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13
QUICK START GUIDE
ible results.
Solid Samples:
• Solid samples with larger pieces may need to be pulverized or ground in an analyti-
cal mill. These samples can be added with a weighing boat by removing the sample
port plug.
• Semisolid samples with non-homogeneous water content may need to be homog-
enized before addition. The sample can be added using a syringe without the needle
by removing the sample port plug.
Liquid Samples:
• Samples with low viscosity will be added using a syringe with needle (injection
through the septum).
Weigh the syringe before and after injection in order to increase precision.
Sample Volume Preparation
Liquid samples with low viscosity can be added by volume.
Samples should be added using a class A pipette.
Note:
When adding samples using the weighing boat, pipette or syringe without needle, the
septum has to be removed. Therefore the adding operation should be performed quickly in
order to avoid the prolonged exposure of the beaker to atmospheric moisture.
Performing a Titration
• From the main screen press
for analyzing a sample or
for titrant stan-
dardization. You will be prompted to enter the analyte size. Add a prepared sample
according to a preparation method outlined above. Enter the analyte size and press
or
. The titrator will start the analysis according to the selected method.
• At the end of the titration, the message “Titration Completed” will appear on the
titration status, together with the final concentration of the moisture in the sample,
the end point volume, and other relevant information. The titrator re-enters
Standby
mode (if active) in the background.
Содержание HI 903
Страница 1: ...1 QUICK START GUIDE HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 0 ...
Страница 4: ...4 QUICK START GUIDE ...
Страница 7: ...7 QUICK START GUIDE TITRATOR CONNECTIONS Front View Rear View ...
Страница 18: ...18 QUICK START GUIDE QS 903 02 11 ...
Страница 19: ...1 INSTRUCTION MANUAL HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 00 ...
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Страница 24: ...1 2 INTRODUCTION ...
Страница 26: ...2 2 SETUP ...
Страница 30: ...2 6 SETUP 2 3 2 Titrator Rear View 2 3 3 Titrator Left side View ...
Страница 40: ...2 16 SETUP ...
Страница 42: ...3 2 USER INTERFACE ...
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Страница 52: ...4 2 GENERAL OPTIONS ...
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Страница 94: ...6 2 TITRA TITRA TITRA TITRA TITRATION TION TION TION TION ...
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Страница 108: ...7 2 AUXILIARY FUNCTIONS AUXILIARY FUNCTIONS AUXILIARY FUNCTIONS AUXILIARY FUNCTIONS AUXILIARY FUNCTIONS ...
Страница 118: ...8 2 MAINTENANCE PERIPHERALS ...
Страница 147: ...A1 1 APPENDIX 1 Appendix 1 Contents A1 TECHNICAL SPECIFICATIONS A1 3 ...
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Страница 155: ...A3 1 APPENDIX 3 Appendix 3 Accesories A3 TITRATOR COMPONENTS A3 3 ...
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Страница 191: ...1 TITRATION THEORY TITRATION THEORY Principles HI 903 KARL FISCHER VOLUMETRIC TITRATOR Revision 1 0 ...
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Страница 194: ...4 TITRATION THEORY ...
Страница 206: ...16 TITRATION THEORY A B Figure 8 Potential glass electrode mV C ...
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