Agilent Technologies VHS-4 Instruction Manual Download Page 9

ix

VHS-4 Diffusion Pump 

DRAFT 8/7/02

Diffusion Pump Hazards

Designers of systems utilizing diffusion pumps must design out hazards wherever possible. For hazards that cannot be
designed out, warnings, procedures, and instructions on proper use and servicing are provided. Please use guards, safety
features, and interlocks as recommended. 

Refer to Table 1 for a list of general hazards and recommended actions, Table 2 on page x for a list of prohibited actions
that can result in explosions, and Table 3 on page xi for a list of pressurization hazards that can result in damage to
equipment.

THE INSTALLATION, OPERATION, AND SERVICING OF DIFFUSION PUMPS INVOLVES ONE OR MORE OF
THE FOLLOWING HAZARDS, ANY ONE OF WHICH IN THE ABSENCE OF SAFE OPERATING PRACTICES AND
PRECAUTIONS, COULD POTENTIALLY RESULT IN DEATH OR SERIOUS HARM TO PERSONNEL.

Table 1

General Hazards

Hazard

Suggested Corrective Action

Loss of utility: water and/or electricity

Provide sufficient backup water and power supply as 
necessary to effect a safe shutdown under worst case 
conditions

Overpressure in foreline

Provide an interlock to ensure that the power supply to the 
pump heater cannot be activated if the foreline pump is not 
running and/or the pressure in foreline is above 0.5 Torr 
(0.38 mbar)

Overtemperature

Fit temperature sensors and pump fluid level sensors with 
feedback to an interlock on the heater power supply

Insufficient water flow through the main cooling coils 

Use water flow sensor and feedback to interlock the heater 
power supply

Water trapped between inlet and outlet of Quick Cool coil, 
or liquid nitrogen trapped between inlet and outlet of 
liquid nitrogen trap

Provide vent or pressure relief valves for both Quick Cool 
coil and liquid nitrogen trap

Loss of electrical ground integrity

Incorporate ground fault interrupt circuit into heater power 
supply

Positive pressure in pumping system

Integrate pressure relief valve in vacuum system

High voltage 

Prevent personnel contact with high voltages; design and 
attach warnings

Toxicity and Corrosivity

Toxic and/or corrosive gases must be vented to a safe 
location, ensuring adequate dilution or scrubbing to safe 
levels, taking all action required to meet air quality 
standards

Explosion

Integrate pressure relief valves in all systems using 
pumps 10 inches or larger in diameter. 

Do not use hydrocarbon-based pumping oils

Summary of Contents for VHS-4

Page 1: ...m technologies VHS 4 Diffusion Pump Part No 699901021 Rev No D Date October 2000 NOTICE This document contains references to Varian Please note that Varian Inc is now part of Agilent Technologies For more information go to www agilent com chem ...

Page 2: ...D R A F T 8 7 0 2 Copyright 2000 Varian Vacuum Technologies VHS 4 Diffusion Pump ...

Page 3: ...ng standard s or other normative documents auf das sich diese Erklärung bezieht mit der den flogenden Norm en oder Richtlinie n übereinstimmt auquel se réfère cette déclaration est conforme à la auz norme s ou au x document s normatif s al que se refiere esta declaración es conforme a la s norma s u otro s documento s normativo s waamaar deze verklaring verwijst aan de volende norm en of richtlijn...

Page 4: ...serious risk It is the responsibility of the user to maintain safe operating conditions at all times Varian assumes no liability for personal injury or damage resulting from operation or service of the equipment Varian has no control over the use of this equipment and is not responsible for personal injury or damage resulting from its use The safe use and disposal of hazardous or potentially hazar...

Page 5: ... improper use by untrained persons non authorized interference with the equipment or any action contrary to that proved for by specific national standards This manual uses the following standard safety protocol WARNING The warnings are for attracting the attention of the operator to a particular procedure or practice which if not followed correctly could lead to serious injury CAUTION The cautions...

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Page 7: ... 4 Unpacking 4 Pump Oil Installation 4 Vacuum System Connections 4 Cooling Water Connections 5 Electrical Connections 5 Thermal Switch 6 Section II Operation 7 Startup Procedure 7 Shutdown Procedure 8 Section III Maintenance and Service 9 General 9 Periodic Inspection 9 Cleaning 9 Cold Cap Removal Installation 10 Jet Assembly Removal Installation 11 Heater Replacement 12 Adding Pump Fluid 12 Secti...

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Page 9: ...vide an interlock to ensure that the power supply to the pump heater cannot be activated if the foreline pump is not running and or the pressure in foreline is above 0 5 Torr 0 38 mbar Overtemperature Fit temperature sensors and pump fluid level sensors with feedback to an interlock on the heater power supply Insufficient water flow through the main cooling coils Use water flow sensor and feedback...

Page 10: ...s with clean dry oil free compressed air Oxygen and other strong oxidizers are even more dangerous than air Certain conditions of temperature and pressure can cause a combustible mixture to explode The larger the diffusion pump the greater the risk of explosion and the greater the risk of dam age and injury Never operate large diffusion pumps utilizing hydrocarbon oils without a complete safety an...

Page 11: ...nous and Corrosive Compounds When pump ing poisonous reactive and or corrosive gas vapors or chemicals proper operation and regeneration do not always ensure that all hazardous materials have been totally removed If hazardous gas vapors chemicals or combustible mixtures are pumped suf ficient quantities may exist during operation or remain after regeneration to cause severe injury or death Pump Fl...

Page 12: ...oils from previous use turns to steam when the pump is reheated This steam must be allowed to escape with out contacting personnel Whenever possible design the water system with interlock valves so that power cannot be applied to the pump unless water is flow ing in the main cooling coils not Quick Cool coils High Voltages Diffusion pump heaters operate at voltages high enough to kill Design syste...

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Page 32: ...ian India PVT LTD 101 108 1st Floor 1010 Competent House 7 Nangal Raya Business Centre New Delhi 110 046 India Tel 91 11 5548444 Fax 91 11 5548445 Italy Varian Vacuum Technologies Via F lli Varian 54 10040 Leini Torino Italy Tel 39 011 997 9111 Fax 39 011 997 9350 Japan Varian Vacuum Technologies Sumitomo Shibaura Building 8th Floor 4 16 36 Shibaura Minato ku Tokyo 108 Japan Tel 81 3 5232 1253 Fax...

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