Koehler K41100 Скачать руководство пользователя страница 26

 

 
 
 
 

K41100

 

6 - MAIN CAUSES OF POOR RESULTS  

 

Since the function of the appliance is to process a sample, the cause of poor results may 
not be attributable to the appliance.  
Poor  manipulation  of  samples  (with  absorption  of  humidity  at  the  end  of  the  test), 
inaccurate weighing, an error in entering the weight, an error in identifying the samples 
may all cause errors in the expression of results.  

In the case of a doubtful result, it is appropriate to:  

  Check  the  condition  of  the  cover  after  the  test.  If  leaks  have  occurred  at  that  

 

location  there  will  be  traces  on  the  cover.  Also,  check  there  are  no  deposits  on  

 

the oven mouth and the oven cover that could adversely affect oven  
Air tightness.  

 Check that the exhaust of the oven is not partially or completely blocked.  

 Check that the gas system is properly open and that the flow rates are correct.  

  Ensure  that  the  load  placed  in  the  vials  is  not  excessive  and  that  there  has  been  

 

no loss by overflowing.  

 Finally, check calibration of the oven thermo-couple.  

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

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Содержание K41100

Страница 1: ...nue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analysis I...

Страница 2: ......

Страница 3: ...in conformance with the applicable standards set forth in this certification Specifications ASTM D4530 This unit is tested before it leaves the factory to ensure total functionality and compliance to...

Страница 4: ......

Страница 5: ...nnectors 13 3 3 Starting up 14 4 USE OF THE APPLIANCE 15 4 1 Description of the temperature regulator 15 4 2 Starting a test 15 4 3 Interruption of a test 18 4 4 Alarm 19 4 4 1 Alarm during a test 19...

Страница 6: ...hed 7 Disconnect the appliance from the mains power when it is not in use Never pull on the cable to disconnect it from the mains Take hold of the plug and remove it from the power socket 8 Allow the...

Страница 7: ...a month in order to check satisfactory condition of pipes and their fastenings In the case of an incident that could result in damage to the appliance excess gas pressure abnormal heating of the appli...

Страница 8: ...to an appliance of which the defect is the result of incorrect use connection to an unsuitable electricity supply absence of ground an act of vandalism or caused by the forces of nature thunder flood...

Страница 9: ...respected scrupulously to avoid any physical injury or damage to your appliance Maintenance Supplies important information concerning the maintenance of your appliance Remark Provides useful advice f...

Страница 10: ...tandard ASTM D 4530 Cooling of oven Accelerated by injection of compressed air for forty minutes Gas connections at the rear of the Instant connections dia 4 mm for appliance nitrogen and dia 8 mm for...

Страница 11: ...K41100 2 3 Description of the appliance 2 3 1 Front panel 8 30...

Страница 12: ...K41100 2 3 2 Rear Panel 9 30...

Страница 13: ...K41100 2 3 3 Accessories I 10 30...

Страница 14: ...er transport or unpacking must not be commissioned To avoid risks of condensation the appliance must be left at room temperature for several hours before it is powered on 3 2 Appliance connections Dep...

Страница 15: ...nterfere with the test by modifying the flow rates and causing leaks through the hot cover of the oven From the side of the appliance take the cover handling hook and the sample vial see photo opposit...

Страница 16: ...nnection of a pipe Simply push the pipe totally home in the connector The connection and leak tightness are made instantaneously 3 2 1 2 Disconnection of a pipe Press the push button on the outside of...

Страница 17: ...e When the temperature regulator is powered on for three seconds it runs a series of automatic tests After each sequence the display shows the temperature measured on the upper display and displays OF...

Страница 18: ...ed by the test Reminder It is vital to be familiar with the standards concerning the tests to be initiated Reminder The installing and removal of samples after the tests requires working with a hot ov...

Страница 19: ...f the test Check that the oven outlet is not blocked by carbon deposits see Para Maintenance Place the vial holder in the oven using the tool supplied see photo Replace the oven cover with the tool pl...

Страница 20: ...Cooling with compressed air for forty minutes Entry of nitrogen in the oven high flow rate 5 End of test Switch off heating and gas supply During the test check that the nitrogen flow rates are corre...

Страница 21: ...the RUN LED goes out To put the program on hold press the key the RUN LED goes out and the HOLD LED lights up HOLD is indicated on the lower display The temperature regulator will remain in this stat...

Страница 22: ...st If a test is in progress the safety device will switch the regulator to HOLD the RUN LED goes out and the HOLD LED comes on HOLD is indicated on the lower display The temperature regulator will rem...

Страница 23: ...regulator to manual mode the AUTO LED goes out and the MAN LED lights up When the oven is cold the regulator reverts to wait mode In the case of an alarm it is always necessary to investigate the caus...

Страница 24: ...ded running the cleaning cable through to clean off any deposits see next paragraph 5 2 General maintenance Depending on the number of analyses and the type of samples used periodic maintenance is nec...

Страница 25: ...rform the same operation in the case of deposits of carbon 5 2 2 Checking the oven temperature To check the oven temperature a control thermocouple must be placed in the oven For this purpose the cove...

Страница 26: ...a doubtful result it is appropriate to Check the condition of the cover after the test If leaks have occurred at that location there will be traces on the cover Also check there are no deposits on th...

Страница 27: ...couple Insulating cover Glass vial 2 ml Glass vial 16 ml Pressure gauge Brass condensates container Glass condensates container Condensates container seal Flow Meter Air electro valve Nitrogen electro...

Страница 28: ...K41100 8 ANNEXES 8 1 Flow meter abacus 25 30...

Страница 29: ...26 30...

Страница 30: ...EUROTHERM 24 08 1 2 3 4 static relay r elais statiq ue 2A L r elay N 1A 10A 1B l og ic AA AB 2 1 LA LB LC BY DATE V V 2A 2B 2C 2D 3A 3D heater chauffe temperature sensor thermocouple Tc nitr og en azo...

Страница 31: ...2 50 KPa solenoid valve lectrovanne NITROGEN solenoid valve lectrovanne valve low flow vanne petit d bit flowmeter d bitm tre manometer BY DATE SIMON M 18 04 05 28 30 Furnace Four Furnace Four KOEHLE...

Страница 32: ...mensions 7 Display 14 16 17 18 19 E END 17 Extension 3 12 16 22 24 F Flow 2 11 12 17 22 23 24 25 Flue 12 16 22 24 G Gas 7 Gloves 4 15 21 24 Goggles 4 15 21 H HOLD 18 19 Holder 12 16 24 Hood 4 12 15 16...

Страница 33: ...1 23 Seal 21 24 Smoke 4 12 15 Stud 22 Switch 14 17 19 20 T Temperature 2 4 7 11 14 15 16 17 18 19 22 24 Test 2 3 4 11 12 14 15 16 17 18 19 20 21 22 23 Thermocouple 7 Tube 13 V Valve 16 24 Vial 7 12 16...

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