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ATAGO 3564, Instruction Manual

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ATAGO 3564 Instruction Manual Download Page 34

33 

●

 

Obtaining  the  temperature  correction  factor  for  a  sample  whose  main 
constituent is other than sugar 

①

 

Measure tap water and ensure that the Brix(%) value is 0.0%. If tap water does not 
read 0.0%, see page 29, section "14.Adjusting to the Reference". 

②

 

Let the sample to be measured continuously run across the prism surface.   
Be  sure  to  keep  the  sample  temperature  CONSTANT  at  less  than  15˚C,  or  greater 
than 25˚C. 

③

 

While  letting  the  sample  run,  follow  the  directions  on  page  32  to  display  the 
temperature correction factor. Make sure this reads 1.00. 

④

 

After the temperature correction factor is verified, return to the Brix(%) display. 
Note the Brix(%) value (A value). 

⑤

 

Return  to  the  temperature  correction  factor  screen  and  adjust  the  temperature 
correction factor to 4.00. 
Return to the Brix(%) display and note the Brix(%) Value (B value). 

⑥

 

The temperature correction factor for the sample can be obtained using the following 
formula: 
C value = true value 

－

  A value 

D value = true value 

－

  B value 

 

D value 

－

  (C value×4) 

Factor = 

D value 

－

  C value 

 

⑦

 

Set the obtained temperature correction factor according to the procedure described 
on page 29 (Any value in the range of 0.80 to 5.00 can be set as the factor). 

N

 

To  obtain  the  true  value  [Brix(%)]  of  the  sample,  measure  the  sample  with  a 
benchtop refractometer that can control the temperature (through a waterbath or 
Internal Peltier Thermo-module). 
The temperature should be 20˚C.

 

 
 

Example of procedure 

①

 

Let tap water run and adjust the Brix(%) value to 0.0%. 

②

 

Keep the sample less than 15˚C or greater than 25˚C. 

③

 

Adjust the temperature correction factor to 1.00. 

④

 

When returning to the Brix(%) value, 43.0% is displayed. This is the A value. 

⑤

 

Adjust the temperature correction factor to 4.00. 

⑥

 

Now, the Brix(%) value is 45.4%. This is the B value. 

⑦

 

When measuring the sample with a benchtop refractometer at a constant temperature 
of 20

℃

, the true value is 45.0%. 

⑧

 

To obtain the temperature correction factor from the above example: 
C value = true value - A value = 2.0 
D value = true value - B value = -0.4 

 

-0.4 - (2.0×4) 

Temperature correction factor =   

-0.4 - 2.0 

= 3.5 

 
⑨

 

For this sample, the temperature correction factor should be set to 3.50. 

 
 

Summary of Contents for 3564

Page 1: ...3564 E19 IN LINE BRIX MONITOR CM 800 Cat No 3564 Instruction Manual ...

Page 2: ...34 Optional 17 1 When the main unit is used alone 17 2 When the AC adapter AD 32 AD 33 or AD 34 Optional is used 18 8 External Output 19 1 Recorder output 19 2 RS 232C output 20 9 Power Supply 24 1 When the main unit is used alone 24 2 When the AC adapter AD 32 AD 33 or AD 34 optional is used 24 10 Measuring Brix 25 11 Setting the temperature scale C F 26 12 Setting the Measurement Interval and Mo...

Page 3: ...the following pages Explanation of indications WARNING If this indication is neglected and the instrument is handled incorrectly serious injury or death may result CAUTION If this indication is neglected and the instrument is handled incorrectly injury and or property damage may result Explanation of symbols This symbol denotes an item of which to be warned or cautioned The contents of warning are...

Page 4: ... ATAGO Distributor for an inspection Do not attempt to repair modify or disassemble the instrument yourself Improper servicing may result in fire electrical shock or burns If the instrument is dropped or is subjected to a strong shock have it inspected by an Authorized ATAGO Service Center Fire or malfunction may result if the instrument is used CAUTION Do not apply water or sample to any part of ...

Page 5: ...ed disconnect the power cable plug from the AC 100 240V outlet When transporting the instrument pack it in the original box When transporting by aircraft disconnect the power DC24V cable or the DC output cable of the AC adapter AD 32 AD 33 or AD 34 optional from the power input terminal of the In line Monitor Carefully read this instruction manual and fully understand the function and operation of...

Page 6: ...shock or burn For repair service of the power cable and plug contact an Authorized ATAGO Service Center Do not cut a plug to extend the power cable of the AD 32 AD 33 or AD 34 CAUTION Do not insert or pull out the connector and plug with wet hands When disconnecting the power cable of the AC adapter AD 32 AD 33 or AD 34 optional from the AC 100 240V outlet remove by pulling on the plug only Pullin...

Page 7: ... power DC24V prior to connecting cables to the individual units If the AC adapter AD 32 AD 33 or AD 34 optional is used pull out the power cable plug from the AC100 240V outlet before connecting Connecting the cables while the power is on may result in electrical shock ...

Page 8: ...the temperature is extremely low Do not leave the instrument in a damp place Do not place or drop heavy objects on the instrument Use this instrument under the condition where humidity is 80 at 31 C or lower falling linearly to 50 at 40 C Main supply voltage fluctuation should not to exceed 10 the nominal voltage Installation categories Overvoltage Categories ｌｌ The pollution degree is 2 according...

Page 9: ...that the Refractive Index in a vacuum is 1 and is called the absolute Refractive Index Generally however this index is seldom used 3 Brix scale The instrument is programmed with the Brix scale based on the Refractive Index of water nD 1 33299 as the reference 0 The Brix scale represents the weight of sucrose expressed by percentage sucrose weight in grams contained in 100 grams of sucrose solution...

Page 10: ... 34 is an adapter that converts AC 220 240V to DC24V for supplying power to the main unit Sample inlet unit IDF ISO clamp union ferrule IDF ISO screw union screw JIS Flange small diameter series compression fitting and hose connector are available Refer to page 38 19 Consumable Parts and Optional Items Recorder output cable 5m Part No RE 65374 10m Part No RE 65375 15m Part No RE 65376 20m Part No ...

Page 11: ... an ambient temperature of 5 to 40 C Because the instrument incorporates highly precise components DO NOT install in locations exposed to direct sunlight or near a heating source or in an environment that is dusty or exposed to corrosive gasses The instrument should be installed in a location that is free from vibration When installing take special care to avoid any strong shock to the instrument ...

Page 12: ...mples to prevent the electric circuit from overheating Mounting screw locations Used to mount the main unit to the stand Operation display Comprised of the operation keys and display C 2 Operation Display page 12 Power DC24V input terminal Terminal to connect the power cable for DC24V input or the DC output cable of the AC adapter AD 32 AD 33 or AD 34 optional RS 232C output terminal Terminal to c...

Page 13: ... Recorder output upper limit value 5 Changing the Number of Decimal Places Displayed Up and down keys Increase or decrease the value in each setting mode The down key also switches the display of each setting mode The temperature is displayed when press the down key while measuring a sample Fig 4 3 3 AC Adapter AD 32 AD 33 or AD 34 Optional Power cable Connects to the AC 100 240V outlet DC output ...

Page 14: ...rews supplied with the stand to mount the main unit and AD 32 AD 33 or AD 34 on the stand or panel plate The depth of the screw locations is 10mm M6 Main unit Fig 5 1 AD 32 AD 33 or AD 34 Fig 5 2 Example of screw configuration Fig 5 3 Main unit or AD 32 AD 33 or AD 34 Washer M6 Spring washer M6 Hexagonal head bolt M6 10 m Hexagonal head bolts spring washers and washers are included as standard acc...

Page 15: ...ore beginning Electrical shock may occur if the unit is mounted with the power connected CAUTION Ensure that the prism is clean and free of any damage and or scratches Completely remove any sample before installing the main unit to piping or equipment 1 Installation of the main unit with the sample inlet unit optional Compression Fitting Hose connector Straight type L type Fig 6 1 ...

Page 16: ...contaminated with solids dirt and or grease If this happens the prism surface must be cleaned by hand C 17 Cleaning the Prism page 36 The sample inlet unit should be installed in such a manner that it can be easily removed to allow access to the prism for cleaning N Suspending the main unit 2 4kg when using the sample inlet unit to connect to the piping is dangerous Use of the optional stand is re...

Page 17: ...ig 6 8 2 Installation of the main unit without the sample inlet unit optional Please note the following when installing the main unit to piping or equipment without using a sample inlet unit optional The size of the prism stage of the main unit is a 3S ferrule The ferrule connection is recommended for installation Install the main unit so that the prism surface is at a right angle to the ground Co...

Page 18: ...nect the power DC24V input cable connector provided to the power DC24V input terminal located at the bottom of the main unit Connect the opening of the input terminal with the connector pin and insert the connector Then fasten the connector by turning the connector ring clockwise To disconnect the power cable fully turn the connector ring counterclockwise and remove the connector Connect the power...

Page 19: ...he connector pin and insert the connector Then turn the connector ring clockwise to fasten the connector To disconnect the DC output cable fully turn the connector ring counterclockwise and remove the connector m At this stage keep the plug disconnected from the AC 100 240V outlet m When AD 32 AD 33 or AD 34 is used the power DC24V input cable provided with the main unit is not used Fig 7 3 AD 32 ...

Page 20: ... 232C 1 Recorder output The Recorder Output provides a 4 to 20mA signal open circuit voltage is approx 24V of the Brix and temperature 15 5 to 160 5 C The Brix range to be output through the 4 to 20mA signal is set as described in Chapter 16 Setting the Recorder Output See page 34 To utilize the 4 to 20mA signal connect the Recorder Output Cable optional to the Recorder Output terminal on the main...

Page 21: ... optional accessory When using the RS 232C cable the main unit and the PC should be separated by no more than 15 meters RS 232C output cable and code tables Fig 8 2 Pin No Code color 1 Black 2 Black White 3 Red 4 Shield Pin No Code color Signal name 2 Black TXD 3 Black White RXD 5 Red S GND 7 8 Fold ...

Page 22: ...a Tarm is used as an example Download Tera Term from a website such as the one below http ttssh2 sourceforge jp index html en 1 Start Tera Term Select serial on the New connection dialogbox Select the port number Click OK Check the port number Control Panel System and Security Device Manager Port 2 Click Setup and then Serial port ...

Page 23: ...ings are conformed to the instrument settings Enter the port number selected in step 1 Click OK 4 Click Setup and then Terminal port 5 Enter the settings as shown below and Click OK Make sure that the Local echo is checked ...

Page 24: ...gher EE EE Error Temperature The temperature output range is 15 5 to 160 5 in the case of C and is 004 1 to 320 9 in the case of F Example C F Output Data Temperature Output Data Temperature LLL L 15 6 C or less LLL L 4 F or less 023 5 23 5 C 050 0 50 F 120 0 120 0 C 250 0 250 F HHH H 160 6 C or higher HHH H 321 F or higher Refractive Index Output Data Refractive Index L LLLLL Equivalent to Brix 2...

Page 25: ...or AD 34 to an outlet be sure to connect the ground pin as well m The main unit has no power switch When power is supplied to the main unit the measurement value display illuminates and the Brix measurement commences 1 When the main unit is used alone Confirm that the power DC24V input cable is properly connected to the main unit and the DC24V power supply When the DC24V power is supplied the main...

Page 26: ...it has no power switch The Brix value will be displayed when sample flows onto the prism surface If there is no sample on the prism surface only air the error message LL L will be displayed The main unit constantly detects the temperature of the prism When the sample temperature is within the range of 5 to 100 C the Brix values are automatically compensated for temperature N When the sample temper...

Page 27: ... the real time measurements in Brix Hold down the key for one second Once t appears press the key c will appear c C F F Use the key to select a scale Press the key to confirm the selection and t will appear Each time the key is pressed the menu item displayed switches in the order of 0 1 2 3 4 5 and Brix Select Brix N The factory default is C ...

Page 28: ...Select Brix Measurement interval c There are 5 options of intervals at which the unit takes measurements The factory default is the shortest interval c 1 wherein measurements are taken every approx one second The other options indicate longer intervals c 2 is twice as slow as c 1 c 3 three times as slow and so forth The measurement interval setting is reflected on the data transmission rate Mode S...

Page 29: ... is displayed press the key 2 will appear This means that readings will be displayed to the 2nd decimal place when Brix values of less than 10 are measured Press the key to change it to 1 This means that readings will be displayed to the 1st decimal place when Brix values of less than 10 are measured Press the and key to switch back to 2 Press the key and 5 will appear Press the key again to switc...

Page 30: ...e key When the Brix value blinks adjust the value to 0 0 for tap water or to the true value for the reference sample by using the and or keys Fig 14 2 Pressing the sets the adjustment and the display returns to 1 Fig 14 1 Each time the is pressed the menu item displayed switches in the order of 2 3 4 5 and Brix Select Brix N If 30 seconds pass when in steps through above the display returns to the...

Page 31: ...rrection values for 5 to 100 C have been set on the instrument If sugar is the main constituent of soluble solids in the sample these values can be used as they are If the temperature correction factor is changed inadvertently refer to page 32 Inputting the temperature correction factor By utilizing these instructions it is possible to set the temperature correction factor back to 1 00 Setting pro...

Page 32: ... 38 0 38 0 37 26 0 42 0 43 0 44 0 45 0 46 0 46 0 47 0 47 0 48 0 48 0 48 0 48 0 48 0 47 0 47 0 46 0 46 0 45 27 0 50 0 51 0 52 0 53 0 54 0 55 0 55 0 56 0 56 0 56 0 56 0 56 0 56 0 55 0 55 0 54 0 53 0 52 28 0 58 0 59 0 60 0 61 0 62 0 63 0 64 0 64 0 64 0 65 0 65 0 64 0 64 0 63 0 63 0 62 0 61 0 60 29 0 66 0 67 0 68 0 70 0 71 0 71 0 72 0 73 0 73 0 73 0 73 0 73 0 72 0 72 0 71 0 70 0 69 0 67 30 0 74 0 76 0...

Page 33: ... on the display Fig 15 2 If 1 00 is displayed the temperature correction value is for sucrose To change this setting press the or keys until the desired factor is displayed Pressing the key sets the adjustment of the temperature correction factor and the display returns to 2 Fig 15 1 Each time the key is pressed the menu item displayed switches in the order of 3 4 5 and Brix Select Brix N If 30 se...

Page 34: ...ue value B value D value C value 4 Factor D value C value Set the obtained temperature correction factor according to the procedure described on page 29 Any value in the range of 0 80 to 5 00 can be set as the factor N To obtain the true value Brix of the sample measure the sample with a benchtop refractometer that can control the temperature through a waterbath or Internal Peltier Thermo module T...

Page 35: ...0 0 Setting procedure Connect the power according to the procedure described on page 24 section 9 Power Supply The current Brix is displayed on the screen If there is no sample on the prism surface LL L will be displayed Press the key for one second t is displayed Press the key again and the display will change to 0 Press the key again to display 3 Fig 16 1 Press the key The current lower limit va...

Page 36: ...ressed the menu item displayed switches in the order of 5 and Brix Select Brix N If 30 seconds pass when in steps through above the display returns to the continuous display of the Brix m Recorder Output when an error message is displayed Please take note of the recorder output signal when an error message is displayed on the main unit Fig 16 3 Example When the upper limit value of the recorder ou...

Page 37: ...used unplug from the outlet before cleaning Detach the clamp band that connects the main unit to the sample inlet unit piping or tank Clean the prism surface carefully with a soft tissue soaked with warm water or ethyl alcohol If the sample solution contains oil or grease use ethyl alcohol to ensure the prism surface does not develop a film Development of a film on the prism could cause erroneous ...

Page 38: ...ge Brix 0 0 to 80 0 Confirm that the error code HH H is replaced by the known Brix HH H The prism surface is dirty Run a sample with a Brix that is known to be within the indication range Brix 0 0 to 80 0 If HH H continues to be displayed the prism surface may need to be cleaned Clean the prism carefully as described on page 36 A sample with a Brix that significantly exceeds the upper limit value ...

Page 39: ...placed as necessary To place an order please contact an Authorized ATAGO Distributor Part name Part number Description Tie band RE 8507 Maximum temperature Max 150 C Quantity 10 pieces For water bath connection O ring Silicon RE 68100 O ring EPDM RE 68115 O ring Viton RE 68002 O ring used to connect the sample inlet unit to the prism stage unit of the instrument ...

Page 40: ...E 67521 2S Straight type IDF ISO screw union screw RE 67523 2S RE 67515 25A Straight type JIS Flange RE 67525 40A RE 67611 1S Sample inlet unit L type IDF ISO clamp union ferrule RE 67621 2S RE 65374 4 pin connector one sided crimp contact 5m RE 65375 4 pin connector one sided crimp contact 10m RE 65376 4 pin connector one sided crimp contact 15m RE 65377 4 pin connector one sided crimp contact 20...

Page 41: ... 1 34325 27 1 37582 47 1 41385 67 1 45822 8 1 34477 28 1 37758 48 1 41592 68 1 46061 9 1 34629 29 1 37936 49 1 41799 69 1 46303 10 1 34782 30 1 38115 50 1 42009 70 1 46546 11 1 34937 31 1 38296 51 1 42220 71 1 46790 12 1 35093 32 1 38478 52 1 42432 72 1 47037 13 1 35250 33 1 38661 53 1 42647 73 1 47285 14 1 35408 34 1 38846 54 1 42863 74 1 47535 15 1 35568 35 1 39032 55 1 43080 75 1 47787 16 1 357...

Page 42: ...ble for sucrose For 15 to 40 C ICUMSA International Committee of Unified Method of Sugar Analysis values are used For 5 to 15 C or 40 to 100 C the values obtained at the ATAGO laboratories are used The temperature correction values for sucrose can be multiplied by any factor in the range of 0 80 to 5 00 Output Optional Cables Recorder output DC 4 to 20mA Any value between Brix 1 through 80 can be ...

Page 43: ...rument where the temperature is between 5 to 40 C Use the instrument under the condition where humidity is 80 at 31 C or lower falling linearly to 50 at 40 C Main supply voltage fluctuation should not to exceed 10 the nominal voltage Installation categories Overvoltage Categories ｌｌ The pollution degree is 2 according to IEC60664 ...

Page 44: ...43 22 Dimensions CM 800α AD 32 AD 33 AD 34 Side Back Front Side Back detecting unit Front display unit ...

Page 45: ...ot covered under the warranty All instruments received for repair are subject to a possible inspection fee If the unit is inspected and found to be either in good working order or is not covered by the warranty the customer will be responsible for any inspection fees repair costs including labor parts and materials use and shipping charges Replacement Part Information Please note that ATAGO cannot...

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