Vitlab 1620506 Скачать руководство пользователя страница 22

4. Operating Exclusions

When the instrument is correctly used, the dispensed liquid comes 
into contact with only the following materials: 
Borosilicate glass 3.3, FEP, ETFE, PFA, PTFE and platinum-iridium.

Never use this instrument for:
–  Liquids which attack FEP, ETFE, PFA and PTFE
–  Solutions containing hydrofluoric acid
–  Solutions which tend to crystallize, fuming acids and concen-

trated bases

–  Suspensions containing solid particles
–  Solutions which decompose and form solid particles (e. g., 

Biuret reagent)

–  Substances which undergo catalytic transformation or react 

with platinum-iridium (e. g., H

2

O

2

)

–  Carbon disulfide as this media inflames easily
–  The instrument should not be used in an aggressive atmos-

phere (e.g., HCl fumes).

–  The instrument must not be autoclaved!

5. Recommended Application Range for VITLAB

®

 continuous

The bottletop-buret VITLAB

®

 continuous E/RS can be used for the following titration media  

(max. conc. 1 mol/l).

Reagent

Acetic acid
Ammonium iron (II) sulfate solution
Ammonium thiocyanate solution
Barium chloride solution
Bromide bromate solution
Cerium (IV) sulfate solution
EDTA solution
Hydrochloric acid
Iron (II) sulfate solution
Nitric acid
Oxalic acid
Perchloric acid
Potassium bromate solution
Potassium bromate bromide solution
Potassium dichromate solution

Reagent

Potassium hydroxide solution
Potassium iodate solution
Potassium permanganate solution
Potassium thiocyanate solution
Silver nitrate solution
Sodium arsenite solution
Sodium carbonate solution
Sodium chloride solution
Sodium hydroxide solution
Sodium nitrite solution
Sodium thiosulfate solution
Sulfuric acid
Tetra-n-butylammonium hydroxide solution
Zinc sulfate solution

22

Содержание 1620506

Страница 1: ...ab com Internet www vitlab com Avant le premier emploi de l appareil rincer l appareil soigneusement ou jeter les premiers volumes dos s efore using the instrument for the first time ensure it is rins...

Страница 2: ......

Страница 3: ...0 9 2 Limpieza est ndar 10 9 3 Limpieza a fondo 11 10 Limpieza o cambio de la v lvula de expulsi n y de dosificaci n inversa 12 11 Cambio de la bater a 12 12 Controlar el volumen 13 13 Ajuste 14 13 1...

Страница 4: ...rante que contacte al fabricante 6 Antes de utilizar el aparato comprobar siem pre que ste funcione correctamente por ej desplazamiento suave del mbolo hermeti cidad y asiento fijo de tubos c nulas et...

Страница 5: ...ep sitos pueden dificultar o imposibilitar el desplazamiento del mbolo por ej soluciones cristalizantes o soluciones alcalinas fuertemente concentradas Para la dosificaci n de medios inflamables tomar...

Страница 6: ...ser introducido en el autoclave 5 Campos de aplicaci n recomendados para VITLAB continuous La bureta acoplable a frascos VITLAB continuous E RS puede emplearse para los siguientes medios de valoraci...

Страница 7: ...e volumen 0 00 a 999 9 ml 6 teclas de funci n 7 bloqueo carcasa exterior 8 volantes 9 empalme del filtro 10 bloque de v lvula GL 45 11 tubo de aspiraci n telesc pico 6 Dibujo de conjunto 12 manija de...

Страница 8: ...i n de acuerdo al frasco a ser utilizado y encajar el tubo de aspiraci n hasta el tope en la v lvula de aspiraci n Efectuar un corte inclinado en el extremo inferior del tubo 3 Enroscar el aparato ros...

Страница 9: ...jo hasta desaparici n de cualquier burbuja de aire en la c nula 4 A fin de iniciar una nueva valoraci n pulsar la tecla Start para que se reinicialice la indicaci n en la pantalla con valor cero 5 La...

Страница 10: ...etirar el aparato del frasco y enroscarlo en otro frasco vac o Mantener la c nula de expulsi n sobre la boca del primer frasco utilizado y vaciar el aparato girando los volantes Despu s hacer girar la...

Страница 11: ...fondo el aparato debe ser en parte desmontado 1 Retirar el tubo de aspiraci n telesc pico y limpiarlo con un cepillo blando para botellas si es necesario reemplazarlo 2 Limpiar la c nula de expulsi n...

Страница 12: ...ci n inversa 13 con la mano hasta el tope 7 Encajar la c nula de expulsi n 15 hasta el tope y enroscar la tuerca de seguridad 14 8 Montar procediendo de manera inversa el soporte de la c nula 16 y la...

Страница 13: ...enga en cuenta las instrucciones de manejo del fabricante de la balanza C lculo para el volumen nominal V0 xi resultados de las pesadas n n mero de pesadas Z factor de correcci n por ej 1 0029 l mg a...

Страница 14: ...mente el ltimo valor indicado en pantalla 2 Pulsar simult neamente la tecla y la tecla mantenerlas pulsadas durante 3 segundos hasta que CAL aparezca parpadeando en la parte superior derecha de la pan...

Страница 15: ...raci n hasta que se pueda sumergir en el l quido La aspiraci n de l quido es imposible La v lvula de aspiraci n est obstruida o adherida Proceder a la limpieza v ase cap tulo 9 si es necesario enviar...

Страница 16: ...EN ISO 8655 Modificaciones t cnicas reservadas 15 2 Datos de corriente y tensi n Tensi n de operaci n 3 V 2 bater as LR03 AAA de 1 5 V cada una Consumo de corriente inferior a 10 mA Tipo de protecci...

Страница 17: ...en corra con la responsabilidad y los costes del env o de vuelta 16 2 Servicio de calibraci n Las normas ISO 9001 y las directivas BPL exigen el control regular de sus aparatos volum tricos Nosotros r...

Страница 18: ...descartarse separadamente de los residuos dom sticos residuos municipales mezclados Seg n la directiva UE 2002 96 CE del Consejo y Parlamento Europeo sobre residuos de aparatos el ctricos y electr nic...

Страница 19: ...g 26 9 1 Emptying 26 9 2 Standard Cleaning 26 9 3 Intensive Cleaning 27 10 Cleaning or replacement of discharge recirculation valve 28 11 Battery replacement 28 12 Volume Check 29 13 Recalibration 30...

Страница 20: ...ched etc 7 Never use force on the instrument Use of force may result in danger to the user or other per sons 1 Safety Instructions Please read the following carefully This Manual does not purport to a...

Страница 21: ...itations Liquids which form deposits may make the piston difficult to move or may cause jamming e g crystallizing solutions or highly concentra ted alkaline solutions When dispensing flammable media m...

Страница 22: ...t must not be autoclaved 5 Recommended Application Range for VITLAB continuous The bottletop buret VITLAB continuous E RS can be used for the following titration media max conc 1 mol l Reagent Acetic...

Страница 23: ...ation mode indicator 5 Titrated volume display 0 00 to 999 9 ml 6 Control keys 7 Lock 8 Hand wheels 9 Air vent opening cap filter connection 10 Valve head GL 45 11 Telescopic intake tube 12 Valve swit...

Страница 24: ...be according to the bottle to be used and push the intake tube into the intake valve as far as it will go Cut the lower end at an angle 3 Screw the instrument thread GL 45 onto the reagent bottle and...

Страница 25: ...ar when the Start or Pause key are pressed and the titration can be continued 6 When the titrating action is finished set the valve switch 12 back to recirculation Attention To avoid splashing of reag...

Страница 26: ...le and mount it on another empty bottle Point the discharge tube into the opening of the used bottle and empty the instrument by turning the hand wheels Then set the valve switch to recirculation and...

Страница 27: ...d For this pur pose the instrument must be partially disassembled 1 Pull off the telescopic intake tube and clean it with a soft bottle brush Replace if necessary especially if cracked or worn 2 Clean...

Страница 28: ...harge recirculation valve by hand 7 Push in the discharge tube 15 Tighten the securing nut 14 8 Mount the discharge tube support 16 and the valve switch 12 When battery power runs low a crossed out ba...

Страница 29: ...lowing steps and is in accordance with DIN EN ISO 8655 Part 6 12 Checking the Volume Calculation for nominal volume V0 xi Weighing results n Number of weighings Z Correction factor e g 1 0029 l mg at...

Страница 30: ...ert to the factory calibration see Chapter 13 3 Reset function Note It is not possible to perform calibration with a value 10 ml or 90 ml as the test volume is then too low or too high At the attempt...

Страница 31: ...mersed in the liquid No liquid is aspirated Intake valve is sticking or clogged Follow Intensive Cleaning procedure Chapter 9 If this does not solve problem follow Repair Service see chapter 16 1 Disp...

Страница 32: ...c error A Random error CV Cat No continuous E 2 5 ml _ 0 2 _ 0 1 1620506 continuous RS 5 0 ml _ 0 2 _ 0 1 1620507 Values based on nominal volume Dispensing volume per rotation of the hand wheels Threa...

Страница 33: ...16 2 Calibration Service ISO 9001 and GLP guidelines require regular examinations of your volumetric instruments We recommend checking the volume every 3 12 months The interval depends on the specifi...

Страница 34: ...ately from household trash mixed municipal waste at the end of their service life According to the Directive 2002 96 EC of the European Parliament and of the Council on Waste Electrical and Electronic...

Страница 35: ......

Страница 36: ...13 1695053 0317 13...

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