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General Requirements 

Operating Environment 

The customer is responsible for providing an acceptable operating environment. Attention paid 

to the operating environment will ensure the continued peak performance of the mass 

spectrometer. 

Temperature/Humidity 

The optimal operating temperature is between 18 and 21 °C (65 and 70 °F). 

NOTE: As laboratory temperature increases, system reliability decreases. All electronic 

components generate heat while operating. This heat must be dissipated to the surrounding air 

if the components are to operate reliably. 

The turbomolecular pump temperature cutoff control protects the bearing to prolong the pump 

lifetime. A laboratory temperature above 30 °C (86 °F) may cause the pump to shut down. 

Operating the MS at optimal temperatures will prolong the turbo pump life. 
There must be good air flow around the system. Your air conditioning system must be capable 

of maintaining a constant temperature (within operational limits) in the immediate vicinity of the 

system. The average steady-state heat load of the 1200L is 6,000 Btu, with a possible short-

term heat dissipation of 15,000 Btu during startup. 
Hot air vented from GC column ovens may contribute to room heating and to the resulting air 

conditioning load. Ducting the GC column oven air out of the lab reduces this heating effect.  
The relative humidity (RH) of the operating environment must be between 40 and 80%, with no 

condensation. Operating the mass spectrometer at very low humidity may result in the 

accumulation and discharge of static electricity, shortening the life of electronic components. 

Operating the system at high humidity may produce condensation and result in short circuits.  
Varian recommends that your laboratory be equipped with a temperature/humidity monitor. This 

will ensure that your laboratory is always in conformance with temperature and humidity 

specifications. 

Particulate Matter 

Take necessary precautions to minimize particulates in the laboratory environment. A layer of 

dust on the electronic components could act as an insulating blanket and reduce heat transfer 

to the surrounding air. 

Vibration 

Ensure that lab benches are free from vibrations, especially those caused by equipment in 

adjoining locations. Because the foreline pump vibrates during operation, install it on the floor 

beneath the mass spectrometer, not alongside the system on the workbench. This is especially 

important when using the 1200L LC, where two foreline pumps are required. 

Exhaust System 

It is your responsibility to provide an adequate exhaust system. Most compounds introduced 

into the mass spectrometer will eventually be exhausted from the foreline pump, along with the 

small amounts of oil vapor that these pumps characteristically emit. Therefore, the pump outlets 

should be connected to a fume exhaust system. Consult local regulations for the proper method 

of exhausting the fumes from your system. LC/MS systems will require venting of the foreline 

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1200/1200L MS Pre-installation Instructions

 

Содержание 1200 GC/MS

Страница 1: ...e relative humidity can be maintained between 40 80 The lab is free of particulate matter The system workbench is free from vibrations The system area is free from electromagnetic disruption and elect...

Страница 2: ...in this manual could cause failures of many types The repair of such failures is specifically excluded from the Warranty and Service contract conditions CAUTION All phases of the installation site pre...

Страница 3: ...densation Operating the mass spectrometer at very low humidity may result in the accumulation and discharge of static electricity shortening the life of electronic components Operating the system at h...

Страница 4: ...hrough doors CAUTION The 1200 MS foreline pump and gas chromatograph are heavy items that require at least two fit people for lifting and moving safely Space and Load Requirements The recommended layo...

Страница 5: ...on devices or test equipment we recommend a separate dedicated power source for their operation Never plug the mass spectrometer and the chromatograph into the same power source or you may overload th...

Страница 6: ...ferably flame treated or solvent washed Ammonia 5 0 Research Grade 99 999 purity A two stage 0 15 psi 0 1 bar pressure regulator that has a stainless steel diaphragm is recommended The output pressure...

Страница 7: ...ation Your GC Accessory Kit includes a GC MS Gas Clean Oxygen Moisture filter CP 17973 and filter base This easy to remove gas filter cartridge combines three highly adsorptive materials in one filter...

Страница 8: ...hin 10 ft 3m of the rear of the 1200L NOTE See Appendix 1 for exact module specifications Power Requirements 1200L GC MS The 1200L GC MS system requires one dedicated duplex single phase power source...

Страница 9: ...1200L GC MS CI Reagent Gases The CI mode for the 1200L MS typically uses methane isobutane or ammonia The amount of gas consumed during CI operation is approximately 1 to 2 mL min The CI reagent gas...

Страница 10: ...ate precautions when using Anhydrous Ammonia and for compliance with all governmental regulations It is the operator s responsibility to understand and adhere to all safe laboratory practices concerni...

Страница 11: ...sed with your filter 1200L LC MS Entrance Before arranging for delivery of the 1200L LC MS to your facility please make sure that all passages to the site of installation are at least 36 in 91 5 cm wi...

Страница 12: ...rces with earth grounds hard wired to the main power panel ground and one 230V 20A power source One of these fourplex power sources is for the mass spectrometer computer and monitor the other fourplex...

Страница 13: ...he CEE 7 7 plug and outlet are shown in Appendix 3 Figure 5 c Gas Requirements 1200L LC MS Nitrogen A Nitrogen gas supply capable of providing up to 12L min of gas regulated at 80 psi is required as a...

Страница 14: ...ld always be kept to a minimum Semiprep and Preparative systems have other requirements limitations with regard to interconnect tubing Typically a system using flow rates up to 200 mL min will require...

Страница 15: ...power sources with earth grounds hard wired to the main power panel ground for the HPLC MS and computer and one 230V 20A power source for the foreline pumps If you have additional sample preparation d...

Страница 16: ...g and corresponding outlet are shown in Appendix 3 Figure 5 a NEMA 5 20P plugs are rated at 20A and 120 Vac The power cables for the computer monitor and printer are approximately 78 in 2m long They a...

Страница 17: ...the line be as short as possible Methane 5 0 Research Grade 99 999 purity A two stage 0 15 psi 0 1 bar pressure regulator that has a stainless steel diaphragm is recommended The output pressure to the...

Страница 18: ...Carrier Gas Helium Helium is required as a carrier gas for the GC with a minimum 99 999 ultra high purity and less than 1 0 ppm each of water oxygen and total hydrocarbons The minimum requirement is o...

Страница 19: ...ing or installation of modules to existing HPLC systems For most analytical HPLC systems flow rates up to 10 mL min 1 16 tubing with an internal diameter ID of 0 005 can be used throughout However 0 0...

Страница 20: ...with the observations Contact the appropriate Varian office to report the damage If no external damage is apparent receiving documents should be signed Received but not inspected to indicate that the...

Страница 21: ...ted and you have accepted the conditions of delivery Spare Parts The 1200 1200L Hardware Operation Manual provides a list of spare parts for routine operation Preventive Maintenance The customer is re...

Страница 22: ...325 Photodiode Array Detector 8 3 21 2 11 7 29 6 18 7 47 5 34 15 5 ProStar 330 Photodiode Array Detector 9 3 23 5 10 2 26 20 50 35 16 ProStar 335 Photodiode Array Detector 8 3 21 2 11 7 29 6 18 7 47...

Страница 23: ...to 12 in 15 to 30 cm Allow vertical clearance above the instrument Dissipate heat and allow for routine maintenance 30 in 76 cm Allow additional bench space beside the Workstation keyboard Enable mous...

Страница 24: ...5 Laser Printer 3 4 1 5 2 Never plug the mass spectrometer and the chromatograph into the same power source otherwise you may overload the power source Never use the free outlet on any of the power s...

Страница 25: ...orten device lifetime It is important to establish the quality of the line power in your laboratory prior to installation of the 1200L LC MS and or GC MS Occasionally line power sources may be of unac...

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