Parr Instrument 4703 Скачать руководство пользователя страница 8

General Purpose Pressure Vessels

P a r r   I n s t r u m e n t   C o m p a n y

8

Vessels with a Flat PTFE or Flexible Graphite Gasket 

The closure bolts may be tightened using either an 
open-end wrench for smaller vessels where the bolt 
torque requirement is less or with a torque wrench 
where additional loading is required for the higher 
operating pressures.  Unless otherwise note on 
documentation accompanying the product, recom-
mended torque values are shown alongside respec-
tive model numbers in subsequent pages on this 
operating instruction manual.

It is important to make sure that the bolts are 
periodically lubricated with a high-temp anti-seize 
compound to insure that they move freely so that 
the desired torque value is obtained in the tighten-
ing procedure.

It is also important to insure that there is uniform 
loading on all of the bolts.   Make sure that the head 
sits level on the cylinder.  Install the split ring and 
tighten all bolts finger tight.

Pick a starting position and tighten the bolt to 5 or 10 
ft-lbs depending on the maximum amount of torque 
to be applied.  For those vessels with a maximum 
torque requirement of 15 ft-lbs, a 5 ft-lb increment 
is appropriate.  For vessels with a maximum of 135 
ft-lbs, 20 ft-lb increments may be used.

Bolt tightening should continue in a criss-cross 
pattern from the initial bolt with the second bolt 180 
degrees from the first and continuing until all bolts 
are tightened.  Repeat this procedure increasing the 
torque to the required level.  

For vessels with PTFE Flat Gasket, after recom-
mended torque value is reached, let the vessel 
stand for about five minutes then re-tighten again to 
recommended torque value. This will compensate 
for any tendency of the PTFE gasket to flow under 
the loading.

Note: 

 It may be possible to extend the life of 

the Flexible Graphite gasket by coating both 

sealing surfaces of the head and cylinder as 

well as the gasket itself with a silicone base 

lubricant. Additionally, it helps to rough up 

the cylinder lip with 120 grit sandpaper to 

insure that the gasket remains in the head 

recess and does not stick to the cylinder.

Vessels with a Metal Gasket

Pressure vessels with a metal gasket require a 
uniform loading on the gasket carefully applied by 
tightening a ring of compression bolts with a torque 
wrench.  The amount of torque to be applied will 
vary with different vessels and with the intended 
maximum working pressure.  Specific sealing 
instructions will be provided for any Parr pressure 
vessels with a metal gasket furnished on special 
order.

Sealing 4740 High Pressure Vessels

Closing operations for the 1.0 inch I.D., Series 4740 
high pressure vessels are similar to those described 
for larger vessels with flexible graphite gaskets, 
except on the 4740 Series the compression screws 
are carried in a screw cap instead of in a split ring.  
When closing a 4740, clamp the cylinder in a vise; 
check the graphite gasket to be sure that it fits 
properly in the head groove; set the head on the 
cylinder and add the compression ring.  Check the 
screw cap to be sure that the six screws have been 
turned back so that they do not project through the 
cap, and then screw the cap onto the cylinder.  Turn 
it down as far as it will go, then back it off about 1/8 
turn.  Now, tighten the screws with a torque wrench 
with an initial 10 ft-lbs using the criss-cross pattern 
described for larger vessels.  After all have been 
tightened to 10 ft-lbs, repeat the procedure, increas-
ing the torque until all have been tightened to the 
recommended 15 ft-lb limit.

Содержание 4703

Страница 1: ...239M 4600 4700 General Purpose Pressure Vessels Operating Instruction Manual...

Страница 2: ...e Block Assemblies 9 Pressure Gages 9 Safety Rupture Discs 9 Coned Pressure Fittings 9 Tapered Pipe Threads 10 MAINTENANCE 10 General Maintenance Notes 10 Periodic Pressure Tests 11 HEAD ASSEMBLY GUID...

Страница 3: ...Assurance Certification Intended Usage This system has been designed for use as a high pressure reactor system It has been designed built and tested to strict physical and electrical standards However...

Страница 4: ...e deliver ing carriers The vessel motor heater and tem perature controller may be packed separately for convenience in shipping but these parts are easily reassembled Examine the components closely fo...

Страница 5: ...hout a pressure venting device it is the cus tomer s responsibility to provide pressure relief in order to protect the operator and the equip ment from destructive high pressures If you need more info...

Страница 6: ...mL Vessel with Split Ring Closure and 4316 Gage Block Assembly 2 Before Closing the Vessel examine the head seal carefully to be sure that it is in good condition The seal should not have any nicks or...

Страница 7: ...ded choice for many applications since PTFE materi als are inert to most chemicals PTFE gaskets will provide good seals under repeated opening and closing of the vessel if the gasket temperature does...

Страница 8: ...lue This will compensate for any tendency of the PTFE gasket to flow under the loading Note It may be possible to extend the life of the Flexible Graphite gasket by coating both sealing surfaces of th...

Страница 9: ...e connections Gages constructed of Alloy 400 are available on special order Safety Rupture Discs Detailed instructions for the safety rupture disc installed in Parr gage blocks and heads are provided...

Страница 10: ...ring and pres sure connections for excessive corrosion Sus pect parts should be replaced by components only supplied by Parr Instrument Company 2 Always use appropriate wrenches on all fittings and va...

Страница 11: ...t regular intervals during the life of each cylinder and particularly whenever the user suspects that the equipment has been over stressed or damaged Some laboratories maintain hydraulic test faciliti...

Страница 12: ...ns for Alloys other thanT316SS For parts made from alternate materials use the codes shown below as a suffix to the standard part number CM Alloy 400 CC Alloy 20Cb3 CH Alloy C 276 CT Alloy 600 CAD Tit...

Страница 13: ...l fittings per page 12 Recommended BoltTorque PTFE Gasket 500 PSI 15 ft lbs 1000 PSI 20 ft lbs 1500 PSI 30 ft lbs 1700 PSI 40 ft lbs Part No Description Flat Gasket Seal 7AC7 Head A socket 7AC8 Head o...

Страница 14: ...l fittings per page 12 Required for maximum working pressure of 7900 psi 544 bar at 538 C for vessel of T316SS Part No Description Flat Gasket Seal 1827HC Head A Socket opening A1828HC Cylinder 75 mL...

Страница 15: ...Head two 1 8 NPT 428HC11 Head A socket 1 8 NPT 428HC22 Head A socket 1 8 NPT for thermowell 425HC Cylinder 125 mL 4 44 deep 425HC3 Cylinder 200 mL 6 94 deep 429HC2 Gasket PTFE 429HC2KL Gasket Flexibl...

Страница 16: ...et 25 ft lbs Flexible Graphite 35 ft lbs Part No Description Flat Gasket Seal 453HC Head A Socket opening 453HC5 Head A Socket 1 8 NPT 453HC79 Head A Socket 1 8 NPT for thermowell 818HC45 Head VGR 452...

Страница 17: ...A122VB STRAIGHT VALVE 526HC SERIES R D 832HC4 DIP TUBE W NUT 836HC GAGE ADAPTER 818HC45 HEAD 452HC CYLINDER 300mL 288VBAD MALE CONNECTOR 366VBA_ HEX COUPLING A455HC SPLIT RING ASSY 457HC2 GASKET 454HC...

Страница 18: ...CE orders Maximum WorkingTemperature with FKM O ring with FFKM O ring 225 C 300 C Part No Description O ring Seal 2321HC2 Head A socket opening 2321HC3 Head A socket 1 8 NPT 2340HC11 Head VGR 2342HC...

Страница 19: ...T RING ASSY A456HC DROP BAND W SCREW 2341HCJV O RING 832HC4 DIP TUBE W NUT 288VBAD MALE CONNECTOR A472E THERMOCOUPLE 366VBA_ HEX COUPLING A888HC2 R D HOLDER ASSY 2342HC CYLINDER 300mL A122VB STRAIGHT...

Страница 20: ...429HC2KL Gasket Flexible Graphite 454HC Compression Ring A455HC Split Ring A456HC Drop Band 232HCFDE Bolt for Split Ring 1443HC2 DIP TUBE 50mL 1443HC DIP TUBE 25mL 593HC SERIES PRESSURE GAGE 836HC GAG...

Страница 21: ...i A122VB Valve Straight 1 8 NPT M Recommended BoltTorque PTFE or Flexible Graphite 15 ft lbs max Part No Description A146VB Valve Angle 1 8 NPT M A472E4 Thermocouple 5 1 2 A472E Thermocouple 7 1 2 A83...

Страница 22: ...ng Limits Maximum Working Pressure T316SS 1900 psi 131 bar Maximum WorkingTemperature with PTFE confined flat gasket 350 C Recommended BoltTorque PTFE Gasket 25 ft lbs Flexible Graphite 35 ft lbs Note...

Страница 23: ...hermowell for 2000 mL vessel 265HC7 Thermowell for 1000 mL vessel 48HC Thermowell Gasket silver 48HCCN Thermowell Gasket nickel 48HCFG Thermowell Gasket gold plated A472E2 Thermocouple 9 1 2 1000mL A4...

Страница 24: ...0mL Part No Description Flat Gasket Seal 2330HC12 Head B socket 2330HC13 Head B socket thermowell 2300HC19 Head VGR thermowell 2302HC Cylinder 600 mL 2302HC10 Cylinder 1200 mL 2304HC Compression Ring...

Страница 25: ...e ratings please consult Parr Instrument Company Series 4650 Model Size Head Style 4651 250 mL VGR thermowell 4652 500 mL VGR thermowell 4653 1000 mL VGR thermowell Working Limits Maximum Working Pres...

Страница 26: ...1 4 NPT M A129VB Valve Straight 1 4 NPT M X 1 4 T A147VB Valve Straight 1 4 NPT M 658HC Valve Extension 208HC15 Gage Adapter 2 1 4 NPTF 94CA Plug Hex Head 1 4 NPT Brass 686HC DipTube 1 G 686HC3 DipTub...

Страница 27: ...AngleValve 1 4 NPT M A147VB Valve Straight 1 4 NPT M A707HC2 Rupture Disc Assembly See Manual 231M 708HCP10CT Rupture disc Inconel 1000psi 708HCP20CT Rupture disc Inconel 2000 psi 708HCP30CT Rupture...

Страница 28: ...or above 16 req 265HC4 Thermowell 7 75 deep 265HC10 Thermowell 11 87 deep 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated A472E6 Thermocouple 15 1 2...

Страница 29: ...T M T316SS A279VBAD Valve angle 3 8 NPT M T316SS 265HC15 Thermowell 15 94 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated 1571HC Head Lift Rings 1593...

Страница 30: ...e PTFE or Flexible Graphite 500 PSI 25 ft lbs 1000 PSI 50 ft lbs 1500 PSI 75 ft lbs 1900 PSI 100 ft lbs Part No Description Flat Gasket Seal 2957HC11 Head VGR two valves thermowell 2955HC Cylinder 10...

Страница 31: ...mowell gasket gold plated 265HC6 Thermowell 5 75 deep 265HC8 Thermowell 10 19 deep 36HC5 Handles 1368HC TorqueWrench 1369HC Torque Adapter A472E2 Thermocouple 9 1 2 SS A472E6 Thermocouple 15 1 2 SS 25...

Страница 32: ...3 8 tube 35HC Compression nut short 365HC Connecting tube 3 8 OD x 3 length 366HC Collar L H thread 3 8 tube 4VB3 Packing ring PTFE 2 required 4VB4KL Packing ring Flexible Graphite 40HC Collar L H thr...

Страница 33: ...i 56HCPD 0 1000 psi 56HCPF 0 2000 psi 56HCPG 0 3000 psi 56HCPH 0 5000 psi 56HCPK 0 10000 psi Series 593HC Pressure Gages 3 1 2 diameter T316SS Part No Description 593HCP1AD 0 100 psi 593HCP2AD 0 200 p...

Страница 34: ...325HC COMPRESSION PACKING GASKET NUT SEE NOTE 1 51HC TUBE INLET NUT SEE NOTE 2 40HC BUSHING 366HC BUSHING 35HC SEE NOTE 1 326HC COMPRESSION NUT SEE NOTE 1 365HC COMPRESSION 366HC BUSHING 427HC GAGE BL...

Страница 35: ...C SERIES PRESSURE GAGE 302VBAD HANDLE VALVE PACKING 8VB2 123VB2 NUT NEEDLE 20VBHB 112VB4AK VALVE ORIFICE RING 527HC 126VB 6VBAA PACKING LANTERN RING BLOCK GAGE BUSHING 40HC COMPRESSION 325HC 427HC2 SE...

Страница 36: ...2 3 9 M R 1 1 0 4 1 8 1 7...

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