Shimadzu TOC-V CPH Скачать руководство пользователя страница 12

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TOCV-CP_IMshort_Control-ver-2_Rev07F

Page 12 of 22

(Software version ≥ 2.00)

effective date: September 2007

Overview about several possibilities to create a Calibration Curve:

Wizard -2

Calibration curve

type

Calibration points are
distributed uniformly over
concentration range

Edit calibration curve
point manually

Calibration curve
according to
DIN 38402/P-51

Calibration curve according to
USP/EP

Application

Normal calibration curve, data
points are added
automatically, helps by
multiple point calibration
curve

Normal calibration
curve, data points are
added manually

!Normally used!

Special calibration curve:
always10 points, first point
and last point are injected
10times all other points only
one time; Linearity and
homogeneity are calculated

Special calibration curve:
Always 2 points:
0 and 500ppb
(United States Pharmacopoeia or
European Pharmacopoeia

Wizard -3

Same

Wizard -4

Units
Concentration range
No. of Cal points
No of Injections
No of Washes
SD Max
CV Max
Sparge time
Acid addition

Selectable default: ppm

Enter range: e.g 0-5
Enter No of Points: e.g.

Selectable (1/20)
Selectable (0-10)
Selectable (0-9999)
Selectable (0-100%)
Selectable (0-20min)
Selectable (0-20%)

Selectable default: ppm

Disable
Disable

Selectable (1/20)
Selectable (0-10)
Selectable (0-9999)
Selectable (0-100%)
Selectable (0-20min)
Selectable (0-20%)

Selectable default: ppm

Enter range: e.g. 10-100
Recommended: 10
Recommended: 1

Selectable (0-10)

Disable
Disable

Selectable (0-20min)
Selectable (0-20%)

Recommended: ppb

Fixed conc. range:0-500

Fixed No. of Cal. Points: 2

Selectable (1/20)
Selectable (0-10)
Selectable (0-9999)
Selectable (0-100%)
Selectable (0-20min)
Selectable (0-20%)

Wizard -5

Calib. Points list
Inj. Volume
Calibration Points

Recommended value

Example:

0ppm

5ppm

10ppm

Calculated automatic.

Empty calibration
points list. Manually
filling via [ADD]

Recommended value

List of 10 calibration points
in the range from 10 – 100
(as example)

Recommended value

List: 0ppb

500ppb

Wizard -6

Same

Содержание TOC-V CPH

Страница 1: ...SHIMADZU TOC V Series TOTAL ORGANIC CARBON ANALYSER Short User Manual TOC V CPH CPN TOC Control V Version 2 00 ...

Страница 2: ...n 2 4 Others II Sample Table Editor 1 Create a calibration curve 2 Create a method 3 Create a sample run 4 Schedule File 4 1 Create a new schedule file 4 2 Export the sample table as schedule file 4 3 Insert a schedule 5 Vial Number III Analysis 1 Connect the system 2 Start the analysis 3 Sample Window 4 Edit Mode 5 Stop the analysis 3 3 3 3 5 6 6 6 6 7 8 9 13 15 18 18 18 18 19 20 20 20 21 22 22 ...

Страница 3: ... user name and password Sample Table Editor Sample Table Editor opens to start the TOC instrument 1 2 H W Settings to configure a new system to view or modify the instrument settings Parameter Action Description Start Click on the H W Settings button User Name Password Enter exact user name and password H W Settings H W Settings opens 1 2 1 New System to configure a new instrument Parameter Action...

Страница 4: ...a buzzer will sound with the press of each instrument key Auto regeneration of IC solution If this item is selected IC reagent will automatically be generated in special situations Please refer to the User Manual Enable ready status check Select this option to enable the Ready Status Check function recommended thus software always verifies Ready Status of instrument prior to starting measurement T...

Страница 5: ...e edited by the user determined by the hardware automatically set based on Com Port Finish Button The system configuration is created and the newly created system configuration is displayed as an icon in the H W Setting List window 1 2 2 H W Setting List to view or modify instrument parameters of already defined systems Parameter Action Description Open Select the Instrument System icon and press ...

Страница 6: ... Add a Log Event to add an event to the Log Browser 2 3 User Authentication 2 3 1 User Account to create new user to edit user information of already registered users to deactivate accounts Parameter Action Description Start Click on User Accounts User Name Password Enter exact user name and password first time Admin no password New User Select User New Change existing user accounts Select User Ed...

Страница 7: ...at a user can access Each of the four user levels has a default list of access rights displayed in this field The administrator can use this list to add or remove access rights for main user user and guests Please refer to the Administration Menu OK Click on the OK button to create a new account 2 3 2 Change Password to change the password of user ID 2 4 Others 2 4 1 LIMS Settings The LIMS related...

Страница 8: ...indows design 1 Menu bar 2 Tool bar for the file 3 Tool bar for the instrument 4 Status indication for instrument 5 File viewer for Sample tables Calibration curves Methods Control samples and Schedule files 6 Tabs to change the file viewer 7 Output bar 8 Status bar with name of the Login 9 Sample table name of the sample table file in the header 10 Display of the sample information according to t...

Страница 9: ...oints manually Select the option to enter the calibration point concentration manually on a subsequent Wizard page the calibration Points list Calibration Curve according to DIN 38402 P 51 Select this option to create a calibration curve according to DIN 38402 This type consists 10 calibration points with 10 injections of the lowest and highest standards and a single injection of the intermediates...

Страница 10: ...nts Enter the number of calibration standards No of Injections Enter the minimum maximum number of injections for the standards No of Washes Enter the number of times the syringes is washed with sample SD Max Enter the standard deviation limit This limit is used to assess the analysis result CV Max Enter the coefficient of variation limit This limit is used to assess the analysis result Sparge Tim...

Страница 11: ...lation coefficient If the calibration curve contains less than 3 calibration points error judgement is not possible and this option will have no effect Failure Action 1st time Continue Stop Repeat Select the process to be conducted if an error occurs Records the error and continue the measurement Records the error and stops analysis Records the error and re analyse the calibration curve Failure Ac...

Страница 12: ...ame Same Wizard 4 Units Concentration range No of Cal points No of Injections No of Washes SD Max CV Max Sparge time Acid addition Selectable default ppm Enter range e g 0 5 Enter No of Points e g 3 Selectable 1 20 Selectable 0 10 Selectable 0 9999 Selectable 0 100 Selectable 0 20min Selectable 0 20 Selectable default ppm Disable Disable Selectable 1 20 Selectable 0 10 Selectable 0 9999 Selectable...

Страница 13: ... The entered value will be used in the concentration calculation No of Determinations Enter the number of times each sample is to be measured This means determination of same sample in different vials Enable disable USP EP Select this item to ensure that the results are compliant to the USP EP standard File Name Enter a method file name Method Wizard 3 Calibration Curve Parameter Action Descriptio...

Страница 14: ...r NPOC analysis Acid Addition Enter the percentage of acid to be added to the sample Multiple Injections If this item is selected multiple injections are made from a single sample aliquot This larger aliquot is drawn in the syringe in one aspiration and is sufficient to accommodate all of the repeat injections Use blank check area If selected the blank check value is subtracted from the analysis r...

Страница 15: ...on Description Method To create the sample group using measurement parameters from a specified method Enter the desired method or select the method using the Browse button Calibration Curve To create the sample group using the measurement parameters from a specified calibration curve Enter the desired calibration curve or select the curve using the Browse button Edit parameters manually To insert ...

Страница 16: ...btained from the method or calibration curve identified in page 1 Enter other name if desired Index Start Select this option to start counting index Each sample added receives an increased counting index number Insert Cal Curve Control Samples Select this option to insert calibration curves and control samples alon with the samples Click Finish to insert the group of samples into the sample table ...

Страница 17: ...ginning of the sample group Select this item to insert a control sample before the sample analysis Always after number of samples Select this item to inert a control sample after every fixed number of samples Enter that number in the box At the end of the sample group Select this item to insert a control sample at the end of the sample analysis Control Templates Displays the information related to...

Страница 18: ...able Editor Enter information in the schedule in the same manner as in the Sample Table Enter the vial information by clicking the button Save the Schedule file in the schedule folder 4 2 Export the Sample table as Schedule File The Contents of a sample table can be exported as a Schedule file The Schedule file can be exported in either sample table format or text format Click File Export Schedule...

Страница 19: ...ection volume exceed the capacity the vial is marked red Vial is displayed if the total injection volume exceeds the vial capacity Acid addition Select a vial in the drawing to display the percent of acid to be added to the vial Sparge Time Select a vial in the drawing to display the length of time sparging will be conducted in that vial Required Sample Amt Select a vial in the drawing to display ...

Страница 20: ...played Keep running The instrument remains in the Ready state at the completion of the analysis sequence even after analysis is completed Shut down instrument The instrument automatically turns off at the completion of the analysis sequence Sleep The instrument enters the sleep state and restarts at a specified date and time Auto restart time To set the restart time Standby To verify the settings ...

Страница 21: ...on Description Graph Current Peak All Peaks Calibration Curve Displays the peak profile of the highlighted injection Displays all injection peaks for the selected sample Displays calibration curve for calibration standards only This function is not available during real time analysis Parameter Table Displays the sample parameter of measured sample Injection Table Displays the result of the injecti...

Страница 22: ... be conducted Adding and deleting samples Changing analysis parameters and vial numbers Printing reports for samples that are already analysed Click Start button to cancel the Edit Mode and restart analysis 5 Stop of Measurement Parameters Action Description Stop of Measurement Select Stop in Instrument menu Peak Stop This option interrupts processing of the current injection and analysis proceeds...

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