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18

 

 

2.

  

set

 

the

 

ramp

 

rate,

  

3.

  

set

 

a

 

new

 

target

 

temperature

 

(command

 

class

 

5).

 

The

 

target

 

temperature

 

may

 

be

 

above

 

or

 

below

 

the

 

current

 

temperature;

 

as

 

soon

 

as

 

it

 

is

 

set,

 

the

 

ramp

 

will

 

begin,

 

up

 

or

 

down,

 

to

 

that

 

new

 

target.

 

After

 

reaching

 

the

 

target,

 

the

 

controller

 

will

 

hold

 

at

 

that

 

temperature.

  

At

 

any

 

time

 

a

 

new

 

ramp

 

rate

 

and

 

target

 

temperature

 

can

 

be

 

set

 

to

 

start

 

a

 

new

 

ramp.

 

Once

 

you

 

are

 

done,

 

set

 

the

 

ramp

 

rate

 

to

 

0.

  

Otherwise,

 

setting

 

a

 

new

 

target

 

temperature

 

later

 

will

 

initiate

 

a

 

ramp

 

to

 

that

 

target

 

temperature.

 

 

Notes:

   

 

The

 

minimum

 

settable

 

ramp

 

rate

 

is

 

0.01

 

°C/minute.

 

 

For

 

higher

 

ramp

 

settings,

 

the

 

observed

 

rate

 

may

 

be

 

lower

 

than

 

that

 

calculated

 

from

 

RT

 

and

 

RS

 

or

 

it

 

may

 

be

 

nonlinear

 

over

 

part

 

of

 

the

 

temperature

 

range

 

because

 

the

 

maximum

 

possible

 

rate

 

of

 

heating

 

or

 

cooling

 

is

 

limited

 

(and

 

dependent

 

on

 

the

 

ramp

 

direction

 

as

 

well

 

as

 

on

 

the

 

temperature).

 

 

When

 

the

 

ramping

 

process

 

is

 

completed

 

the

 

controller

 

will

 

send

 

a

 

response

 

of

 

the

 

form

 

[F1

 

TT

 

#]

 

as

 

a

 

notification

 

of

 

the

 

end

 

of

 

the

 

ramp.

  

This

 

response

 

can

 

be

 

blocked

 

at

 

any

 

time

 

by

 

previously

 

sending

 

the

 

command

 

[F1

 

TT

 ‐

]

 

(see

 

command

 

class

 

5).

 

 

 

 

 

 

 

 

 

 

 

 

 

11.

 

 

Heat

 

Exchanger

 

Temperature

 

 
[F1 HL ?]

 

What

 

is

 

the

 

high

 

temperature

 

limit

 

for

 

the

 

heat

 

exchanger?

 

......[F1 HT 60]

 

The

 

heat

 

exchanger

 

high

 

temperature

 

limit

 

is

 

60

 

ºC.

 

[F1 HT ?]

 

What

 

is

 

the

 

current

 

temperature

 

of

 

the

 

heat

 

exchanger?

 

 

 

......[F1 HT 39]

 

The

 

current

 

heat

 

exchanger

 

temperature

 

is

 

39

 

ºC.

 

[F1 HT +3] 

Start

 

periodic

 

heat

 

exchanger

 

temperature

 

reports

 

every

 

3

 

seconds.

 

[F1 HT -] 

Stop

 

periodic

 

heat

 

exchanger

 

temperature

 

reports.

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 
 

 

 

 

 

 

12.

  

Cell

 

Changing

 

 

These

 

commands

 

will

 

have

 

an

 

effect

 

only

 

for

 

a

 

sample

 

holder

 

with

 

multiple

 

cuvette

 

positions.

 

 
[F2 DI] 

Device

 

initialize:

 

move

 

to

 

home

 

position.

 

[F2 PI] 

Device

 

initialize:

 

move

 

to

 

home

 

position

 

and

 

reply

 

when

 

 

  

done.

 

......[F2 DL 1] 

Device

 

is

 

finished

 

moving.

  

(Original

 

reply

 

was

 

OK

 

rather

 

than

 

DL

 

1)

 

[F2 DL 3] 

Device

 

locate:

 

move

 

to

 

position

 

3.

  

(Device

 

should

 

be

 

 

  

initialized

 

prior

 

to

 

using

 

this

 

command

 

for

 

the

 

first

 

time.)

   

[F2 PI] 

Device

 

initialize:

 

move

 

to

 

home,

 

then

 

to

 

position

 

1

 

and

 

reply

 

when

 

 

  

done.

 

......[F2 DL 1] 

Device

 

is

 

in

 

position

 

1.

 

Содержание Turret 6

Страница 1: ...19 8606 Tel 509 624 9290 Fax 509 624 9488 E mail quantum qnw com Web www qnw com Turret 6 6 Position Temperature Controlled Cuvette Turret for UV Vis Spectrophotometry Manual Product Overview 3 18 201...

Страница 2: ...g the MenU BUTTON 6 3 Features of the Turret 6 8 A GENERAL DESCRIPTION 8 B CUVETTE HOLDER 9 C CUVETTE Z HEIGHT 9 E COOLING WATER FOR THE PELTIER 10 F DRY GAS TO MINIMIZE CONDENSATION 11 G EXTERNAL TEM...

Страница 3: ...spectrophotometer 2 TC 1 Temperature Controller 3 power cable 4 USB cable 5 6 magnetic stir bars 6 vinyl tubing to connect water and gas B DEPENDING ON YOUR ORDER THE SHIPMENT MAY ALSO CONTAIN BATH 1...

Страница 4: ...to the back of the TC 1 Temperature Controller on the 15 pin connectors labeled Sample and reference 5 Plug the power cable into the back of the TC 1 Temperature Controller and into a wall socket The...

Страница 5: ...age push the left arrow once to get to the Set Position page Once there use the top and bottom arrows to choose a position e g position 5 Press the SET button The cuvette holder will move to position...

Страница 6: ...lowly When it has locked onto a new target temperature the green LED will remain lit A rapidly flashing red LED usually means a loose electrical cable or inadequate water flow for the Peltier unit Not...

Страница 7: ...own arrows and press SET The page will update to show the Current rate in min to be the same as the Ramp rate With ramping set turning on temperature control will generate a linear ramp to the target...

Страница 8: ...to six cuvettes The center of the tower is hollow permitting light to pass into the entrance hole through the tower through a cuvette and exit the opposite side from the entrance A plastic cover enclo...

Страница 9: ...be light tight CAUTION Accidently attaching a water line to the dry gas barb will severely damage the instrument Attach the lines with care B CUVETTE HOLDER The Turret 6 holds standard 10 x 10 mm cuve...

Страница 10: ...tap for brief use You will need a flow of 100 300 ml minute This flow should require a pressure of about 3 5 psi 0 2 0 3 bar Do not exceed an input water pressure of 25 psi 1 7 bar as damage may occu...

Страница 11: ...to temperature changes Also the fine coiled wires of the YSI 423 conduct very little ambient heat to the thermistor at the end Excellent Series 500 probes can be obtained with diameters less than a mm...

Страница 12: ...he temperature controller is not receiving a reasonable response from the sensor on the heat exchanger Either the sensor has failed or a cable is not making a good connection E8 inadequate coolant war...

Страница 13: ...10 C temperature precision 0 05 C cuvette size outside dimensions 12 5 x 12 5 mm minimum cuvette height 30 mm magnetic stirring speed 0 to 1700 rpm cuvette z height 8 5 or 15 mm specified when orderin...

Страница 14: ...be established through a USB connection between the computer and the controller In this case the controller includes electronics which convert the USB connection to a serial communications port Howeve...

Страница 15: ...stirrer speed F1 MS 300 The lowest stirrer speed is 300 rpm F1 SS S 1000 Set stirrer speed to 1000 rpm F1 SS S 0 Turn stirrer off and set the speed to zero F1 SS Turn stirrer on and set it to the most...

Страница 16: ...us F1 IS R The controller has been powered off and back on again 7 Current Sample Temperature F1 CT What is the current temperature of the holder F1 CT 22 84 The current temperature is 22 84 C F1 CT 3...

Страница 17: ...n F1 PA Start automatic reporting of probe temperature every temperature increment set by the command above F1 PT 30 5 The current probe temperature is 30 5 degrees F1 PA Stop automatic reporting of p...

Страница 18: ...l send a response of the form F1 TT as a notification of the end of the ramp This response can be blocked at any time by previously sending the command F1 TT see command class 5 11 Heat Exchanger Temp...

Страница 19: ...buttons and the display on the front When a computer program is in use the TC 1 will automatically send reports to the program whenever a manual change has been made The commands in this section are i...

Страница 20: ...20 R1 TT R Stop reporting manual changes for the reference target temperature R1 RR R Stop reporting manual changes for the reference ramp...

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