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THMS600 / HFS600

Temperature Controlled Stage

USER GUIDE

Linkam Scientific Instruments

Содержание BCS196

Страница 1: ...THMS600 HFS600 Temperature Controlled Stage USER GUIDE Linkam Scientific Instruments...

Страница 2: ...rocedure 14 Purging the Stage Method 1 14 Purging the Stage Method 2 15 Appendix 16 Window Assembly 16 Lid Window Assembly 16 Bottom Window Assembly 16 Troubleshooting 17 Alternate Configuration THMS6...

Страница 3: ...ical high temperature IR stage BCS196 Biological cryo stage Before Setting Up Your Equipment Please register your products by going to the technical support section of our web site www linkam co uk Yo...

Страница 4: ...o your health and safety manual for instructions on how to handle liquid nitrogen safely Always use in a well ventilated room Pressure Warning The THMS600 PS has been designed specifically for use at...

Страница 5: ...any reason it gets wet then unplug it from the mains and contact Linkam Scientific Technical Support 6 The equipment is not intended to be used outdoors 7 If any problems occur then turn all Linkam e...

Страница 6: ...5mm Condenser lens WD 12 5mm XY Manipulators travel 16mm Aperture hole 2mm Weight 0 62Kg THMS600 System The system consists of a THMS600 stage a T95 System Controller and optional LNP95 liquid nitroge...

Страница 7: ...dy water cooling connector 12 Sample chamber 13 Earth safety contact for lid 15 Heating element wire 16 Stainless steel cooling tube 17 22mm diameter pure silver heating block 18 Platinum temperature...

Страница 8: ...e centre of the field of view and lock the stage in place by tightening the Locking Thumbscrew 3 For other types of microscope substage refer to the diagram included with the stage adaptor Setting up...

Страница 9: ...zers The System is supplied with a Vacuum Tweezers Kit which consists of a Vacuum Pump 1 and tweezers 2 Connect the tubing at the end of the tweezers to the Regulator Valve 3 connection Use the dial o...

Страница 10: ...ge above 300 C for a pro long period of time the metal casing body of the stage can get quite hot Connect the tubing as shown in the opposite picture Note If you have an LNP95 Liquid Nitrogen Cooling...

Страница 11: ...e holder Load the sample into the quartz crucible Use as little sample as possible to ensure a small thermal load and therefore better temperature sensitivity Microscope objectives require a flat surf...

Страница 12: ...tweezers as shown and place a 16mm glass cover slip 2 into the stainless steel ring Tap the edges lightly to ensure that it sits flat against the surface of the block If the cover slip does not sit pe...

Страница 13: ...de of this white connector is the Gas Purging Tube 3 There is a valve opening Insert connector 4 inserted into the end of this tube During the purging procedure insert this connector into the Gas Purg...

Страница 14: ...se a finger on the right hand to block the gas outlet for a few seconds to allow pressure build then release the gas Repeat this for a few minutes to purge the stage 7 Look at the change of reflection...

Страница 15: ...a gas flow rate of 1 5L min 5 With the gas flowing through the Sample Chamber block the gas outlet for a few sec onds and releasing the gas outlet valve with a finger Repeat this for a few minutes to...

Страница 16: ...and reassembled in the order indicated The Lid Insert should be screwed down until the cover slips are held firmly then turn the assembly over and screw down the Lid Insert until it is felt to come t...

Страница 17: ...ed If any damage has occurred to any of these items then it will be necessary to replace them If no damage is found check that the silver block is not constricted This can be checked simply by blowing...

Страница 18: ...HMS600 PS is designed for use with pressurised air For use with other gases please contact support linkam co uk THMS600 PS Stage Specifications Maximum temp at atmospheric 600 C Minimum temp at atmosp...

Страница 19: ...lator 8 Side door locking thumbscrew 9 Y Sample manipulator 10 Liquid nitrogen cooling connector 11 Stage body water cooling bypass loop connector 12 Stainless steel liquid nitrogen cooling tube 13 Pr...

Страница 20: ...nylon pressure tubing 6mm outer diameter 3mm inner diameter is connected to the pressurised gas inlet with a push to fit connection Make sure the end 10mm of the tubing is free of dirt grease and has...

Страница 21: ...stem The system consists of a FTIR600 stage a T95 LinkPad System Controller and optional LNP95 liquid nitrogen cooling pump LINK System control software and digital video capture can be added as an op...

Страница 22: ...used to keep the sample in place The FTIR600 Vertical Stage has the same specifi cations and works in exactly the same way as the standard FTIR600 The heater assembly is locat ed on the side the Gas P...

Страница 23: ...in a vertical position 1 Heating element carrier assembly 2 Gas purge valve with Tubing 3 Gas Purge Valve 4 Base Stand Assembly 5 Stage body water connector 6 Vertical Sample Holder Assembly Post and...

Страница 24: ...nected To connect the Gas Purge Valve with Tubing use one hand to hold the black and blue colour gas valve 2 then firmly and push the tubing into the hole as far it can go Note to remove the Gas Purge...

Страница 25: ...ows 140 overall THMSEL600 System The system consists of a Ellipsosmeter High Temperature Stage and T95 LinkPad System Controller LINK System control software and digital video capture can be added as...

Страница 26: ...ocking thumbscrew 8 Stage body water connector 9 Heating element wire 10 Stainless steel tube 11 Stage body water connector 12 Gas purge valve 13 Sample holder ramp 14 Stage door 13 Y Sample manipulat...

Страница 27: ...x 0 17mm Side Windows Assembly Use the Side Window Locking Tool 5 to remove the Side Window Locking Ring 6 and reassem ble the Side Window as shown in the diagram 5 Side Window Locking Tool 6 Side Wi...

Страница 28: ...l 16mm Aperture hole 1 3mm Weight 0 62Kg THMSG600 System The system consists of a THMGS600 stage a T95 LinkPad System Controller and LNP95 liquid nitrogen cooling pump system LINK System control softw...

Страница 29: ...soft metal it can get scratched easily especially by using sharp fine tweezers This can cause a ridge to form which prevents the sample window from sitting flat on the block with the resulting air gap...

Страница 30: ...next to the end of the sample holder With one hand carefully lift the G7T about 1mm off the silver heating block and slide the 7mm sample window directly underneath the circular sample holder Release...

Страница 31: ...re Make sure the gap in the SCO 1 is aligned with the stem 2 of the Sample holder The gap in the SCO allows movement of the Sample Holder when the XY manipulators are used To improve temperature stabi...

Страница 32: ...nser lens WD 12 5mm XY Manipulators travel 16mm Aperture hole 1 3mm Weight 0 62Kg BCS196 System This Cryostage System consists of the BCS196 cryostage a T95 LinkPad System Controller and LNP95 liquid...

Страница 33: ...nnector 12 Sample chamber 13 Earth safety contact for lid 14 Hinge for stage door 15 Heating element wire 16 Stainless steel cooling tube 17 22mm diameter pure silver heating block 18 Platinum tempera...

Страница 34: ...17 5 Sample Holder To convert a standard BCS196 with this option it must be returned to Linkam for modifications to suit the following 1 Warm transfer post 2 Quench Cooling Transfer Manipulator 3 QSM...

Страница 35: ...ip the retaining catch 2 Pull the retaining catch out from the sample holder 3 Relocate the retaining catch within locating slot also shown on page 16 Problem The retaining catch has disengaged and is...

Страница 36: ...gin to load the sample holder into the stage see page 11 for additional information 2 Check that the return catch locates within the alignment slot inside BCS196 stage correctly If this return catch d...

Страница 37: ...the push manipulator 5 in the other give it a 1 4 turn anti clockwise to make sure the locating pin is in the long slot and not the locked position then push the manipulator all the way until it stops...

Страница 38: ...he sample onto the W7S In order to vitrify the sample the sample holder must be moved to the warm post before cooling the silver block to the specified temperature Do this by pushing the Push manipula...

Страница 39: ...manipulators so that the sam ple assembly is placed centrally on the silver block 3 Find out where the sample melts by freezing the sample and then slowly heating 5C min Note when the last crystal mel...

Страница 40: ...WD 12 5mm Aperture hole 2mm Probe Maximum voltage 300V AC Maximum ampere 4A HFS600E PB4 PB2 System The system consists of a HFS600E PB4 PB2 stage with 4x 2x BNC Connectors a T95 LinkPad System Control...

Страница 41: ...9 Stage chamber 10 Outlet Inlet Gas Connector 11 BNC connector 14 Heating element wire 15 Stainless steel cooling tube 16 Platinum temperature sensor 17 Probe 18 Metal plate for probe 19 Pure silver...

Страница 42: ...the probe from the stage Note the Probe has a very sharp needle tip be careful not to hurt yourself with it BNC Wire Connection Use an adjustable spanner 3 or a pair of pliers and unscrew the BNC soc...

Страница 43: ...end of the yellow wire to the desired length and strip 5mm of the insulation Fold the bare wire in half Use the supplied M1 Hex Key 1 and turn the grub screw 2 on the side of the Probe Assembly 3 4 tu...

Страница 44: ...holds the magnetic foot of the Probe in place Adjust the length of the needle Pull end of the needle to the desired length and use a wire cutter to cut the needle shorter Bend the tip of the needle U...

Страница 45: ...the supplied M1 Hex Key 1 to shorten or lengthen the grub screw 2 to change the angle of the needle Note the probe is spring loaded and makes better contact with the sample if the needle is adjusted...

Страница 46: ...meter Lid top window assembly Ellipsometer Side Windows Assembly Use the Side Window Locking Tool 5 to remove the Side Window Locking Ring 6 and reassem ble the Side Window as shown in the diagram 6 S...

Страница 47: ...47 This page is intentionally blank...

Страница 48: ...el 44 0 1737 363 476 Fax 44 0 1737 363 480 Email support linkam co uk Unit 8 Epsom Downs Metro Centre Waterfield Tadworth Surrey KT20 5LR UK www linkam co uk Version 1 05 1109 Powered by TCPDF www tcp...

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