Hach PHC729 Скачать руководство пользователя страница 18

Section 9 Troubleshooting

Problem

Possible cause

Solution

Decreased probe performance
causes slow stabilization and
prevents accurate calibrations or
measurements.

The glass sensor is dirty.

Clean and condition the probe.
Refer to 

Clean the probe

on page 11.

The reference junction is
clogged.

Clean and condition the probe.
Refer to 

Clean the probe

on page 11.

The filling solution has
contamination.

Replace the filling solution.
Refer to 

Replace the filling

solution

 on page 14.

The probe is not conditioned
to the sample sufficiently.

Condition the probe. Refer to 

Preparation for use

 on page 5.

The glass sensor has
become dry.

Soak the probe tip in buffer
solutions. Refer to 

Soak

procedure for dry probes

on page 15.

The calibration slope of the
probe has changed.

Increase the accepted slope limit
settings if possible, or contact
technical support.

Sample properties cause slow
stabilization or inaccurate
measurements.

The sample temperature is
low, or there is a large
temperature difference
between samples.

Increase the sample
temperature or adjust the
temperature of different samples
to be the same (within 2 °C
(3.6 °F)).

Procedure problem causes slow
stabilization and prevents
accurate calibrations or
measurements.

The filling hole is closed.

Open the filling hole during use.

The electrical connection
through the reference
junction is not sufficient.

Shake the probe in the buffer
solution or adjust the probe on
the sample surface to refresh
the reference junction.

An incorrect buffer solution
was used or the buffer
solution has contamination.

Use the specified buffer
solutions of good quality.

The protective tape was not
removed from the filling
hole.

Remove the tape from the filling
hole. Refer to 

Preparation for

use

 on page 5.

Section 10 Consumables

Note: Product and Article numbers may vary for some selling regions. Contact the appropriate distributor or refer to
the company website for contact information.

Description

Quantity

Item no.

Electrode filling solution, saturated KCl

59 mL

1

25118026 

KCl crystals

15 g

S21M001 

Electrode cleaning solution for regular maintenance

500 mL

2965249 

1

Larger quantities are available.

16

   

English

Содержание PHC729

Страница 1: ...DOC022 53 80433 PHC729 05 2021 Edition 2 User Manual...

Страница 2: ......

Страница 3: ...rocedure 8 Section 6 Sample measurement 9 6 1 Sample requirements 9 6 2 Sample measurement notes 9 6 3 Sample measurement procedure 9 Section 7 Verify the calibration 10 7 1 Verification procedure 10...

Страница 4: ...Table of Contents 2...

Страница 5: ...r the best accuracy do not use the probe to measure the pH of very alkaline samples Figure 1 Probe overview 1 Probe soaker bottle with storage solution 5 Probe soaker bottle holder 2 Filling hole plug...

Страница 6: ...but not improper use or wear Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical PHC729 probe is intended for use by individuals in the laboratory who measure the p...

Страница 7: ...probe with a blocked filling hole will not operate correctly New probes are filled with electrolyte filling solution and have a soaker bottle that contains storage solution to keep the glass bulb and...

Страница 8: ...e meter starts for the first time or after battery replacement 8 Connect the probe to the meter 9 Remove the filling hole plug before use Keep the level of the electrolyte filling solution above the l...

Страница 9: ...2 or more pH units apart For a one point calibration use a pH buffer near the expected sample pH Use the default calibration options or change the options in the probe settings menu Use the single di...

Страница 10: ...ffer solution Make sure that the sensor and reference junction are fully in the solution Do not put the probe on the bottom or sides of the beaker 6 Shake the probe from side to side to refresh the re...

Страница 11: ...e specified operating temperature of the probe Refer to Specifications on page 3 6 2 Sample measurement notes Read the notes that follow before sample measurements Rinse the probe with deionized water...

Страница 12: ...ay shows the pH buffer solution to use for verification Note Menu name for HQd meters Run check standard 2 Prepare or pour the pH buffer solution into a beaker 3 Open the filling hole 4 Rinse the prob...

Страница 13: ...ater Dry the probe body with a lint free cloth 4 Soak the probe in pH 4 buffer for 20 minutes 5 Rinse the probe with deionized water Dry the probe body with a lint free cloth Table 1 Cleaning solution...

Страница 14: ...crystals to the probe The filling solution in the probe contains crystals of potassium chloride KCl that keeps the filling solution saturated with KCl When the sample temperature is more than 60 C 140...

Страница 15: ...ttle 2 Measuring scoop 5 Saturated KCl solution 3 KCl crystals Table 2 KCl quantity at high temperatures Temperature KCl quantity 60 C 140 F 0 5 g 0 5 cm 0 2 in 70 C 158 F 0 625 g 80 C 176 F 0 750 g 9...

Страница 16: ...d KCl crystals from the probe as possible Discard the solution and KCl crystals 3 Remove the remaining KCl crystals as follows a Fill the probe half full with deionized water Close the filling hole b...

Страница 17: ...N O T I C E Probes can become permanently damaged if kept in a storage solution that is not specified by the manufacturer Use only the specified storage solution saturated KCl Do not store the probe i...

Страница 18: ...perature difference between samples Increase the sample temperature or adjust the temperature of different samples to be the same within 2 C 3 6 F Procedure problem causes slow stabilization and preve...

Страница 19: ...lution kit Singlet one use packets 20 mL each 2 x 10 pkg 2769920 pH 7 00 and 10 01 buffer solution kit Singlet one use packets 20 mL each 2 x 10 pkg 2769820 pH color coded buffer solution kit NIST 500...

Страница 20: ...5013 Beaker 30 mL plastic green 80 pkg SM5014 Beaker dispenser and holder 30 mL 1 923 656 Beaker holder 30 mL 1 923 556 Beaker 100 mL polypropylene 1 108042 Filling hole plug clip on 1 M035J35 LIS low...

Страница 21: ......

Страница 22: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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