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USER MANUAL 

 

 

3. Apparatus Assembly 

 
 
3.1 

Before use, check that the filter support screen is clean. If necessary, the screen must be  

            cleaned by boiling in a high boiling point aromatic solvent. When more than 2 % of the sinter  
            area remains blocked by particulate matter after such cleaning, discard the screen and install  
            a new one. 
 
3.2  

The filtration unit must be clean and dry before assembly. Stack the two previously dried and 

 

weighed filter media on top of the sinter support with the mesh imprint side down, using forceps, 

 

placing the one from the lower numbered weighing bottle on the bottom. Apply slight vacuum 

 

to aid in centering the filter media, and place the top portion of the filtration apparatus  

            carefully  on to the media before clamping. 
 

Shut off the vacuum and pass steam at 100 ±1°C through the heating/cooling coils for 10 min 

 

prior to sample addition. 

 

4. Sample Addition 

 
 

4.1   

Into a 30 mL beaker, pour approximately 11 g of the fuel sample prepared as described in 9.1 

 

and weigh to the nearest 0.01 g. 

 

Connect the vacuum source and apply vacuum to an absolute pressure of 40 ±2 kPa minimum 

 

(61.3 kPa vacuum). Heat the contents of the beaker to 100 ±2°C. Then transfer the contents at 

 

100 ±2°C (Note 3) to the center of the filter medium, taking care that no sample touches the 

 

walls during transfer (Note 4). Reweigh the beaker to the nearest 0.01 g. The quantity 

 

transferred should be 10 ±0.5 g. When filtration is not complete in 25 min, discontinue 

 

the test and repeat using 5 ±0.3 g of sample. If filtration is still not complete in 25 min, report 

 

the result as filtration exceeds 25 min. 

 

 

NOTE 3— 

It is expedient to weigh the beaker plus stirrer plus temperature measurement  

 

 

 

device before and after transfer to avoid errors incurred by attempting to obtain 

 

 

 

a net weight. Any convenient means of heating the fuel sample to 100 ±2°C may 

 

 

 

be used, such as hot plate, water or oil bath, or an oven when equipped with a  

 

 

 

suitable stirrer. Samples that overheat above 105°C must be discarded and 

 

 

 

not reused. 

 

NOTE 4— 

For samples of high viscosity or high sediment, level fi ltration will be aided by  

 

 

 

small stage or even dropwise addition. It is preferable to avoid complete  

 

 

 

coverage of the fi lter medium with unfi ltered oil sample. 

 

 

 

For samples of low fi ltration rate the pressure of 40 ±2 kPa should be  

 

 

 

 

maintained for the 25-min period.

 

Содержание K4831X

Страница 1: ...re Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis Instrumentation Custom Design Manufacturing K4831X Total Sediment Tester ...

Страница 2: ... Page 2 ...

Страница 3: ... Page 3 USER MANUAL CONTENTS Notice Guarantee Safety information and suggestions Technical specifications of the device Accessories Spare parts Procedure Guarantee certificate ...

Страница 4: ...es etc it is essential to contact the manufacturer Whoever intervenes with the device will act under his own responsibility and cause the immediate suspension of the warranty Before proceeding with a maintenance service remove the plug from the socket The manufacturer declines every kind of responsibility for all the operations not in conformity to the aforesaid dispositions or performed by person...

Страница 5: ...if any The manufacturer is not responsible for the possible damages caused to the device due to wrong connections to the power supply if any In case of extraordinary maintenance personally realised by the customer during the warranty period the guarantee will immediately be suspended The manufacturer reserves himself the right to bring in any moment and without warning changes and innovations resp...

Страница 6: ...NS BELOW 1 Avoid to lean on the apparatus any kind of material 2 Oversee the operating zone in order to avoid the approaching of operators without qualification 3 Always wear suitable clothes 4 Always use masks protective glasses and gloves in conformity to the normative in force 5 Avoid to send water spout on the device 6 Always pay attention when using the apparatus 7 It is severely forbidden to...

Страница 7: ... the end of life is organized and managed by the manufacturer The user that intends to trash this equipment will have to contact the manufacturer and follow the procedure that it has taken to allow separate collection of the apparatus arrived at the end of life Appropriate differentiated collection for the dismantled appliance being subsequently sent out for recycling treatment and for environment...

Страница 8: ...rom 0 to 50 C Storage temperature from 10 to 70 C Ambient relative humidity lower than 90 HR not condensing ACCESSORIES K48319 10 Steam Generator K48319 11 Vacuum Pump K48319 14 GFA filter pack of 100 pcs K48319 9 Thermometer 95 C 105 C SPARE PARTS K48319 14 GFA filter pack of 100 pcs K48319 12 Sintered disc pack of 2 pcs ...

Страница 9: ...media for 20 min in the oven at 110 C Transfer each paper separately rapidly to a numbered weighing bottle and allow to cool in the cooling vessel to room temperature 5 to 10 min Where two pan balances are used weigh each weighing bottle plus filter medium by the tare method against an empty similar bottle to the nearest 0 001 g NOTE 1 Caution The Whatman GF A filter media are fragile and are to b...

Страница 10: ...o an absolute pressure of 40 2 kPa minimum 61 3 kPa vacuum Heat the contents of the beaker to 100 2 C Then transfer the contents at 100 2 C Note 3 to the center of the filter medium taking care that no sample touches the walls during transfer Note 4 Reweigh the beaker to the nearest 0 01 g The quantity transferred should be 10 0 5 g When filtration is not complete in 25 min discontinue the test an...

Страница 11: ...sed before the first solvent washing to ensure complete coverage of the filter medium area by solvent The vacuum should then be gently reapplied for the subsequent operations 6 Apparatus Disassembly 6 1 After the filter medium appears dry discontinue the vacuum supply Using the forceps carefully remove each filter medium separately and transfer them to the oven at 110 C Dry for 20 min and quickly ...

Страница 12: ...filtration is not complete within the specified 25 min report the results as filtration time exceeds 25 min 8 2 Test Report The test report shall contain at least the following information 8 2 1 The type and identification of the product tested 8 2 2 A reference to this test method 8 2 3 The result of the test see 8 8 2 4 Any deviation by agreement or otherwise from the standard procedures specifi...

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