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GENERAL INFORMATION 

 

The TBS Solvent Recovery System is designed for recovering solvents used in Histopathology with a boiling 
point between 50 - 180° C.  Using a closed system with  fractional distillation design, the Solvent Recovery 
System can be operated simply and safely. 
 
This Manual - Reading this manual is essential for correct and safe use of this equipment. 
 
Application - The TBS Solvent Recovery System will successfully and economically recover most solvents 
used for dehydration, extraction of fat and as an inter medium (Xylene, acetone, ethanol, toluene, etc.). 
 
Function - The waste solvents, distilland from tissue processors and/or tissue stainers, are heated inside the 
distillation vessel of the recycler, converted to vapor and then condensed back into a liquid.  A thermostat 
and a timer will control the process.  The vaporized solvent is directed through a collection pipe to an air 
cooled distilling condenser where the vapor is condensed back into liquid.  The distillate is then collected in 
a closed container on the outside of the unit. The recovery rate of the solvent will depend on the grade of 
contamination of the waste solvent being recycled. 
 
Separation Module - The TBS Solvent Recovery System utilizes the principle of Simple Distillation, 
however, it will achieve the results of Fractional Distillation using the Separation Module and Baffle.  The 
Switching Module allows an operator to set a fraction temperature at which the distillate of the different 
solvents will be separated.  The fraction temperature is set relative to the boiling point of the solvent you 
wish to recover.  This fraction temperature is easily set at the beginning of each  recovery cycle. 
 
Safety Measures - TBS Solvent Recovery Systems work ONLY with atmospheric pressure.  Should the 
thermal oil temperature exceed the maximum set value of the working thermostat by more than 25°C or if a 
defective cooling fan allows the distillate to emerge at a temperature higher than 40°C (104°F), the 
distillation process will be interrupted by a complete and total shut down of the unit.  The unit will shutdown 
if the Thermal Oil temperature exceeds 225°C. 
 
TBS solvent Recovery Systems have been extensively tested and approved by the ETL Testing Laboratories 

 

  

 

OPERATIONAL SAFETY 

 

General

 - TBS Solvent Recovery Systems adhere to ETL guidelines for safety and manufacturing. It is 

suggested that your laboratory purchase an appropriate fire extinguisher to be placed within ten feet of any 

electrically heated equipment. 

 

TBS recommends that the Safety Officer for your facility be contacted for proper storage and disposal of any 

hazardous substance being recycled. 

 

Location

 - It will be necessary for to contact the Environmental health and Safety Officer and the local fire 

marshal regarding placement recommendations for your Solvent Recovery System.  

 

Содержание SR12

Страница 1: ...Triangle Biomedical Sciences Inc Solvent Recovery System Operation And Service Manual SR12 Version 1 2 Serial ___________________...

Страница 2: ...ION 4 Application 4 Function 4 Separation Module 4 Safety Measurers 4 OPERATIONAL SAFETY 4 Location 4 Solvent Containment 4 Safe Exposure Temperature 5 OPERATING PROCEDURES 6 Purpose 6 Procedure for A...

Страница 3: ...Page 3 GLOSSARY 15...

Страница 4: ...ansfer the benefit of such warranties to the user This warranty supersedes and is given in lieu of all implied warranties and is void if user does not provide unit with continuous ample electrical pow...

Страница 5: ...illation using the Separation Module and Baffle The Switching Module allows an operator to set a fraction temperature at which the distillate of the different solvents will be separated The fraction t...

Страница 6: ...on the floor under your recovery unit This pan is recommended for use as a safety pan to prevent solvents from spilling onto the floors in case of an over flow due to operator error Appropriate 3 gal...

Страница 7: ...taminated solvent in the distilling chamber up to 3 gallons NOTE Take special care NOT to allow any contaminated solvent to enter the Vapor Collector Duct Manifold when you are filling the distilling...

Страница 8: ...hen operating This could create a dangerous situation Xylene 1 Place clean and dry collection containers under each of the lower distillate solvent outlet nozzles left and right 2 Verify that the Ther...

Страница 9: ...overy cycle has been completed let the unit cool to at least 50 C prior to opening the secured top Premature opening will allow a release of solvent fumes into the surrounding atmosphere and can also...

Страница 10: ...156 377 Cyclohexane 81 260 Cyclohexanon 155 419 1 2 DiChlorethane 84 412 DiEthyl Cellosolve 121 208 DiEthyl Ketone 104 445 Ethanol 82 400 Ethyl Acetate 79 427 Ethyl Amyl Keytone EAK 160 Ethylene Glyc...

Страница 11: ...113 46 80 Carbon Tetrachloride Tetrachloromethane 78 110 1 1 2 2 Tetrachloroethane Acetylene Tetrachloride 147 160 Tetrachloroethylene Pestabil Vors Perchloroethylene Per 121 150 Trichloroethane 1 1...

Страница 12: ...o control the temperature of the thermal oil that transfers heat to the distilling chamber Range 40 200 C Note The oil temperature is generally 15 20 C higher than the temperature of the contaminated...

Страница 13: ...time lasts much longer than 4 hours 1 Contaminated solvent contains too much water 2 Thermal oil level is low 3 Thermal oil is old and dirty 4 Heating elements need cleaning 1 Replace the solvent 2 Ad...

Страница 14: ...er 11 Cooling Fan Motor Expl Proof 12 3 Way Fraction Switch Expl Prf 13 Heater Cable Sheath Pipe Expl Prf 14 Solvent Receiver Tanks 15 Solvent 16 Oil Discharge 17 Thermal Oil Level Indicator 18 Workin...

Страница 15: ...g Thermostat T1 384010 Safety Thermostat T2 465000 White Warning Light 465001 Red Warning Light 465002 Green Warning Light 475000 Ventilator Motor 468402 Heating Element 385007 Timer 425002 Control Kn...

Страница 16: ...since the distlland mixture is forced into the area in which only pure material is desired Fraction A portion of the collected separated material recovered from the head of the still Fractional Disti...

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