks They are outlined in this chapter Bruker Service Approved Customer Personnel Personal protective equipmen...

Page 38: ...ess Approved Customer Personnel Indicator Possible reason Solution Performed by Ceiling height too low for assembly on magnet stand Site does not meet the required conditions Choose another site that...

Page 39: ...lve the drop off plate the reduction and sealing flanges the bottom plate a Bruker Service Defective pumping unit or pumping line Check pumping unit and pumping line A vacuum of at least 10 6 mbar mus...

Page 40: ...ly Transfer pressure too high Stop cooling Adjust correct transfer pressure Bruker Service Vacuum in RT vessel does not reach 5 x 10 5 mbar within 48 hours O rings are leaky Check and clean O rings an...

Page 41: ...fully remove all liquid nitrogen using the precooling tube 3 Use the dipstick to check that the helium vessel is empty no liquid nitrogen or frozen nitrogen Bruker Service After some intervals of flus...

Page 42: ...ck that the helium vessel is empty no liquid nitrogen or frozen nitrogen Bruker Service Transfer of liquid helium does not start The transportation dewar is empty Refill or replace transporta tion dew...

Page 43: ...ret between Helium Level Sensor and connector Bruker Service The Helium Level Sensor is defective Check the Helium Level Sensor using the 0 calibration plug Bruker Service The helium level does not re...

Page 44: ...it can be inserted correctly into the connector Bruker Service Main coil heater test fails Power supply defective Replace the power supply Bruker Service Connector or cables defective Clean connectors...

Page 45: ...g for the warm helium gas to remove small ice spots from the connector Bruker Service The magnet system quenches Loss of superconductivity see After a Quench on page 52 Bruker Service The helium level...

Page 46: ...wrong position Change the switch position Bruker Service Shims do not affect the NMR signal Shim heater current is not correct The shim switches are not opened Set the shim heater current to the speci...

Page 47: ...es in loose S or U shapes Approved Customer Personnel If the problem is still not solved contact Bruker Service Approved Customer Personnel Magnet system is touching the magnet stand Check the level a...

Page 48: ...is not level Stop the pneumatic isolators Check the level of the cryostat Bruker Service Defective leveling valve Replace leveling valve or isolator Bruker Service Defective membrane of an isolator Re...

Page 49: ...ore than 600 mm from the top of the helium turrets Bruker Service The helium boil off is too high The Helium Level Sensor is in service mode or has been used too often Switch off Helium Level Sen sor...

Page 50: ...ut of MICS is false Helium Level Sensor defective Contact Bruker Service immediately Approved Customer Personnel Helium level at constant level no change during days Helium Level Sensor defective Cont...

Page 51: ...control cable to the current lead and to the Power Supply correctly Bruker Service The switch Main Coil OFF Shim Coil is not on the Shim Coil position Switch Main Coil OFF Shim Coil on the Shim Coil p...

Page 52: ...e shim system 6 Start the refill with liquid helium as soon as possible 7 Contact Bruker Service immediately Figure 6 1 Magnet system during a quench A quench is the very fast de energizing of the mag...

Page 53: ...Personal protective equipment Protective goggles Protective gloves Safety shoes 7 2 Cleaning Clean the RT vessel of the magnet system and the magnet stand with a dry or slightly damp cloth Only use w...

Page 54: ...s case contact Bruker Service Approved Customer Personnel weekly Cryostat Check the nitrogen level Refill liquid nitrogen if necessary Follow the safety instructions of the supplied manual Refilling P...

Page 55: ...55 ZTKS0173 Z31990 04 8 Disassembly 8 1 Safety Approved Persons Bruker Service only...

Page 56: ...56 ZTKS0173 Z31990 04 Disassembly...

Page 57: ...net System Identifier Type Magnet Identifier Serial Number Year of Construction Cryostat Identifier Specification Helium Vessel Specification Nitrogen Vessel Specification Vacuum Chamber Weight empty...

Page 58: ...kg Operational weight completely filled with magnet stand 600 kg Weight magnet stand 96 kg Weight magnet stand ready for transportation including box 153 kg Weight magnet system empty ready for trans...

Page 59: ...59 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 3 3 Dimensions Cryostat Front View Figure 9 1 Dimensions of the cryostat front view...

Page 60: ...ht for transportation 1604 mm H3 Height Cryostat bottom plate to flow system 1763 mm S Height Magnet Stand floor to bottom plate 570 mm M1 Distance magnetic center to bottom flange calculated Refer to...

Page 61: ...ULH Top View Keep at least an additional free space of 1 5 m around the magnet system for service Figure 9 2 Dimensions of the cryostat top view Cryostat Dimensions Value Unit W1 1236 mm W2 1116 mm D3...

Page 62: ...en vessel 2 Safety valve of the nitrogen vessel 3 One way valve of the helium vessel 4 Quench valve Opening pressure mbar psi One way valve of the nitrogen vessel 10 0 15 Safety valve of the nitrogen...

Page 63: ...ghts display the nitrogen level see Figure 9 4 Nitrogen Level Sensor Material No Value Unit Level Sensor Type Z122404 12 1126 860 D325 Diameter 12 mm Overall length 1126 mm Active length 860 mm Table...

Page 64: ...the helium fill in turret Helium Level Sensor Material No Value Unit Level Sensor Type Z58103 1500 874 D37X Overall length 1500 mm Active length 874 mm Calibration 0 Calibration resistor Z53168 viole...

Page 65: ...net during cooling down and warming up the magnet system PT 100 Sensor Measure the resistance with a maximum current of 1 mA Temperature Unit Resistance Unit Room Temperature 293 K 107 8 273 K 100 0 2...

Page 66: ...with a maximum current of 0 1 mA Temperature Unit Resistance Unit Room Temperature 300 K 220 Liquid Nitrogen 77 K 265 40 K 300 20 K 350 10 K 420 8 K 450 6 K 500 5 K 540 Liquid Helium 4 2 K 575 Table...

Page 67: ...d and de energized Persistent Mode In the persistent mode the current flows exclusively within the magnet The circuit has no connection to the outside The magnetic field cannot be switched off Technic...

Page 68: ...0 mT 0 37 m 0 64 m 3 0 mT 0 40 m 0 70 m 1 0 mT 0 46 m 0 87 m 0 5 5 Gauss mT 0 50 m 1 00 m 0 2 mT 0 62 m 1 23 m 0 1 mT 0 78 m 1 46 m 0 05 mT 1 00 m 1 75 m max magnetic field B0 at access point 275 1 m...

Page 69: ...Helium needed for cool down 300 l Helium needed for energizing cryo shimming and quench reserve 300 l Table 9 13 Cryogenic Agents Consumption during Installation Cryogenic Agents Value Unit Nitrogen v...

Page 70: ...Figure 9 9 Nitrogen Level Graph mm litres 0 1282 0 0 133 8 30 2 60 0 80 0 100 0 305 0 top of N2 vessel 1061 9 minimum allowed level 25 6 0 of nitrogen level sensor 1225 0 0 100 of nitrogen level sens...

Page 71: ...lium Level Graph mm litres 0 top of helium vessel 941 0 101 6 0 46 0 142 5 20 40 60 80 100 120 minimum level during energizing 574 0 59 6 minimum allowed level 162 3 12 5 top of coil 474 6 48 2 0 of h...

Page 72: ...0 PIN Con SHIM Shim Coils From To PIN C D E F PIN S 10 PIN Con SHIM 19 PIN Con CONTROL Shim Coil to Heater common From To PIN T High current Con 19 PIN Con CONTROL High Current to Sense From To High c...

Page 73: ...ents Value Unit Main heater current mA Shim heater current mA Table 9 16 Heater currents Shim Switch Heater Operation Z0 not detected Z1 automatic Z2 permanent Z3 automatic X automatic Y automatic XZ...

Page 74: ...01 2500 85 01 to 100 01 500 100 01 to 104 04 200 Overshoot 0 3 of final current Final current to Overshoot 50 10 minutes break at overshoot current Overshoot to Final current 50 Total energizing time...

Page 75: ...r from bottom flange MCB mm Shimsystem Offset SO see Figure 9 11 and refer to the supplied Test Protocol AST mm Table 9 19 Magnetic center Figure 9 11 Magnetic center and shimsystem offset SO MC Magne...

Page 76: ...ents Value Unit Shim current rate A min Z1 Shim current A Z2 Shim current A Z3 Shim current A X Shim current A Y Shim current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current...

Page 77: ...urrent A Y Shim current A XZ Shim current A YZ Shim current A XY Shim current A X2 Y2 Shim current A Shimsystem Offset design value Refer to the supplied Test Protocol AST mm Shimsystem Offset Custome...

Page 78: ...78 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH This page is intentionally left blank T h i s p a g e w i l l b e r e p l a c e d b y s p e c i f i c t e c h n i c a l d a t a...

Page 79: ...79 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 21 Current Lead Figure 9 12 Current Lead 55 pin...

Page 80: ...80 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 21 1 Wiring Diagram Magnet Figure 9 13 Wiring Diagram Magnet...

Page 81: ...81 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 21 2 Wiring Diagram Magnet Control and Shims Figure 9 14 Wiring Diagram Magnet Control and Shims...

Page 82: ...82 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 21 3 Wiring Diagram Magnet Diagnostic and Temperature Sensors Figure 9 15 Wiring Diagram Magnet Diagnostic and Temperature Sensors...

Page 83: ...removal of the current lead After inserting the shorting plug the current flows through the shorting plug and no longer through the current lead and the power supply 1 Shorting Plug Tool for fitting a...

Page 84: ...84 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 22 Nitrogen Refill Report Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature...

Page 85: ...85 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH Table continued Nitrogen level before refill Nitrogen level after refill Refill Volume l Date Time Signature...

Page 86: ...86 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH 9 23 Helium Refill Report Helium level before refill Helium level after refill Refill Volume l Date Time Signature...

Page 87: ...87 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH Table continued Helium level before refill Helium level after refill Refill Volume l Date Time Signature...

Page 88: ...88 ZTKS0173 Z31990 04 Technical Data MS 400 54 Ascend ULH...

Page 89: ...avy Weights 20 Intended Use 14 Key Word and Symbol 13 Low Temperatures 19 Magnetic Field 16 Persons 14 Quench 18 Safety Devices 15 Signs and Labels 16 Slippage 19 Spare Parts 15 Spontaneous Ignition a...

Page 90: ...90 ZTKS0173 Z31990 04 Warning Signs...

Page 91: ...h 52 Figure 9 1 Dimensions of the cryostat front view 59 Figure 9 2 Dimensions of the cryostat top view 61 Figure 9 3 Safety valves of the cryostat 62 Figure 9 4 Nitrogen Level Sensor 63 Figure 9 5 He...

Page 92: ...92 ZTKS0173 Z31990 04 List of Figures...

Page 93: ...nsor 64 Table 9 9 Characteristic Values of PT 100 Sensor 65 Table 9 10 Characteristic Values of IBT Carbon Sensor 66 Table 9 11 Specification of the Magnet 67 Table 9 12 Fringe field data of the magne...

Page 94: ...94 ZTKS0173 Z31990 04 List of Tables...

Page 95: ...bbreviations Abbreviations Description ACD Automatic Cooling Device MICS Magnet Information and Control System NMR Nuclear Magnetic Resonance RS Radiation Shield RT Room Temperature used as prefix of...

Page 96: ...96 ZTKS0173 Z31990 04 Glossary...

Page 97: ...ebruary 2013 Update of magnetic center 03 June 2013 New layout of title page and last page 04 August 2017 Update of Technical Data inserted shim system offset shim switch heater operation and mandator...

Page 98: ...Bruker Corporation info bruker com www bruker com Order No Z31990...

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