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Страница 143: ...pproximately 1 mL into the titration vessel through the septum using the needle Pay attention not to get any standard on the electrode or beaker walls If necessary swirl the titration vessel by hand x Clear the needle of residual standard by in taking a very small volume of air from the titration vessel If a hanging drop of standard is seen on the end of the needle dip the end of the needle briefl...

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Страница 145: ...nter the sample size x Dispense 0 8000 g to 1 0000 g of solvent into the titration vessel through the septum using the needle Pay attention not to get any sample on the electrode or beaker walls If necessary swirl the titration vessel by hand x Clear the needle of residual sample by in taking a small volume of air from the titration vessel If a hanging drop of solvent is seen on the end of the nee...

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Страница 147: ...L x Press Start Stop to pre titrate the reagent x Fill the syringe and needle with the sample x Weigh the syringe needle and sample x Press Start Analysis You will be prompted to enter the sample size x Enter the Estimated Bromine Index The titrator will recommend the optimal sample size to be added to the titration vessel Dispense the amount provided from the optimal sample size into the titratio...

Страница 148: ... Applications r 1 0 Results Titration Report Method Name BrIndex of Aromatics Time Date 12 00 Jan 01 2013 Sample Size 0 4978 g Bromine Consumed 1 609 mg Result 323 33 mg 100g Titration Duration 4 36 mm ss Generator Electrode Type HI 900518 Titration went to Completion Operator Name Analyst Signature _______________________ ...

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