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I. Safety 

1. Overview 

 

This operating manual is prepared for the laboratory instrument operators. Please read this manual 
carefully  before  using  the  instrument  and  conduct  the  operation  according  to  the  manual.  Personnel 
who  are  not  familiar  with  the  instrument  operation  or  safety  information  shall  not  operate  the 
instrument.  
This  instrument  adopts  the  current  most  advanced  technology  for  design  and  manufacturing.  But  the 
improper use of this instrument will cause a potential safety hazard.  
The instrument manufacturer has made the assessment on the possible hazard:  
-Inexperienced personnel operating the instrument 
-Failure to operate the instrument according to the normal regulations 
-The operators of this instrument shall know all the below mentioned warnings. 

 
2. Safety  

Warning: This instrument is only used for laboratory. If the instrument is damaged due to the 

failure of conducting the operation according to the manual during the use, the manufacturer refuses to 
bear all consequences.  

Warning: If the failure of using the instrument properly or conducting the operation according 

to the operating manual causes any consequences, the company will not bear the safety problem of 
instrument use.  

Warning: The failure of operating the instrument as required by this manual will weaken the 

safety performance of the instrument.  

Warning: Please conduct the treatment of various solutions used in the test according to the laboratory 

safety regulations. Operators shall wear the rubber gloves, lab coats and goggles. 
 

Warning: Oral intake of boric acid will cause acute poisoning, which is mainly embodied in 

gastrointestinal  symptoms,  nausea,  emesis,  abdominal  pain,  diarrhea,  etc.,  and  then  dehydration, 
shock,  coma or acute renal failure, or high fever, liver and kidney  damage, convulsions and even 
cause  death  if  serious.  It  is  easily  absorbed  by  the  damaged  skin  and  causes  poisoning.  Chronic 
poisoning  long-term  absorption  of  small  amount  of  boric  acid  in  gastrointestinal  tract  or  skin  will 
lead to mild digestive tract symptoms, dermatitis, baldness and liver and kidney damage.  

Warning: Sodium hydroxide has causes irritation and shows high corrosivity. The powder or 

smog will irritate the eyes and respiratory tract and corrode nasal septum. Direct contact of skin or 
eyes  with  sodium  hydroxide  may  cause  burns,  and  accidental  take-in  can  cause  gastrointestinal 
burns, mucosal erosion, bleeding and shock.  

Warning:  Sulfuric  acid  (95-98  %)  has  intense  irritation  and  corrosive  effect  upon  the  skin, 

mucosa, and other organs. Vapor or mist may cause conjunctivitis, conjunctival edema, and corneal 
opacity,  and  consequently  blindness;  it  may  cause  respiratory  irritation,  and  may  cause  dyspnea 
and pulmonary edema in severe cases. High concentration may cause the laryngospasm or glottic 
edema,  and  finally  death  by  suffocation.  Oral  take-in  may  cause  digestive  tract  burns  and  thus 
elcosis. It may cause gastric perforation, peritonitis, renal damage, shock, etc. in severe cases.  

Warning:  The  temperature  of  the  digestive  tract will  reach  100 

  during  the  experiment. 

After completing the distillation, take the testing tube out with test tube holder for avoiding scald.  
 
 
 
 
 
 
 
 

Содержание KJD20

Страница 1: ...KJD20 Kjeldahl Automatic Distiller Please read the User Manual carefully before use and follow all operating and safety instructions user manual english...

Страница 2: ...r maintenance In case of any faults do not try to repair it yourself If help is needed you can always contact your dealer or Labbox via www labbox com Please provide the customer care representative w...

Страница 3: ...l wear the rubber gloves lab coats and goggles Warning Oral intake of boric acid will cause acute poisoning which is mainly embodied in gastrointestinal symptoms nausea emesis abdominal pain diarrhea...

Страница 4: ...ring the instrument operation Notes Make sure that the liquid solution does not contact the power line and electric parts inside the instrument Notes Stop using the instrument in the case of failure a...

Страница 5: ...ck wear parts and these spare parts can be inquired in the user s manual and user s guide The quality guarantee responsibility of quick wear parts is only limited to the damage caused by the material...

Страница 6: ...m released during the reaction are condensed and collected into the receiving flask where the boric acid with mixed indicator is added III Specifications 1 Technical Specifications a Measurable amount...

Страница 7: ...llation Conditions The Kjeldahl Distillation Unit should be installed in neither excessively hot cold or humid places nor places with excessive sunlight exposure Commonly the room temperature should b...

Страница 8: ...e that the discharging performance is good View of Right Side Fig 3 Fig 3 View of right side 8 Ventilation hole for alkali bottle 9 Ventilation hole for boric acid bottle 10 Ventilation hole for disti...

Страница 9: ...nually When the digestion is finished cool it At the same time do the blank test VII Operation Instruction 1 Preparation of the Chemical Reagent 1 Add distilled water into the distilled water bottle w...

Страница 10: ...will return to the initial interface Auto key Press the key to Enter the interface for automatic test parameter modification when the instrument is under the initial interface or test selection inter...

Страница 11: ...initial interface provides three modes test maintenance and help You may use Left and Right key to target test button and press OK key for the test mode See Fig 2 Fig 2 You may use Left and Right key...

Страница 12: ...4 after input of parameters and press Back key for the previous interface Fig 4 Press OK key for the test The test will be carried out automatically by the system and adding boric acid adding dilutio...

Страница 13: ...Fig 7 Fig 7 2 Manual test The system will offer safety notes first as shown in Fig 8 when you select the manual test interface Fig 8 Press OK key for manual test interface Each option may be selected...

Страница 14: ...des flushing of alkali piping liquid adding for calibration function commissioning safety setting and flushing of alkali piping The alkali piping shall be flushed regularly in strict accordance with t...

Страница 15: ...will Back to maintenance interface after flushing Fig 13 Liquid adding for calibration Liquid adding for calibration includes calibration by dilution water alkali solution boric acid solution or drip...

Страница 16: ...f the liquid received in the Please enter volume section and press OK key for end of calibration Or press Return key to quit calibration Fig 16 Press OK key and a small interface will appear as shown...

Страница 17: ...icated by and incorrect positioning or no placement is indicated by Press Return key and all the components will close down automatically Fig 18 Safety Setting Safety setting is mainly aimed at test f...

Страница 18: ...y accumulate 4 Water scale may accumulate in the distilling bottle after a long time which can influence the heating efficiency Follow the procedures listed below to remove it Firstly turn off the ins...

Страница 19: ...alkali solution from its bottle and fill the water instead if the instrument will not be used for a long time Install nitrogen tube back to the instrument and start manual mode of adding alkali soluti...

Страница 20: ...20...

Страница 21: ...www labbox com...

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