Agilent Technologies Cary 600 Series User Manual Download

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Contents

Agilent Cary 600 Series FTIR Spectrometers and Microscopes User’s Guide

Purge gas

Laser 23

Liquid nitrogen

Installation requirements

Training 25

Documentation 26

Conventions 26

Unpacking and Installation

Unpacking 27

Installing the software

Spectrometer and microscope connections

Spectrometer 28

Microscope 31

Connecting the motorized stage cables

Programming accessories for hardware recognition

Operation 35

Lights 36

Turning on the system and filling the Dewar

Spectrometer 36

Microscope 38

Performing a collect

Spectrometer 40

Microscope 40

Accessing the Help

Turning off the system

Summary of Contents for Cary 600 Series

Page 1: ...Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide...

Page 2: ...ed in this document are furnished under a license and may be used or copied only in accordance with the terms of such license Restricted Rights Legend If software is for use in the performance of a U...

Page 3: ...c cooling 8 Compressed gas cylinders 9 Storage 10 Electrical hazards 10 Laser safety 11 Labeling 12 Laser aperture locations 14 Other precautions 14 Warning and caution messages 15 Information symbols...

Page 4: ...lation 27 Unpacking 27 Installing the software 28 Spectrometer and microscope connections 28 Spectrometer 28 Microscope 31 Connecting the motorized stage cables 32 Programming accessories for hardware...

Page 5: ...Contents Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide 5 5 Maintenance 43 Routine 46 Cleaning 46 Spare parts 46 6 Troubleshooting 47...

Page 6: ...Contents 6 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide This page is intentionally left blank...

Page 7: ...erly you have an accurate fast flexible and safe analytical system Unless specified otherwise this manual covers the Agilent Cary 660 670 680 Spectrometers and the Agilent Cary 610 FTIR Microscope If...

Page 8: ...ial hazards If the instrument is used in any manner not specified by Agilent this protection may be impaired Develop safe working habits that do not depend upon the correct operation of the interlocks...

Page 9: ...y or death Store and handle compressed gases carefully and in strict adherence to safety codes Secure cylinders to an immovable structure or wall Store and move cylinders in an upright vertical positi...

Page 10: ...er day makes it impractical Electrical hazards The Agilent Cary 600 Series FTIR spectrometers microscopes and some accessories contain electrical circuits devices and components operating at dangerous...

Page 11: ...A and CE standards for light emitting products An attenuated portion of the laser beam passes into and through the spectrometer sample compartment Although not powerful enough to harm your skin should...

Page 12: ...ry 600 Series FTIR spectrometer The laser safety warning just above the Purge and Air Bearing connections states Laser radiation Do not stare into beam Class 2 laser product IEC 60825 1 2007 Max outpu...

Page 13: ...ide 13 Figure 2 Laser safety warning located on top of internal compartment cover Near apertures The following image shows the laser safety warning located near all apertures on both the Agilent Cary...

Page 14: ...ign of the 600 Series spectrometer and the 610 FTIR microscope normally precludes this Always wear appropriate safety equipment and clothing Figure 4 Laser aperture locations on the spectrometer indic...

Page 15: ...ry safety practices governing the use handling and disposal of such materials are strictly observed These safety practices should include the wearing of appropriate safety clothing and safety glasses...

Page 16: ...on the spectrometer and associated documentation The hazard they depict is shown below each symbol Electrical shock Extreme cold Eye hazard Heavy weight danger to feet Heavy weight danger to hands Hot...

Page 17: ...es with the requirements of one or more EU directives When attached to the rear of the product indicates that the product has been certified evaluated to CSA 61010 1 and UL 61010 1 Color coding The va...

Page 18: ...onformity This declaration is the legal declaration by Agilent that the product complies with the directives and also shows the EN standards to which the product was tested to demonstrate compliance E...

Page 19: ...sures 1 Relocate the radio or antenna 2 Move the device away from the radio or television 3 Plug the device into a different electrical outlet so that the device and the radio or television are on sep...

Page 20: ...Safety Practices and Hazards 20 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide This page is intentionally left blank...

Page 21: ...are for both Unless specified otherwise this manual covers the Agilent Cary 660 670 680 Spectrometers and the Agilent Cary 610 Microscopes If you have purchased the spectrometer only skip all instruc...

Page 22: ...ignificantly above sea level Free from corrosive and flammable fumes Free from strong electromagnetic fields Free from vibrations Performance degradation may result from the exposure of the spectromet...

Page 23: ...itor the flow of the purge gas A regulator is required if the source pressure is greater than 60 psi 420 kPa Tubing should be clean and free of any dust and debris Do not use tubing treated with talcu...

Page 24: ...t and clothing Liquid nitrogen WARNING Extreme Cold Hazard Liquid nitrogen is very cold and can cause damage to the human body Use appropriate protective equipment when handling liquid nitrogen If you...

Page 25: ...ating requirements of the Cary 600 Series FTIR system You must prepare your laboratory according to these instructions before the Cary 600 Series FTIR can be installed You should keep the Site Prepara...

Page 26: ...ur local Agilent sales and service office Documentation This User s Guide provides basic instructions for installing operating and maintaining your Agilent Cary 600 Series FTIR spectrometers and micro...

Page 27: ...f any of the listed items are missing stop immediately and call Agilent customer service 2 Carefully check the exterior of the shipping containers for any external damage Stains on the containers may...

Page 28: ...aged Installing the software While your Agilent representative will install the Resolutions Pro software for you during the installation process it may become necessary to re install it if the compute...

Page 29: ...nd socket on the rear of the spectrometer 2 Connect the power cord to the rear of the spectrometer 3 Connect the other end of the power cable to the electrical power outlet 4 If you have a purged spec...

Page 30: ...sed to connect an external detector 3 Analog Expansion Provides alternate signal paths and controls 4 FPA TRS Used to connect either an FPA detector or TRS accessory 5 USB 2 0 Data system connector to...

Page 31: ...witch on the rear of the microscope is in the off 0 position Figure 8 Power switch and socket on the rear of the microscope USB to PC cable also shown 2 Connect the power cord to the rear of the micro...

Page 32: ...nection see Figure 8 5 Connect the Video out connector to the back of the microscope and then to the video capture card installed in the computer Figure 10 Video capture card installed in PC with Vide...

Page 33: ...S 232 serial cable Power Connects to the power transformer USB Currently not used Joystick Connects to the joystick Z Connects to the Z axis motor used to control the stage height see 2 on Figure 12 u...

Page 34: ...the Service Application software to program or reprogram your programmable accessory to work with the hardware recognition capabilities Most components are programmed in the factory however some may r...

Page 35: ...oscope If you have purchased an Agilent Cary 620 FTIR microscope see the User s Guide supplied with that instrument To access the Resolutions Pro Help 1 Start the Resolutions Pro software 2 Press F1 o...

Page 36: ...ized and needs attention Solid green The spectrometer has initialized and is ready Flashing green The spectrometer is scanning Bottom A D over range Off Normal operation Flashing blue The A D exceeds...

Page 37: ...re the spectrometer has reached operating temperature your data may not be accurate 2 If you have a cryogenically cooled detector MCT or InSb fill its Dewar with liquid nitrogen as follows WARNING Ext...

Page 38: ...liquid nitrogen f Replace the plug g Lower the spectrometer cover 3 Turn on the computer and monitor 4 If you are setting up your spectrometer or if you change the spectrometer detector beamsplitter o...

Page 39: ...id nitrogen 3 Carefully fill the detector Dewar with liquid nitrogen using the provided funnel This takes about 2 5 medium sized Styrofoam cups 475 milliliters 16 ounces of liquid nitrogen Minimize sp...

Page 40: ...spectrometer are 1 Set up the hardware based on the experiment you wish to perform 2 Find the centerburst 3 Run a background collect 4 Load a sample 5 Run a collect For instructions on how to access t...

Page 41: ...y push the black lever away from you Accessing the Help To access the Resolutions Pro Help 1 Start the Resolutions Pro software 2 Press F1 on the keyboard to display the Help 3 Click the Contents tab...

Page 42: ...isable the screen saver because it may interfere with long data collections If you want to have a dark screen during long periods of disuse it is better to turn off the monitor To shut down the comput...

Page 43: ...rts 46 This chapter includes information on how to access the Agilent Cary 600 FTIR spectrometers and microscopes maintenance procedures that may be carried out by an operator Any maintenance procedur...

Page 44: ...ure to the lamp This lamp should always be turned off when the instrument is not in use or when the cover is opened This is easily accomplished by selecting the other source position in the software U...

Page 45: ...uld cause retinal eye damage if prolonged direct viewing occurs This is a Class 2 laser product not powerful enough to harm your skin should your hand intercept it The optical design of the 610 FTIR n...

Page 46: ...Click the plus icon next to Maintenance to expand it Cleaning Any spills in the sample compartment or on the spectrometer or microscope should be immediately wiped up The exterior surfaces of the inst...

Page 47: ...eshooting For troubleshooting help refer to the Resolutions Pro Help To access the Troubleshooting section of the Help 1 Start the Resolutions Pro Software 2 Press F1 on the keyboard to display the He...

Page 48: ...Troubleshooting 48 Agilent Cary 600 Series FTIR Spectrometers and Microscopes User s Guide This page is intentionally left blank...

Page 49: ......

Page 50: ...scribes the following Safety Practices and Hazards Introduction Unpacking and Installation Operation Maintenance Troubleshooting Agilent Technologies 1997 2000 2004 2010 2013 Printed in Malaysia 05 13...

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