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Thermo Scientific

iCE 3000 Series Pre-Installation Requirements Guide (P/N 9499 500 30031, Version 1.6)

3-1

Chapter 3

System Accessories

Required Accessories

•

Data Station. See

Chapter 6, “Communications Interface”

Optional Accessories

•

Thermo Scientific™ GFS33 Graphite Furnace and Autosampler for
iCE™ 3300 AA spectrometer

•

Thermo Scientific™ SOLAAR Validator Package

•

Thermo Scientific™ SOLAAR

Security

Software

•

Thermo Scientific™ ID100 Auto Dilutor

•

Thermo Scientific™ VP100 Continuous Flow Vapor Generator
(includes T-Cell and Mercury Cell)

•

Thermo Scientific™ EC100 Electrically Heated Cell System

•

Thermo Scientific™ STAT (Slotted Tube Atom Trap) Accessory

•

Air Compressor KNF N035 (Series N 035 A_.18 Pumps,
Diaphragm Vacuum Pumps and Compressors, KNF Neuberger,
Inc.)

•

CETAC™ ASX-520 Autosampler (requires dedicated RS-232 on
Data Station)

•

CETAC™ ASX-260 Autosampler (requires dedicated RS-232 on
Data Station)

•

Thermo Scientific™ NESLAB ThermoFlex™ recirculating chiller

Request site requirement guides for any purchased accessories.

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Содержание Thermo Scientific iCE 3000 Series

Страница 1: ...iCE 3000 Series AA Spectrometers Pre Installation Requirements Guide 9499 500 30031 Version 1 6 March 2018 ...

Страница 2: ......

Страница 3: ...9499 500 30031 Version 1 6 March 2018 iCE 3000 Series AA Spectrometers Pre Installation Requirements Guide ...

Страница 4: ...struments Inc ThermoFlex is a trademark of Thermo Fisher Scientific Inc All other trademarks are the property of Thermo Fisher Scientific Inc and its subsidiaries Thermo Fisher Scientific Inc provides this document to its customers with a product purchase to use in the product operation This document is copyright protected and any reproduction of the whole or any part of this document is strictly ...

Страница 5: ...apter 3 System Accessories 3 1 Required Accessories 3 1 Optional Accessories 3 1 Chapter 4 Transportation 4 1 Package Size 4 2 Short Term Storage 4 3 Transit Damage 4 3 Warranty 4 3 Chapter 5 Working Area Requirements 5 1 Introduction 5 2 Location 5 3 Environmental Requirements 5 4 Electrical Requirements 5 4 Spectrometer Size 5 6 Gas Requirements 5 7 Acetylene 5 8 Air 5 9 Argon and Nitrogen 5 9 N...

Страница 6: ...Contents ii iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific Chapter 6 Communications Interface 6 1 Chapter 7 Special Agreements 7 1 ...

Страница 7: ...llation site of the iCE 3000 Series AA spectrometer and associated equipment Safety requirements for the installation are also detailed Thermo Scientific iCE 3000 Series AA spectrometers are designed to operate reliably under carefully controlled environmental conditions Operating a system or maintaining it in a condition outside the power and operating environment specifications described in this...

Страница 8: ...from the main flow of text Viewpoint Orientation The expressions left and right used in this manual always refer to the viewpoint of a person that is facing the front side of the instrument NOTICE Points out possible material damage data loss impaired data quality and other important information in connection with the instrument Tip Highlights helpful information that can make a task easier Always...

Страница 9: ...vity expressions such as choose File Directories are used rather than pull down the File menu and choose Directories Any command enclosed in angle brackets represents a single keystroke For example press F1 means press the key labeled F1 Any command that requires pressing two or more keys simultaneously is shown with a plus sign connecting the keys For example press Shift F1 means press and hold t...

Страница 10: ...n 1 6 Thermo Scientific Reference Documentation In addition to this guide Thermo Fisher Scientific provides other documents for the iCE 3000 Series AA spectrometers Reference documentation for the iCE 3000 Series spectrometers includes the following iCE 3000 Series Operating Manual This manual is provided on the software CD ...

Страница 11: ...1 With the serial number S N of your instrument request access on our customer SharePoint as a customer at www thermoscientific com Technicaldocumentation 2 For the first login you have to create an account Follow the instructions given on screen Accept the invitation within six days and log in with your created Microsoft password 3 Download current revisions of user manuals and other customer ori...

Страница 12: ...Using this Manual Contacting Us 1 6 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 13: ...ed equipment Safety requirements for the installation are also detailed The choice of an operating site for the instrument will be influenced by local considerations for example ease of access and availability of electrical power Logical planning of the installation can save both time and money The objective of this guide is to provide information that will enable the best site to be chosen and to...

Страница 14: ...Introduction 2 2 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 15: ... Thermo Scientific ID100 Auto Dilutor Thermo Scientific VP100 Continuous Flow Vapor Generator includes T Cell and Mercury Cell Thermo Scientific EC100 Electrically Heated Cell System Thermo Scientific STAT Slotted Tube Atom Trap Accessory Air Compressor KNF N035 Series N 035 A_ 18 Pumps Diaphragm Vacuum Pumps and Compressors KNF Neuberger Inc CETAC ASX 520 Autosampler requires dedicated RS 232 on ...

Страница 16: ...System Accessories Optional Accessories 3 2 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 17: ...area to the installation site must be checked for suitability The largest pallet size should be used to calculate clearances All items should be transported to the installation site on pallets in their original packaging and the right way up Under no circumstances may any package be moved without its pallet unless under the direct control of an authorized Thermo Fisher Scientific field service eng...

Страница 18: ...Depth Height Weight iCE 3500 1070 mm 42 2 in 740 mm 29 2 in 760 mm 30 in 64 kg 141 lbs iCE 3400 1070 mm 42 2 in 740 mm 29 2 in 760 mm 30 in 60 kg 132 lbs iCE 3300 660 mm 26 in 700 mm 27 6 in 760 mm 30 in 55 kg 121 lbs iCE 3300GF 660 mm 26 in 700 mm 27 6 in 760 mm 30 in 48 kg 106 lbs Table 4 2 Dimensions and weights of packed accessories Accessory Width Depth Height Weight Furnace 715 mm 28 2 in 55...

Страница 19: ...ome invalid Transit Damage Before accepting delivery of any equipment the packages should be inspected for signs of obvious damage The nature of the damage should be noted on the delivery notice and signed by the carrier s representative Within the time stated in the Thermo Fisher Scientific terms and conditions an inspection should be performed for concealed damage The local Thermo Fisher Scienti...

Страница 20: ...Transportation Warranty 4 4 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 21: ...ents Contents Introduction on page 5 2 Location on page 5 3 Environmental Requirements on page 5 4 Electrical Requirements on page 5 4 Spectrometer Size on page 5 6 Gas Requirements on page 5 7 Water Temperature Control on page 5 10 Waste Storage on page 5 11 Spectrometer Fume Extraction on page 5 12 Sample Fume Extraction on page 5 15 ...

Страница 22: ...ons specified The laboratory must offer dry even temperature and dust free conditions with no possibility of condensation forming Sample preparation activities and corrosive materials should be located in a separate room to avoid problems due to corrosive fumes A comprehensive risk assessment must be performed that is specific to the handling of solvents samples and sample preparation handling of ...

Страница 23: ...4 mm 480 mm Ensure that the exhaust is correctly positioned above the LH compartment flame EC100 T Cell or Mercury Cell and RH compartment furnace Make sure that the ventilation is on before igniting the flame using the EC100 T Cell or Mercury Cell or before firing the furnace Do not run any of those when the ventilation is turned off Organic or volatile solvents should not be stored even for a sh...

Страница 24: ...5 and 30 C and 20 to 60 m v for an ambient temperature between 30 and 40 C Atmospheric conditions must be non condensing The instrument room should be at a positive pressure with respect to rooms with a corrosive atmosphere Electrical Requirements The spectrometer will require an electrical supply at 100 to 240 VAC 300 VA 50 60 Hz The spectrometer will be supplied with a 2 m mains cord with USA ty...

Страница 25: ...cal requirements It must be possible to electrically isolate the instrumentation Table 5 1 Disconnection device and suitable fusing Disconnection device Fusing The disconnection device can be a switch or a circuit breaker It must comply with the following disconnect all current carrying conductors approved to IEC60947 1 and or IEC6947 3 rated 32 A or higher suitably located and easily reached mark...

Страница 26: ...re based on CETAC specifications for the ASX 520 family Table 5 3 Spectrometer dimensions and weights Spectrometer Width Depth Height Weight iCE 3500 780 mm 30 1 in 577 mm 22 7 in 520 mm 20 5 in 54 kg 119 lbs iCE 3400 780 mm 30 1 in 577 mm 22 7 in 520 mm 20 5 in 54 kg 119 lbs iCE 3300 567 mm 22 3 in 589 mm 23 2 in 510 mm 20 1 in 45 kg 99 lbs iCE 3300GF 567 mm 22 3 in 589 mm 23 2 in 510 mm 20 1 in ...

Страница 27: ...e use Only the gas tubing supplied with the spectrometer should be used The gas tubing supplied will terminate in 3 8 in BSP thread connections All gas supplies should be regulated and connected within 1 m of the instrument A comprehensive Risk Assessment must be performed that is specific to the gas requirements CETAC ASX 260 330 mm 13 in 508 mm 20 in 610 mm 24 in 8 4 kg 18 5 lbs CETAC ASX 520 52...

Страница 28: ...mits and in an environment free from naked lights or sparks NOTICE Acetylene is usually supplied in cylinders containing about 6 16 m3 220 ft3 of the gas dissolved in acetone As the acetylene is used the pressure in the cylinder decreases This can result in release of acetone that can lead to erratic results and possible instrument damage A cylinder must be considered exhausted at 7 bar 100 psi Th...

Страница 29: ...urnace requires argon or nitrogen gas at 1 04 bar 15 psi with a purity of 99 999 Argon gas is the preferred purge gas A vapor system requires a pressure of 0 34 bar 5 psi Nitrous Oxide A flame spectrometer may require nitrous oxide gas for some applications Nitrous oxide must be supplied at 2 75 bar 40 psi at a flow rate of 8 L min Special grade AA nitrous oxide must be used with the maximum impur...

Страница 30: ...Flex 900 230 V 50 Hz 7 A or 115 V 60 Hz 13 A 696 36 627 mm 27 4 14 2 24 7 in The furnace is supplied with plastic connecting tubing of 6 5 mm ID Connection to the water chiller should be within 3 m of the instrument If a greater distance is required insulated tubing must be used The water quality shall be distilled or deionized water of approximately 18 M cm3 Thermo Fisher Scientific does not reco...

Страница 31: ...tainer can cause the waste container to burst or the liquids in the waste container can return back to the flame compartment with a loud flashback Use only waste containers with a wide neck CAUTION Hazardous Mixture Risk of injuries The mixture in the waste container may be toxic and or corrosive and can be harmful in contact with the skin Pay attention to the Material Safety Data Sheets MSDS Stab...

Страница 32: ...ltering of hazardous toxic fumes No compounds that may form acetylides must be in contact with exhaust fumes Requirements of the Exhaust System The exhaust system must fulfill the following requirements Over the Flame The entire extraction system must not be made of flammable material The hood of the extraction system over the flame must have a circular cross section of at least 250 mm 10 in the t...

Страница 33: ...nstalling an automatic supervision of the air flow If it can be ensured that the flow rate is at least 10000 L min 355 ft3 min and or that only acetylene flames are used the distance between hood and fan can be reduced to 3 5 m The temperatures that effectively appear within the duct depend on several factors Therefore Thermo Fisher Scientific strongly recommends measuring the resulting temperatur...

Страница 34: ...ity of the analysis when increasing the flow to values beyond the specified minimum The upper limit of the flow rate may be determined by the point at which the signal is negatively impacted In particular an unnecessarily high flow rate may cause the flame to flicker and or to decrease the stability of the analytical data which will be reflected in higher relative standard deviations WARNING Hot S...

Страница 35: ...separate extraction should be considered if significant numbers of volatile or acidic samples are left in the proximity of the instrumentation even those in an autosampler Figure 5 2 Extraction positions iCE 3000 Series 250 mm 511 mm 150 mm 566 mm 588 mm 362 mm 150 to 230 mm 594 mm 788 mm Æ 250 Æ 150 Æ 80 Æ 110 360 mm 657 mm 529 mm The extraction system must not be affected by external weather con...

Страница 36: ...Working Area Requirements Sample Fume Extraction 5 16 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 37: ...sional Windows Vista Ultimate or Windows 7 Professional 20 GB hard drive 512 MB RAM An USB connection for spectrometer communication Some accessories require a dedicated RS 232 port A separate Ethernet card is required for networking A printer port may be required A suitable PC is available from your local Thermo Fisher Scientific organization The Thermo Fisher Scientific field service engineer is...

Страница 38: ...Communications Interface 6 2 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

Страница 39: ...ies Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 7 1 Chapter 7 Special Agreements This chapter should detail any special agreements which have been arranged with your local Thermo Fisher Scientific organization ...

Страница 40: ...Special Agreements 7 2 iCE 3000 Series Pre Installation Requirements Guide P N 9499 500 30031 Version 1 6 Thermo Scientific ...

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