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6875D Freezer/Mill
1300-87052-1A, REV 1
SPEX SamplePrep LLC
Page 3 of 36
TABLE OF CONTENTS
SECTION
DESCRIPTION
PAGE
1.0
Introduction ........................................................................................................................ 4
2.0
Specifications ...................................................................................................................... 5
3.0
Unpacking ........................................................................................................................... 6
4.0
Setting Up ............................................................................................................................ 7
4.1
Electrical Connection ......................................................................................................... 7
4.2
Power Switch and Controller ............................................................................................ 8
4.3
Liquid Nitrogen
Connection………………………………………………………………………………………….9
4.4
Lid, Coil Assembly and Gate, LN Sensor ........................................................................... 10
4.5
Grinding Vial Sizes, Adapters, and Vial Openers ............................................................ 11
5.0
Touchscreen Display ......................................................................................................... 12
5.1
Logo Screen ....................................................................................................................... 12
5.2
Control Panel..................................................................................................................... 13
5.3
Changing Settings.............................................................................................................. 17
5.4
Saved Protocols ................................................................................................................. 18
6.0
Operation .......................................................................................................................... 20
6.1
Standard Auto Fill………………………………………………………………………………………………………20
6.2
Manually Adding Liquid Nitrogen ..................................................................................... 21
6.3
Loading Vials into the Freezer/Mill................................................................................... 24
6.4
Removing Vials from the Freezer/Mill.............................................................................. 24
6.5
Opening, Emptying, and Cleaning Freezer/Mill Vials ....................................................... 24
6.6
Checking the Liquid Nitrogen Level .................................................................................. 27
7.0
Resources .......................................................................................................................... 27
7.1
Run History………………………………………………………………………………………………………………..27
7.2
Accessories (Electronic Version)…………………………………………………………………………………28
7.3
Training………….………………………………………………………………………………………………………….29
7.4
System Settings
…………………….…………………………………………………………………………………..30
7.5
Technical Support………….…………………………………………………………………………………………..30
8.0
Maintenance……………………………………………………………………………………………………………..3
1
9.0
Trouble-Shooting Guide .................................................................................................... 32
10.0
Warranty ........................................................................................................................... 34
10.1
Product Specifications ...................................................................................................... 34
10.2
To Arrange a Return Shipment ......................................................................................... 34
11.0
Instrument Disposal .......................................................................................................... 35
12.0
Contact Us ......................................................................................................................... 36