Linseis Chip-DSC 10 Скачать руководство пользователя страница 4

 How To Low temperature measurements   

 

3. Preparation of the Chip-DSC 100 System 

3.1 Peltier system 

o

 

Affordable and easy to use cooling option for investigations near room temperature 

o

 

Δ

T up to 30 K below ambient temperature is possible 

o

 

 The system is already installed and can be turned on by the switch at the side of your Chip-

DSC 100 

3.2 Intracooler System 

o

 

Closed system and easy to use cooling option for investigations at lower temperatures 

o

 

up to -99 °C at coolfinger is possible 

o

 

 insert the coolfinger carefully in the hose of the adapter in your Chip-DSC 100 

o

 

Tighten the screw at the bottom of the cooling hose 

o

 

Turn on the Intracooler directly at the back of the cooling system (attend the instructions of 
your Intracooler) 

Содержание Chip-DSC 10

Страница 1: ...1 How To Low temperature measurements with Chip DSC Linseis Messgeräte GmbH Gerlach Stand 26 08 2021 ...

Страница 2: ...Preparation of the Chip DSC 10 System 3 2 1 Peltier system 3 2 2 QuenchCooling system 3 3 Preparation of the Chip DSC 100 System 4 3 1 Peltier system 4 3 2 Intracooler System 4 3 3 manual LN2 system 5 3 4 Automatic LN2 system 6 4 Calibration hints 7 5 Measurement hints 7 ...

Страница 3: ...continuous cooling option with thermo electric generators o ΔT up to 30 K below ambient temperature is possible o place the cooling block on the ready to use Chip DSC 10 o tighten the screws at the blue main plate o connect the Peltier cooler with power supply and turn on the cooling device 2 2 QuenchCooling system o Easy to use and efficient cooling option with liquid nitrogen for lowest temperat...

Страница 4: ...ed and can be turned on by the switch at the side of your Chip DSC 100 3 2 Intracooler System o Closed system and easy to use cooling option for investigations at lower temperatures o up to 99 C at coolfinger is possible o insert the coolfinger carefully in the hose of the adapter in your Chip DSC 100 o Tighten the screw at the bottom of the cooling hose o Turn on the Intracooler directly at the b...

Страница 5: ...ns at lowest temperatures o investigations from 150 C are possible o open the cap of your Quench cooling reservoir o Fill the reservoir with liquid nitrogen until you reach the required temperature o To avoid evaporated liquid nitrogen in your lab it is possible to connect an additional tube at the outlet of your cooling option ...

Страница 6: ...est temperatures o investigations from 150 C are possible o adjust the level of the temperature sensor in your liquid nitrogen reservoir o Connect the tube of your Dewar bottle with the inlet of your Chip DSC 100 o To avoid evaporated liquid nitrogen in your lab it is possible to connect an additional tube at the outlet of your cooling option ...

Страница 7: ... t evaporate when you put them from balance to the precooled measurement cell e g by using closed crucibles 5 Measurement hints o Make sure the measurement cell is closed properly to avoid convection and condensation o Using dry gas also helps to avoid condensation also purge while changing the sample o For liquid samples make sure they don t evaporate when you put them from balance to the precool...

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