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SPRAY DRYER

ADL311/ADL311S

Instruction Manual

- Version 3 -

●

Thank you for purchasing "Spray Dryer, ADL 311/311SS" of

Yamato Scientific Co., Ltd.

●

To use this unit properly, read this "Instruction Manual"

thoroughly before using this unit.

Keep this instruction manual around this unit for referring at

anytime.

：

WARNING!:

Carefully read and thoroughly understand the important

warning items described in this manual before using this

unit.

Yamato Scientific Co. LTD.,

This paper has been printed on recycled paper.

Содержание ADL311

Страница 1: ... this unit Keep this instruction manual around this unit for referring at anytime WARNING Carefully read and thoroughly understand the important warning items described in this manual before using this unit Yamato Scientific Co LTD This paper has been printed on recycled paper This paper has been printed on recycled paper This paper has been printed on recycled paper This paper has been printed on...

Страница 2: ...priate Condition 22 Caution during operation 23 6 Maintenance Method 24 Daily Inspection and Maintenance 24 7 Long storage and disposal 26 When not using this unit for long term When disposing 26 Matters to consider when disposing of the unit 26 8 When a trouble occurs 27 Safety unit and error indications 27 Confirmation and language select for the manual 28 Trouble Shooting 29 9 After Service and...

Страница 3: ...require hospitalization or outpatient visits for a long time Note 2 Minor injury means a wound or an electrical shock that does not require hospitalization or outpatient visits for a long time Note 3 Property damage means damage to facilities devices and buildings or other properties Meanings of pictograms This pictogram indicates a matter that encourages the user to adhere to warning caution incl...

Страница 4: ... Hazard of explosion Caution General cautions Electrical shock Burning Caution for no liquid heating Caution for water leak For water only Poisonous material Prohibitions General bans Fire ban Do not disassemble Do not touch Compulsions General compulsions Connect ground wire Install levelly Pull out the power plug Regular inspection ...

Страница 5: ...ng of this unit is dangerous for non specified service person never repair the unit by the customer himself Do not use the power cord if it is bundled or tangled Do not use the power cord if it is bundled or tangled If it is used in this manner it can overheat and fire may be caused Do not damage power cord Do not damage power cord by bending pulling or twisting forcedly It may cause the fire or e...

Страница 6: ...recovery from a power failure Do not perform unattended operation during activating the unit Do not perform unattended operation during activating the unit Since the unit is in idling status and the nozzle is blocked of after the operation using sample the temperature around outlet is increased and the remaining sample is flown from the sample tube disconnected from the unit and this failure may c...

Страница 7: ...the user 2 Pay attention to the color of each core wire when connecting the power cord Be sure to check that the breaker on the power source equipment side is turned OFF when connecting power cord without fail Note that the ADL311 does not attach the power plug as standard component Select the appropriate power plug and terminal matching to the power capacity of the power source equipment to be co...

Страница 8: ...page 42 15 List of Dangerous Substances 可燃性ガス爆発性ガス 5 Do not use explosive or flammable substances Never use explosive substances flammable substances and substances that include explosive or flammable ingredients in this unit Explosion or fire may occur ADL311S supports organic solvents by connecting it to the optional GAS410 Carefully read the operation manual of GAS410 and take special care for...

Страница 9: ...fied value or whether other device s uses the same power line of this unit If the phenomena might be found change the power line of this unit to the other power line For connecting of the device to the power source ask the dealer that you purchased this unit from or an electrical contractor for safe 9 Handling of power code Do not entangle the power cord This will cause overheating and possibly a ...

Страница 10: ...series Use a separate power supply for a unit with a heater and its total current exceeds 2A Temperature output terminal The temperature output signals for the Outlet outlet temperature and the Inlet inlet temperature are 4 20mA for the measure temperature of 40 240 Current output of 4 20mA Measured temperature of 40 240 Conversion formula Current output I mA 0 08 x measured temperature T 10 Measu...

Страница 11: ...nly Spray nozzle Air spray tube Outlet temperature sensor Stage UP DOWN handle inside the door For blind plate for recorder optional Blower inside the door GAS410 optional connecting nipple For ADL311S only Temperature output terminal Fuse for service outlet Suction hose Service outlet AC100V 2A Cooling water nozzle port O D φ 10 5 Pressurized air inlet O D φ 7 Product collecting container Cyclone...

Страница 12: ... controller on the selected side is used to control the temperature Setting and display of inlet temperature This is used to set an outlet temperature display the measured temperature and as an overheat preventive device Setting and display of inlet temperature This is used to set an inlet temperature display the measured temperature and as an overheat preventive device Pressure meter This meter i...

Страница 13: ...g to use the unit in an AC220V or AC240V district The terminal block is located inside the door at the front control assembly T1 R S 240V 220V 200V 0 V 2 Connecting an earth The power cord of this unit is an earthed 3 core captire cable VCT that integrates an earth wire and you must earth the green wire 電圧側黒電圧側白接地極屋内配線機器緑 3 Connection of the exhaust duct In an environment where hot air or f...

Страница 14: ...culating unit such as CF300 or to a tap water faucet to allow cooking water circulating 6 Open the package of the mini spray attachment GF300 and check for damages to glass and other parts or any missing parts 7 Install the distributor and aluminum honeycomb assembly onto the top of the unit Install the O ring P16 into the φ 20 groove on the top of the distributor install using three M6 x 20 hex b...

Страница 15: ...by hand to lift the stage When the glass chamber reaches the top of the main unit turn the handle by about half a rotation from that position and then securely fix the glass chamber 10 Install the outlet temperature sensor into the pipe at the glass container connecting port and insert the plug into the socket on the top of the main unit Temp sensor connection Drying chamber Stage handle Inside th...

Страница 16: ...cting ferrule D Connecting ferrule D 1 Connecting the cyclone and the glass chamber Power clamp 40A Packing 40A 4 Connecting the cyclone and the product collecting container Product collecting container Container holding band 3 Connecting the cyclone and the connecting ferrule Power clamp 50A Packing 50A O ring P100 Put tightly inside the cover ...

Страница 17: ... for outlet temperature while the control at the lower part is used for indicating inlet temperature and temperature setting You select temperature control for inlet or outlet temperature using SWITCHING When you want to control temperature by the outlet temperature select inlet temperature at the start of operation switch to outlet temperature once the temperature has stabilized Setting ranges wi...

Страница 18: ...n the left diagram and fix the tube with flattened with the pump bracket Set distilled water as the specimen Example Specimen of distilled water set When specimen is not sprayed any more it is suspected that the orifice of the spray nozzle is clogged which can be cleared by pressing the plunger at the upper part of the nozzle P24 Cleaning After Using Exploded view of the spray nozzle The needle P2...

Страница 19: ...ed so that the inlet and the outlet temperature will be stable at the temperatures you want Example Adjust liquid sending speed so that the outlet temperature will be stable at around 75 or slightly lower temperature Influences below are of specific settings on the outlet temperature when the inlet temperature is constant Sent specimen liquid amount small outlet temperature high Dry air amount lar...

Страница 20: ...n to distilled water 12 Turn the heater OFF wait until the outlet temperature drops to 45 or less and turn the blower OFF To avoid a malfunction do not allow the blower operation stopping with the outlet temperature at 45 or over 13 Turn the power switch OFF 14 Remove the container holding band and take out the product collecting container When taking out the container take care the powder attache...

Страница 21: ...he lamp is on the blower is in operation When the lamp is on the blower is in operation When the lamp is on the liquid sending pump is operating in the normal direction When the lamp is on the liquid sending pump is operating in the normal direction When you want to abort processing of the sample or when the nozzle is clogged Abort sending liquid following operations of the ending process P18 8 to...

Страница 22: ...r each dial value of the blower and average flow rate of the drying air Refer to the value for the guideline of the work If air amount is too low the blower filter or the suction filter may be clogged Clean the filter according to the maintenance method see P 25 Besides since the flow rate of the drying air for each dial is differed depending on the frequency of the power source 50Hz or 60Hz pay a...

Страница 23: ...work yourself since it is dangerous and not recommended 3 Do not touch the part with high temperature The chamber cyclone and peripheral part become high temperature during and just after operation Do not touch these parts for there may be caused heat injury Caution 1 Do not put anything on this unit Do not put anything on this unit It will cause injury if fall 2 During a thunder storm During a th...

Страница 24: ... reduce the difference between the temperature around inlet and that around outlet When the reason is in the property of the sample itself adjust the sample by adding the special additive etc グラフ 1 5 In the case that the hygroscopicity is high the product may become the moist powder in the container Change the drying condition following the method in 4 or if required heat up the container for prod...

Страница 25: ...tube made of silicon is oxidized by halogen solenoid or acid strong and may be broken by swelling Therefore pay attention to the treatment during operation 11 When the high temperature is set to the temperature around inlet for the operation supplying too excessive airflow of the blower to the unit may not reach the temperature to the setting one caused by not keeping balance with the heater capac...

Страница 26: ...er completing the operation remove the attachments following the process Preparations on P 11 in reverse order 2 Clean the portion of attachment to which the powder is adhered 3 Flow the distilled water into the sample tube by pressing the pump switch and remove the contaminant attached to the inner of the part 4 Remove the spray air tube and sample tube from the spray nozzle and disassemble the n...

Страница 27: ...he filter after being immersed into the solvent that hot water approx 40 Celsius degree and neutral detergent are mixed at a rate of 5 95 one whole day and night then rinse it with water and air dry it 4 When assembling reversely execute the above procedure Turn the soft surface of the filter to windward when installing the filter Suction filter Regularly clean the suction filter 1 The suction fil...

Страница 28: ...We request you to disassemble this unit as possible and recycle the reusable parts considering to the environmental protection The feature components of this unit and materials used are listed below Component Name Material Parts of Main Unit Casing Bonderizing steel plate baked with melamine resin coating Stainless steel Insulating material Ceramic Felton Specimen bed Stainless steel Production pl...

Страница 29: ...t 230 or over Malfunction of the blower When the measured temperature exceeds the set upper limit upper limit of inlet temperature 230 upper limit of outlet temperature 110 Over Heat will appear the heater output will stop and when that status continues for one minute the temperature error above will be displayed The safety unit will perform automatic REV operation for five seconds when a temperat...

Страница 30: ...on and language select for the manual You can select English or Chinese with the language select function as the OSD language for the manual Confirmation and language select for the manual Pressing ESC key will return to the standby screen ...

Страница 31: ...ayed error Activated the protection circuit without turning on the blower switch Heater disconnection Heater switch failure Heater circuit failure and wiring failure Connect correctly Solve the problem and turn ON the switch Turn ON the blower and then turn ON the heater switch Replace the part Replace the touch panel or sequencer Maintain the part or replace the thermo regulator Feeding pump does...

Страница 32: ...blower and pump Adjusting circuit failure and wiring failure Lack of capacity of heater due to excessive drying airflow Maintain the part or replace the thermo regulator No error For operating this unit with high temperature decrease the flow rate of the drying air or increase the setting value In the case if the error other than listed above occurred turn off the power switch and primary power so...

Страница 33: ...and other information and send it to our customer service center by Facsimile 03 3231 6523 Then store it securely Warranty period is one full year from the date of purchase Repair service for free is available according to the conditions written on the warranty card For repairs after the warranty period consult your dealer one of our sales offices or our customer service center Paid repair service...

Страница 34: ...valve Temperature adjustment range INLET 0 220 differed depending on airflow OUTLET 0 60 Temperature adjustment accuracy 1 Temperature display Digital display of the temperature around Inlet Outlet metal sheathed thermocouple element K Adjusting range for drying air 0 0 7m3 min Power supply 1 AC200V single phase 16A AC220V 17A AC240V 18A External dimensions 2 W D H 580 420 1125 Weight Approx 80kg ...

Страница 35: ...r holding band Packing 40A 50A Power clamp 40A 50A Cap Connecting ferrule D PFA wave shaped tube 1 1 2 3 feet long for connecting the cyclone Hose clip Distributor O rings P16 P135 included Hex bolt M6 x 20 Flat washer M6 Spring washer M6 Aluminum honeycomb Pipe Spray nozzle Round single ended wrench Polyethylene tank for 100g of 5 sodium chloride solution Warranty card 1set 1set 1 1 1each 1each 1...

Страница 36: ...34 11 Wiring Diagram ADL311 Wiring Diagram ...

Страница 37: ... panel M1 Blower motor PLC Sequencer M2 Liquid sending pump motor TH1 TH2 Temperature sensor SC Service outlet TIC1 Inlet temperature controller F Current fuse 2A TIC2 Outlet temperature indicator X1 Power relay FCS PC Blower speed control substrate X2 FAN relay PUMP PC Liquid sending pump speed control substrate SW1 Power switch SSR Solid state relay SW2 Inlet outlet temperature control selector ...

Страница 38: ...36 11 Wiring Diagram ADL311S Wiring Diagram ...

Страница 39: ...equencer SC Service outlet TH1 TH2 Temperature sensor F Current fuse 2A TIC1 Inlet temperature controller X1 Power relay TIC2 Outlet temperature indicator X2 FAN relay FCS PC Blower speed control substrate SW1 Power switch PUMP PC Liquid sending pump speed control substrate SW2 Inlet outlet temperature control selector switch SSR Solid state relay SW3 Nozzle detection reset switch H1 H2 Heater CN1...

Страница 40: ...id valve Distributor 3 way solenoid valve ADL311S only Drying chamber Needle valve Cap Pressure meter Outlet temperature sensor Spray nozzle Cyclone Liquid sending pump Product collecting container Nozzle cooling connecting port For connecting optional unit GAS410 Only ADL311S Connecting pressurized air Suction ...

Страница 41: ...ontainer for product Time after the sample is sprayed with the nozzle till it is fed into this container does not take 0 5 seconds Moreover since the sample powder is always surrounded with the solvent vapor moisture vapor the temperature does not rise extremely around the particle due to the vaporization heat Therefore in case of the heat sensitive material such as an enzyme disintegration can be...

Страница 42: ...cal pipe Yamato Scientific 4210026024 O ring P145 4 types D Viton For upper cylindrical pipe Yamato Scientific 4210026045 Pressure meter DU 1 4 60 3K Nisshin Gauge 5050036002 Needle valve 2412T S 1 8 7 Kojima 3150116002 Toggle switch 2M 2032 Nikkai LT00027715 Switch HLS112A G Fujisoku 2010086022 Volume RV24YN20S B103 077C TOCOS LT00027710 Volume RV24YN20S B204 069C TOCOS LT00027711 Motor FY8PF15N ...

Страница 43: ...7662 Socket PTF08A Omron LT00017832 Stepdown transformer AD21 015KB2 TOYOZUMI LT00000982 Switching power LEA50F 24 COSEL LT00027661 Fan control substrate YY0609 A FSPC Ryowa LT00020329 Liquid tube GAS41 40610 Silicone Yamato Scientific LT00027796 Fuse FGMB 125V2A 200P MISUMI LT00027794 Parts for ADL311S Part name Standards Manufacturer Code No Micro switch SS 01GL2 Nozzle port Omron A0020084 Solen...

Страница 44: ...00 40100 Silicone Yamato Scientific LT00027544 Connecting ferrule D GF300 40080 LT00027543 PFA wave formed tube 1 1 2 3 feet 915mm long IIDA GOMU LT00027545 Hose clip JCS Win 2A φ35 50 Black Okada Industry LT00038408 Packing 40A Silicone OSAME INDUSTRIES F0220141 Packing 50A Silicone OSAME INDUSTRIES F0220143 Power clamp 40A OSAME INDUSTRIES R0100009 Power clamp 50A OSAME INDUSTRIES R0100012 Produ...

Страница 45: ...te sodium chlorate ammonium chlorate and other chlorates Potassium perchlorate sodium perchlorate ammonium perchlorate and other perchlorates Potassium peroxide sodium peroxide barium peroxide and other inorganic peroxides Potassium nitrate sodium nitrate ammonium nitrate and other nitrates Sodium chlorite and other chlorites Calcium hypochlorite and other hypochlorites Flammable substances Ethyl ...

Страница 46: ...LB 2 Before using this unit Be sure to connect the earth wire Use the dedicated outlet for power supply 4 Operating procedures Preparations 1 2 10 Specifications Power supply 2 Installation of the attachment Preparations Connecting the exhaust duct Connection to the compressor Connection of the spray nozzle cooling mechanism as necessary Checking the contents of the GF300 set Installation of the d...

Страница 47: ...zzle Approx 5 min PUMP switch OFF Choke spray pressure to 0 Turn the HEATER switch OFF Turn the BLOWER switch OFF when the outlet temperature dropped to 45 or less Turn the POWER switch OFF Collect powder Clean the containers according to the maintenance method 4 Operating procedures Operating procedures 11 When specimen has been 12 Turn the heater OFF 12 Turn the heater OFF 13 The power switches ...

Страница 48: ...ting instruction Never attempt to perform matters prohibited in this operation instruction Otherwise an unexpected accident may result Notice Descriptions in this operating instruction are subject to change without notice We will replace a manual with a missing page or paging disorder Instruction Manual SPRAY DRYER ADL311 ADL311S Version 3 October 27 2008 Revised May 22 2017 Yamato Scientific Co L...

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