Malvern Zetasizer Nano Series Скачать руководство пользователя страница 10

 6

Size test   

Zeta Potential test 

a.

Take a square plastic cuvette (not a glass one) from the consumables pack.

b.

Fill it with between 1.0mL and 1.5mL of the supplied 

Installation Sample

 (DTS1050) from the  

syringe, as follows.

c.

Tilt the cuvette and allow it 
to fill slowly:

ill  7935

To stop bubbles forming, let the 
sample flow down the inside.

d.

The sample depth should be 
between 10 and 15 mm.

   

ill 7936

e.

Push the lid securely onto 
the cuvette:

ill 7937

a.

Take a supplied 

Folded capillary cell

 and rinse this with ethanol or methanol.  A syringe or wash 

bottle can be used. Use sufficient fluid to just wet the surface of the cell and the electrodes.

b.

Flush de-ionised water through the cell five times. To do this, insert a syringe of water in one port,  
an empty syringe in the other. Flush the syringe’s contents through the cell into the empty syringe.

c.

Invert the cell 

:

 

ill 7938

d.

Slowly inject the 

DTS1050

 sample 

from its syringe into the cell, filling the 
U tube to just over half way 

.

e.

Check no air bubbles form in the cell. 
Tap the cell gently to dislodge any that 
do form.

f.

Turn the cell upright and 
continue injecting slowly 
until the liquid reaches the 
bottom of the ‘luer’ outlet 

 

ill 7939

g.

Check again for bubbles 
in the cell. Tap the cell 
gently to dislodge these.

h.

Check that the elec-
trodes are com-
pletely immersed.

i.

Remove the syringe 
and insert a cell 
stopper in each 
port: 

 

ill 7940

j.

Remove any liquid 
spilt on the elec-
trodes.

Max: 15mm

Min: 10mm

2

1

3

Содержание Zetasizer Nano Series

Страница 1: ...I N S T R U M E N T S Zetasizer nano series Self installation and Quick start guide Read this first MRK825 02...

Страница 2: ......

Страница 3: ...Zetasizer Nano series Self installation and Quick start guide MAN0383 Issue 1 1 July 2007...

Страница 4: ...efore disclaim all liability for any changes errors or omissions after the date of publication No reproduction or transmission of any part of this publication is allowed without the express written pe...

Страница 5: ...covers Always stand it on its feet not its side ill 7929 ill 7930 2 Site requirements The site must be Indoors and away from strong light avoid windows Away from heat sources like radiators On a horiz...

Страница 6: ...t be connected to a protective earth a Unpack the cables from the Installation Kit pack b Connect the USB cable to the USB connectors on the instrument and the computer c Connect the power cable to th...

Страница 7: ...strument is switched on If the above suggestions do not help replace the fuses as shown in the Essentials Manual this is a task for the supervisor not operators Amber light If there is no system not r...

Страница 8: ...4...

Страница 9: ...as described here For example if the instrument reported just now that it will test only Zeta Potential measurement skip the Size test procedure below a When the software has been started select Tools...

Страница 10: ...e electrodes b Flush de ionised water through the cell five times To do this insert a syringe of water in one port an empty syringe in the other Flush the syringe s contents through the cell into the...

Страница 11: ...spot mark This must face towards the front of the Nano ill 7943 c Push the cuvette down so it s firmly located then push down the chamber lid ill 7944 a Press the button to open the measure ment chamb...

Страница 12: ...gerprints grease and dust b In addition for a Size test Check that between 1 0mL and 1 5mL is injected into the cuvette giving a sample depth of 10mm to 15mm as shown in Step 4 above Check that the tr...

Страница 13: ...vanced users To run an SOP 1 Select the command Measure Start SOP 2 Available SOPs are listed in a dialogue Select the SOP to use and click the Open button 3 Follow any on screen instructions to run t...

Страница 14: ...e measurement file currently open To view the result select this record and then click one of the Report tabs The following examples show The Intensity PSD M report for a size test top report The Zeta...

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