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21

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• The calibrated value will be shown on the display and the third expected buffer value will be

automatically selected.

• After the second calibration point has been confirmed, press 

ESC 

to exit without performing the

third calibration point.

Point 3 calibration

• Remove the electrode holder with electrodes from the top of the beaker.
• Place the third buffer solution in a beaker and place in beaker holder. Rinse the probes in a

beaker with third buffer rinsing solution.

• Place the electrode holder (with electrode) in the beaker with third buffer and secure top by

locking. Press 

STIR

.

• If necessary press the 

ARROW

 keys in order to select correct buffer value.

•  The 

(unstable measurement) symbol will be shown on the display until the reading

becomes stable.

• When the reading is stable and close to the selected buffer, the  (unstable measurement)

symbol will disappear and the 

Confirm

 key will become active.

• Press 

Confirm

 to confirm the calibration. The instrument stores the calibration value and returns to pH

meter/titrator calibration menu, where the date and time for the last pH calibration will be updated.

Notes:

• A buffer confirmed during the calibration process is removed from the list of calibration buffers

available for further calibration points.

• If the value measured by the instrument is not close to the selected buffer a 

“Wrong Buffer”

error message will be shown on the display.

Check if the correct buffer has been used or regenerate the pH electrodes by following the

Cleaning Procedure (see the “pH Cleaning Procedure” section). If necessary change the buffer

or the electrode.

• When the reading is stable and close to the selected buffer, the  (unstable measurement)

symbol will disappear and the 

Confirm

 key will become active.

• Press 

Confirm

 to confirm the calibration.

• Press 

ESC 

to exit calibration.

Notes:

• To clear a previous calibration and to return to the default value, press 

Clear 

at any time

after entering calibration mode. The 

“Calibration cleared”

 message will be shown for

a few seconds on the display. If 

Clear 

is invoked during the first calibration point the

instrument returns to the measurement mode.

• The 

Clear 

key is displayed only if a previous calibration exists.

Point 2 calibration

• The calibrated value will be shown on the display and the second expected buffer value will be displayed.
• Remove the electrode holder with electrodes from the top of the beaker.
•  Place the second buffer into the beaker and place in beaker holder. Rinse the electrodes in a

beaker containing the second buffer rinsing solution.

•  Place the electrode holder (with electrodes) on the top of the beaker, lock cap by turning.
• If necessary press the 

ARROW 

keys in order to select a different buffer value.

• The  (unstable measurement) symbol will be shown on the display until the reading becomes stable.
• When the reading is stable and close to the selected buffer, the  (unstable measurement)

symbol will disappear and the 

Confirm

 key will become active.

• Press 

Confirm

 to confirm the calibration.

Содержание HI 84430

Страница 1: ...1 Instruction Manual HI 84430 TOTAL ACIDITY MINITITRATOR pH METER for Water Analysis www hannainst com...

Страница 2: ...mail us at tech hannainst com This instrument is in compliance with directives TABLE OF CONTENTS PRELIMINARY EXAMINATION 4 GENERAL DESCRIPTION 4 SPECIFICATIONS 6 PRINCIPLE OF OPERATION 8 FUNCTIONAL AN...

Страница 3: ...precipitates solids suspensions oils samples containing polyvalent cations aluminum iron manganese chromium may react slowly with the titrant causing a drifting end point To eliminate or diminish the...

Страница 4: ...le acidity high range mg L 400 4000 mg L as CaCO3 meq L 8 80 meq L as CaCO3 Resolution Titratable acidity low range 0 1 mg L 0 1 meq L Titratable acidity high range 1mg L 1meq L Accuracy 5 of reading...

Страница 5: ...than 3 7 only total acidity can be determined The HI 84430 utilizes two different titrant solutions to cover the entire measurement range The titrantsusedhavedifferentconcentrations appropriateforeach...

Страница 6: ...titrator top Purge the titrant Calibrate the pump Prepare the sample Run a titration and log sample results 5 Functional key area 6 Indicates that the displayed value can be changed using ARROW keys 7...

Страница 7: ...ut saving the new value pH resolution Options 0 1 0 01 Press the displayed function key in order to change the pH resolution Options C F Press the function key in order to change the temperature unit...

Страница 8: ...es on the screen Press the function key to select this option Tutorial Option AM PM or 24 hours Press the functional key to select the new value Time format Press to highlight the value to be modified...

Страница 9: ...ial link between the instrument and a PC Both must use the same setting Baud rate Option 0 to 9999 This option is used to set the instrument s ID The instrument ID is used while exchanging data with a...

Страница 10: ...olution to be used for the first calibration point Put the first beaker with calibration buffer in the beaker holder Place the electrode holder on the top of the beaker and secure it by turning clockw...

Страница 11: ...heck if the correct buffer has been used or regenerate the pH electrodes by following the Cleaning Procedure see the pH Cleaning Procedure section If necessary change the buffer or the electrode When...

Страница 12: ...temperature reading is out of the defined temperature range of the buffer 0 to 45 C the Wrong Buffer Temperature error message will be displayed and the symbol C will blink on the display Calibration...

Страница 13: ...key from the titrator main screen The purging stops automatically after 5 minutes To access the Purge key follow the next steps From the instrument main screen pH meter screen press Titrator function...

Страница 14: ...he electrode holder on the top of the beaker and secure it by turning clockwise Immerse the pH electrode approximatively 2 cm 0 8 into the standard paying attention not to touch the stir bar Insert th...

Страница 15: ...the beaker and secure it by turning clockwise Insert the temperature probe into the dedicated guide tube Immerse the pH electrode approximatively 2 cm 0 8 into the sample to be tested paying attention...

Страница 16: ...t of range the symbol is displayed in front of the reading From the titrator main screen press Titration To enter titrator main screen from pH meter mode press Titrator and then Titration If the tutor...

Страница 17: ...a calibration hasn t been performed the message Not Calibrated will be displayed If GLP pump is pressed one of the next screens is displayed Press Delete to enter record deleting mode Press Delete Al...

Страница 18: ...ayed preceded by the symbol and the MTC message The manually set temperature can now be adjusted with the ARROW keys from 20 0 to 120 0 C pH MEASUREMENT The HI 84430 may be used as a pH meter for dire...

Страница 19: ...to return to the previous screen without deleting If the pH log is empty the message No Records will be displayed VIEW DELETE RECORDED pH DATA To view or delete previously logged pH records press MEN...

Страница 20: ...eference thermometer The unstable measurement symbol will be shown on the display until the reading becomes stable When the reading is stable and close to the selected calibration point the unstable m...

Страница 21: ...he HI 92000 Windows compatible software optional HI 92000 also offers graphing and on line help features Data can be exported to the most popular spreadsheet programs for further analysis To connect y...

Страница 22: ...arameters setting The answer string contains Instrument ID 4 chars Calibration alarm time out 2 chars Concentration unit 1 char 0 mg L 1 meq L Acidity type 1 char 0 Total LR 1 Total HR 2 Strong LR 3 S...

Страница 23: ...o s p u s e t a u t c u l f g n i d a e R e s i o n n w o d d n a n o i t c n u j y t r i d d e g g o l C l e v e l e t y l o r t c e l e w o L s e d o r t c e l e H p e l b a l l i f e r y l n o n o...

Страница 24: ...ake all necessary steps to correct interferences Any variation introduced by the user to the supplied equipment may degrade the instrument EMC performance To avoid damages or burns do not put the inst...

Страница 25: ...l 210 823 5192 Fax 210 884 0210 Indonesia Tel 210 4584 2941 Fax 210 4584 2942 Japan Tel 03 3258 9565 Fax 03 3258 9567 Korea Tel 02 2278 5147 Fax 02 2264 1729 Malaysia Tel 603 5638 9940 Fax 603 5638 98...

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