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17 

 
  

Target limits 

When a test result is expected to fall within a 
specific range, the corresponding min and max 
values can be entered into these fields. When a test 
result falls outside the specified range, this value 
will appear in red.  
 

Calibrate 

The automatic calibration is used to determine the 
correct light settings and the exact size of an 
artificial droplet placed in front of the camera.  
For a detailed description of the calibration 
procedure, see Section 4.1.  
 
 
 
 
 
 

9.2

 

The Main program 

This section describes the functions available in the main program screen. 
 

Static Mode

  

is designed to capture a single reading of the static contact angle at ”equilibrium”. 
This value can be measured on smooth, non-porous surfaces not penetrated by the 
test liquid. Typical examples are water droplets on hydrophobic release papers and 
polymer barriers (e.g. liquid container board). 

 

Dynamic Mode

  

captures a video sequence during the interaction between the liquid and the surface. 
Here the dynamic wetting (contact angle), liquid penetration (volume) and 
spreading are measured as a function of time.  

 

Advancing Mode

   is designed to characterise the “wetting hysteresis” as a liquid droplet advances 

across a dry surface and then retracts from a wet surface. This measurement 
requires a reversible pump flow, which is not possible to do with the micro pump 
built into the PGX+Measuring Head.  
 

SuperLow Mode

   is designed for measurement of very low static contact angles below 10 degrees 

related to super clean surfaces.  
 

View Mode

 

produces a report from previously saved data.  

 

Surface Tension

    enables testing of the purity of the test liquid.   

A sufficiently big pendant droplet is pumped out at the dispensing tip and the 
surface tension is determined from the droplet shape.  
 

Surface Energy

   must be determined from calculations using contact angles. Different models exist 

for these calculations using one, two or more liquids in specific combinations.

 

 

Options 

opens a window with the current configuration settings and additional help text.  
This screen is also used for diagnostics and selection of different languages.

 

 
 
 

 
                                                                                                         

 

Fig. 9.4 Image Control Panel with Targets 

Содержание PGX+

Страница 1: ...T Th he e P PG GX X M Me ea as su ur ri in ng g H He ea ad d User s Manual Program version 4 0...

Страница 2: ...2...

Страница 3: ...cing Mode 9 7 SuperLow contact angles 9 8 View Mode 9 9 Surface Tension 9 10 Surface free Energy SFE 9 11 Options Screen 9 12 Enhance Mode 9 13 Baseline Curtain settings 9 14 Camera Gain Threshold 9 1...

Страница 4: ...cal requirements This version of the PGX software can be installed under the following operating systems Windows 10 Windows 8 Windows 7 32 64 bit Windows XP Vista 32 64 Please note the PGX instrument...

Страница 5: ...r on the screen c Finally a message may appear This system must be restarted to complete the installation Press OK to continue d Connect the PGX instrument to the USB port you wish to use e Start the...

Страница 6: ...rument sole The calibration plate has a similar mark indicating the full sphere Place the PGX instrument on top of the calibration plate with its reference mark positioned above the dot as indicated i...

Страница 7: ...displayed in red the instrument must be re calibrated Section 4 1 An optional way to validate the instrument is to place the instrument on top of the calibration plate and perform a measurement in St...

Страница 8: ...e test might require special arrangements like a fixture into which the test specimen can be inserted One example is a metal can or a round glass bottle where it will be necessary to position the drop...

Страница 9: ...ilitre syringe with the RED tip to fill the container with distilled water DO NOT use tap water as this will leave residuals inside the liquid system c Insert the RED dispensing tip into the air hole...

Страница 10: ...m or warping materials e g newsprint cigarette tipping paper should be mounted on top of a flat backing material using a soft sticky adhesive material 6 2 Setting up a test a Check the liquid containe...

Страница 11: ...the empty container c Blow liquid container dry with air d Connect syringe with the RED tip to the dispensing tip and pump air through the tubing until dry e Push the plug back into liquid container...

Страница 12: ...let apply a slightly bigger droplet or move the dispensing tip closer to the test surface A released droplet Fig 7 3 which is immediately transferred to the specimen upon contact with the surface A tr...

Страница 13: ...f A single result can be erased if the result line is selected and the Delete button is pressed g Slide the instrument sideways to a new position h Select Save to store results when the batch is finis...

Страница 14: ...capture the interaction between a liquid and a substrate as a function of time while the liquid droplet penetrates into or spreads across the surface 7 4 Automatic testing in Dynamic Mode Section 9 4...

Страница 15: ...possible outliers far away from the average Click on the associated check box to exclude outliers from the average batch result l Select Save to store results As an option all images in a sequence can...

Страница 16: ...t hand mouse button and click SAVE when finished PLEASE NOTE the button NORMAL is default and cannot be assigned new values Camera Gain offset This feature modifies the live camera image in real time...

Страница 17: ...Here the dynamic wetting contact angle liquid penetration volume and spreading are measured as a function of time Advancing Mode is designed to characterise the wetting hysteresis as a liquid droplet...

Страница 18: ...ow at the top of the screen is updated after each measurement with a new data point showing the contact angle drop volume droplet base or droplet height The Results window is updated with a new data s...

Страница 19: ...operator The file extension PGS will be different if one of the pre defined test liquids has been selected e g Water will give the extension WGS Exit _ Prompts the operator to store pending data befo...

Страница 20: ...or droplet height as a function of time When two or more droplets have been tested the average response for the droplets in a batch is displayed as a continuous line PLEASE NOTE A drop result is exclu...

Страница 21: ...out The test is automatically terminated when this time has elapsed or if the droplet has vanished from the specimen surface It is possible to change the Timeout setting during a batch Remote Control...

Страница 22: ...ct binary mode and slide the handle Gain offset up or down to make the binary image brighter or darker Try to find a position where the contour is continuous and the base of the droplet separated from...

Страница 23: ...e measurement The new top line setting will also update the region setting of the corresponding test button on the Image Control Panel 9 5 4 Make a manual measurement Select the greyscale view and cli...

Страница 24: ...ust be equipped with a fine capillary tube inserted into the PTFE tubing P N 860309 In addition the distance between the dispensing tip and the test surface must be short enough to make sure the dropl...

Страница 25: ...t angle reading is obtained This is referred to as the advancing contact angle The receding phase de wetting Once the advancing angle has been determined the liquid flow is reversed until the droplet...

Страница 26: ...MP button for a short while e Adjust the reference line on the screen to the end of the cannula f Press and hold the PUMP button to pump out a droplet and apply it on the test surface g Wipe the test...

Страница 27: ...droplet and see the rear edge of the droplet Light is then reflected from the rear droplet surface into the camera and the droplet top becomes invisible When the automatic analysis fails or appears i...

Страница 28: ...e and a greyscale image Use the slider below the image to shift to another image 9 8 View Mode This option retrieves previously saved data showing contact angles volumes base diameter or height for th...

Страница 29: ...ble wobbling from side to side which may give an erroneous result The correct droplet size is the volume used immediately before the droplet begins to wobble The algorithm used determines the maximum...

Страница 30: ...test liquid and surface check contact angle is constant over time Surface must by sufficiently smooth Here the operator starts by selecting a Calculation Model from the following options ASTM D5946 Po...

Страница 31: ...tric for the calculation It is possible to force the Geometric method if the parameter SFEMETHOD is changed from H to G see Section 9 18 of this User s Manual The third option Acid Base Lewis uses thr...

Страница 32: ...with the extension sfe e g 45901 sfe When the file has been stored the Save button becomes inactive until a new result is calculated For corona treated polymers water can be used as the single liquid...

Страница 33: ...the droplet base from its background the droplet top can become too bright against the illuminated background This is where the image enhancing routine will be very helpful The enhancing routine is a...

Страница 34: ...at the droplet base This means 0 5 L droplets can be measured down to 3 degrees Similarly a 0 25 L droplet can be measured down to a contact angle of 1 5 degrees For even lower contact angles the dro...

Страница 35: ...ine in Dynamic Mode MINHEIGHT 10 Defines the minimum height of a droplet reduce for smooth surfaces DATADIR C FIBRO PG Default directory for saved data PICSAVING 1 Saves captured images as default 0 n...

Страница 36: ...2 pcs 12 Trouble shooting Camera not found or missing live image or too dark image It is necessary to use the camera drivers supplied with your instrument If you have downloaded later drivers from the...

Страница 37: ...1 5x0 2 mm without inserting a metal needle at the tip Droplet forms nicely at the dispensing tip but does not release from the tip in Dynamic test mode Increase the droplet size to overcome the adhe...

Страница 38: ...the specimen warps when the liquid droplet is applied it might be necessary to attach the specimen strip to a flat surface with a suitable adhesive A 2 Detection of the droplet in Dynamic Mode The dis...

Страница 39: ...d tasks that are not necessary to run in parallel with the PG program You may also try to increase the refresh rate of the display screen and reduce the resolution of the display screen Please note th...

Страница 40: ...plet without air bubbles appears at the dispensing tip press and hold the PUMP button until pump stops i Set the volume selector on top of the instrument to 4 0 L which is the default droplet size for...

Страница 41: ...ing to 0 2 l at a target of 4 0 l If the average volume from six droplets is outside 5 from the target the droplet size can be adjusted with the procedure described below a Locate the volume adjustmen...

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