Parr Instrument 4703 Скачать руководство пользователя страница 5

General Purpose Pressure Vessels

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5

User’s Responsibility

All Parr Reactors and pressure vessels are designed 

and manufactured with great care to assure safe 

operation when used within their prescribed tem-

perature and pressure limits.  But . . . the basic 

responsibility for safety when using this equipment 

rests entirely with the user; who must:

1. 

Select a reactor or pressure vessel

 which has the 

capability, pressure rating, corrosion resistance 

and design features that are suitable for its in-

tended use. Parr engineers will be glad to dis-

cuss available equipment and material options 

with prospective users, but the final responsi-

bility for selecting a reactor or pressure vessel 

that will perform to the user’s satisfaction in any 

particular reaction or test must rest with the user 

– not with Parr.

In exercising the responsibility for the selection 

of pressure equipment, the prospective user 

is often faced with a choice between over- or 

under-designed equipment. The hazards intro-

duced by under-designed pressure vessels are 

readily apparent, but the penalties that must 

be paid for over-designed apparatus are often 

overlooked. 

Recognizing these criteria, Parr reactors and 

pressure vessels are offered in several different 

styles, each designed for convenient use in daily 

operation within certain temperature and pres-

sure limits, using gaskets, closures and other 

elements carefully selected for safe operation 

within the limits specified for that design. But in 

order to preserve the validity of these designs, 

all temperature and pressure limits must be 

observed, and no attempt should be made to 

increase these limits by making alterations or by 

substituting components which are not recom-

mended by Parr Instrument Company.

2. 

Install and operate 

the equipment within a 

suitable barricade, if required, with appropriate 

safety accessories and in full compliance with 

local safety codes and rules.

All standard Parr pressure vessels are provided 

with either a suitable relief device or a means 

to attach one (typically in the form of a plugged 

opening).  When a pressure vessel is delivered 

without a pressure venting device, it is the cus-

tomer’s responsibility to provide pressure relief 

in order to protect the operator and the equip-

ment from destructive high pressures.  If you 

need more information or need help in selecting 

a proper relief device, please contact Parr Instru-

ment Company.

3.  E

stablish training procedures 

to ensure that any 

person handling the equipment knows how to 

use it properly.

4. 

Maintain the equipment 

in good condition and 

establish procedures for periodic testing to be 

sure the vessel remains structurally sound.

Pressure and  Temperature Limits

The working pressure and temperature at which any 

reactor or pressure vessel can be used will depend 

upon the design of the vessel and the materials 

used in its construction.  Since all materials lose 

strength at elevated temperatures, any pressure 

rating must be stated in terms of the temperature at 

which it applies.  The standard material of construc-

tion for Parr Instrument Company is Type 316 Stain-

less Steel.

Limits for vessels made of other materials and for 

other operating temperatures can be obtained from 

Parr Customer Service.  No attempt should be made 

to increase these limits by making alterations or by 

substituting components that are not recommended 

by the Parr Instrument Company.  It must also be 

understood that lower pressure and temperature 

limits may be required for modified reactors and for 

vessels made of special alloys.  

Limits for vessels will be determined by the physi-

cal characteristics of the vessel material and will be 

prescribed on an individual basis.

The maximum working pressure and temperature 

for any vessel is governed by the design of the 

vessel and the strength of the material from which 

it is constructed.  There is also a close relationship 

between working pressure and temperature since 

the strength of any material will normally fall off 

as the temperature is increased.  Temperature and 

pressure limits are also affected by the physical 

properties and temperature limits of the gaskets and 

seals used in the vessel, and by any valves, gages 

or other fittings attached to the vessel. Obviously, 

the safe operating pressure of any system can be no 

higher than that of its lowest rated component.

All Parr reactors show the maximum safe operating 

pressure and temperature imprinted on the cylinder.

Содержание 4703

Страница 1: ...239M 4600 4700 General Purpose Pressure Vessels Operating Instruction Manual...

Страница 2: ...e Block Assemblies 9 Pressure Gages 9 Safety Rupture Discs 9 Coned Pressure Fittings 9 Tapered Pipe Threads 10 MAINTENANCE 10 General Maintenance Notes 10 Periodic Pressure Tests 11 HEAD ASSEMBLY GUID...

Страница 3: ...Assurance Certification Intended Usage This system has been designed for use as a high pressure reactor system It has been designed built and tested to strict physical and electrical standards However...

Страница 4: ...e deliver ing carriers The vessel motor heater and tem perature controller may be packed separately for convenience in shipping but these parts are easily reassembled Examine the components closely fo...

Страница 5: ...hout a pressure venting device it is the cus tomer s responsibility to provide pressure relief in order to protect the operator and the equip ment from destructive high pressures If you need more info...

Страница 6: ...mL Vessel with Split Ring Closure and 4316 Gage Block Assembly 2 Before Closing the Vessel examine the head seal carefully to be sure that it is in good condition The seal should not have any nicks or...

Страница 7: ...ded choice for many applications since PTFE materi als are inert to most chemicals PTFE gaskets will provide good seals under repeated opening and closing of the vessel if the gasket temperature does...

Страница 8: ...lue This will compensate for any tendency of the PTFE gasket to flow under the loading Note It may be possible to extend the life of the Flexible Graphite gasket by coating both sealing surfaces of th...

Страница 9: ...e connections Gages constructed of Alloy 400 are available on special order Safety Rupture Discs Detailed instructions for the safety rupture disc installed in Parr gage blocks and heads are provided...

Страница 10: ...ring and pres sure connections for excessive corrosion Sus pect parts should be replaced by components only supplied by Parr Instrument Company 2 Always use appropriate wrenches on all fittings and va...

Страница 11: ...t regular intervals during the life of each cylinder and particularly whenever the user suspects that the equipment has been over stressed or damaged Some laboratories maintain hydraulic test faciliti...

Страница 12: ...ns for Alloys other thanT316SS For parts made from alternate materials use the codes shown below as a suffix to the standard part number CM Alloy 400 CC Alloy 20Cb3 CH Alloy C 276 CT Alloy 600 CAD Tit...

Страница 13: ...l fittings per page 12 Recommended BoltTorque PTFE Gasket 500 PSI 15 ft lbs 1000 PSI 20 ft lbs 1500 PSI 30 ft lbs 1700 PSI 40 ft lbs Part No Description Flat Gasket Seal 7AC7 Head A socket 7AC8 Head o...

Страница 14: ...l fittings per page 12 Required for maximum working pressure of 7900 psi 544 bar at 538 C for vessel of T316SS Part No Description Flat Gasket Seal 1827HC Head A Socket opening A1828HC Cylinder 75 mL...

Страница 15: ...Head two 1 8 NPT 428HC11 Head A socket 1 8 NPT 428HC22 Head A socket 1 8 NPT for thermowell 425HC Cylinder 125 mL 4 44 deep 425HC3 Cylinder 200 mL 6 94 deep 429HC2 Gasket PTFE 429HC2KL Gasket Flexibl...

Страница 16: ...et 25 ft lbs Flexible Graphite 35 ft lbs Part No Description Flat Gasket Seal 453HC Head A Socket opening 453HC5 Head A Socket 1 8 NPT 453HC79 Head A Socket 1 8 NPT for thermowell 818HC45 Head VGR 452...

Страница 17: ...A122VB STRAIGHT VALVE 526HC SERIES R D 832HC4 DIP TUBE W NUT 836HC GAGE ADAPTER 818HC45 HEAD 452HC CYLINDER 300mL 288VBAD MALE CONNECTOR 366VBA_ HEX COUPLING A455HC SPLIT RING ASSY 457HC2 GASKET 454HC...

Страница 18: ...CE orders Maximum WorkingTemperature with FKM O ring with FFKM O ring 225 C 300 C Part No Description O ring Seal 2321HC2 Head A socket opening 2321HC3 Head A socket 1 8 NPT 2340HC11 Head VGR 2342HC...

Страница 19: ...T RING ASSY A456HC DROP BAND W SCREW 2341HCJV O RING 832HC4 DIP TUBE W NUT 288VBAD MALE CONNECTOR A472E THERMOCOUPLE 366VBA_ HEX COUPLING A888HC2 R D HOLDER ASSY 2342HC CYLINDER 300mL A122VB STRAIGHT...

Страница 20: ...429HC2KL Gasket Flexible Graphite 454HC Compression Ring A455HC Split Ring A456HC Drop Band 232HCFDE Bolt for Split Ring 1443HC2 DIP TUBE 50mL 1443HC DIP TUBE 25mL 593HC SERIES PRESSURE GAGE 836HC GAG...

Страница 21: ...i A122VB Valve Straight 1 8 NPT M Recommended BoltTorque PTFE or Flexible Graphite 15 ft lbs max Part No Description A146VB Valve Angle 1 8 NPT M A472E4 Thermocouple 5 1 2 A472E Thermocouple 7 1 2 A83...

Страница 22: ...ng Limits Maximum Working Pressure T316SS 1900 psi 131 bar Maximum WorkingTemperature with PTFE confined flat gasket 350 C Recommended BoltTorque PTFE Gasket 25 ft lbs Flexible Graphite 35 ft lbs Note...

Страница 23: ...hermowell for 2000 mL vessel 265HC7 Thermowell for 1000 mL vessel 48HC Thermowell Gasket silver 48HCCN Thermowell Gasket nickel 48HCFG Thermowell Gasket gold plated A472E2 Thermocouple 9 1 2 1000mL A4...

Страница 24: ...0mL Part No Description Flat Gasket Seal 2330HC12 Head B socket 2330HC13 Head B socket thermowell 2300HC19 Head VGR thermowell 2302HC Cylinder 600 mL 2302HC10 Cylinder 1200 mL 2304HC Compression Ring...

Страница 25: ...e ratings please consult Parr Instrument Company Series 4650 Model Size Head Style 4651 250 mL VGR thermowell 4652 500 mL VGR thermowell 4653 1000 mL VGR thermowell Working Limits Maximum Working Pres...

Страница 26: ...1 4 NPT M A129VB Valve Straight 1 4 NPT M X 1 4 T A147VB Valve Straight 1 4 NPT M 658HC Valve Extension 208HC15 Gage Adapter 2 1 4 NPTF 94CA Plug Hex Head 1 4 NPT Brass 686HC DipTube 1 G 686HC3 DipTub...

Страница 27: ...AngleValve 1 4 NPT M A147VB Valve Straight 1 4 NPT M A707HC2 Rupture Disc Assembly See Manual 231M 708HCP10CT Rupture disc Inconel 1000psi 708HCP20CT Rupture disc Inconel 2000 psi 708HCP30CT Rupture...

Страница 28: ...or above 16 req 265HC4 Thermowell 7 75 deep 265HC10 Thermowell 11 87 deep 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated A472E6 Thermocouple 15 1 2...

Страница 29: ...T M T316SS A279VBAD Valve angle 3 8 NPT M T316SS 265HC15 Thermowell 15 94 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated 1571HC Head Lift Rings 1593...

Страница 30: ...e PTFE or Flexible Graphite 500 PSI 25 ft lbs 1000 PSI 50 ft lbs 1500 PSI 75 ft lbs 1900 PSI 100 ft lbs Part No Description Flat Gasket Seal 2957HC11 Head VGR two valves thermowell 2955HC Cylinder 10...

Страница 31: ...mowell gasket gold plated 265HC6 Thermowell 5 75 deep 265HC8 Thermowell 10 19 deep 36HC5 Handles 1368HC TorqueWrench 1369HC Torque Adapter A472E2 Thermocouple 9 1 2 SS A472E6 Thermocouple 15 1 2 SS 25...

Страница 32: ...3 8 tube 35HC Compression nut short 365HC Connecting tube 3 8 OD x 3 length 366HC Collar L H thread 3 8 tube 4VB3 Packing ring PTFE 2 required 4VB4KL Packing ring Flexible Graphite 40HC Collar L H thr...

Страница 33: ...i 56HCPD 0 1000 psi 56HCPF 0 2000 psi 56HCPG 0 3000 psi 56HCPH 0 5000 psi 56HCPK 0 10000 psi Series 593HC Pressure Gages 3 1 2 diameter T316SS Part No Description 593HCP1AD 0 100 psi 593HCP2AD 0 200 p...

Страница 34: ...325HC COMPRESSION PACKING GASKET NUT SEE NOTE 1 51HC TUBE INLET NUT SEE NOTE 2 40HC BUSHING 366HC BUSHING 35HC SEE NOTE 1 326HC COMPRESSION NUT SEE NOTE 1 365HC COMPRESSION 366HC BUSHING 427HC GAGE BL...

Страница 35: ...C SERIES PRESSURE GAGE 302VBAD HANDLE VALVE PACKING 8VB2 123VB2 NUT NEEDLE 20VBHB 112VB4AK VALVE ORIFICE RING 527HC 126VB 6VBAA PACKING LANTERN RING BLOCK GAGE BUSHING 40HC COMPRESSION 325HC 427HC2 SE...

Страница 36: ...2 3 9 M R 1 1 0 4 1 8 1 7...

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